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68results about How to "Complete chemical reaction" patented technology

Technology for making acid by combined incineration of waste sulfuric acid and hydrogen sulfide and used incinerator

The invention relates to a technology for making acid by combined incineration of waste sulfuric acid and hydrogen sulfide, and a used incinerator. The technology comprises the following steps: (1) atomizing the waste sulfuric acid, with concentration of greater than or equal to 75%, as a by-product in an oil refinery to form acid mist by combining high pressure pump conveying mechanical atomization with compressed air auxiliary atomization, wherein the grain diameter is smaller than or equal to 80 microns; (2) completely mixing hydrogen sulfide gas, with concentration of 0 to 50%, as the by-product in the oil refinery with hot air in a cyclone air inlet to product mixed gas; and (3) spraying the acid mist into the incinerator by using a waste acid spray gun, meanwhile spraying the mixed gas of hydrogen sulfide gas and hot air into the incinerator by a hydrogen sulfide spray gun and carrying out incineration, pyrolysis and reduction reaction to generate SO2 burner gas, wherein the SO2 burner gas enters an acid making system after the heat is recycled through a heat recovery boiler. During the reaction, the grain diameter of the acid mist is smaller than or equal to 80 microns, and the acid mist is introduced into the incinerator at the same time, so that various reactions can be performed completely and heat loss is reduced furthest at the same time, and produced products meet the requirement of the subsequent acid making technology.
Owner:JIANGSU YONGJI CHEM EQUIP

Method and device for preparing nickel iron roasted ore by utilizing lateritic nickel ore

ActiveCN103468930AFast heat and mass transferShorten decrystallization wateChemical reactionLaterite
The invention discloses a method and a device for preparing a nickel iron roasted ore by utilizing a lateritic nickel ore. The method comprises the following steps: firstly, grinding the lateritic nickel ore into an ore powder, then carrying out high-temperature roasting of the obtained ore powder, during the high-temperature roasting process, allowing the ore powder to be in a pre-reduction system and carry out a high-temperature preheating reduction reaction, followed by allowing the high-temperature roasted ore to go into a rotary kiln for high-temperature calcination, thus obtaining a roasted ore containing nickel pig iron after completing high-temperature calcination, and then after dipping the roasted ore into water for cooling, separating to obtain the nickel iron roasted ore. The device comprises a hopper-type elevator, an air chute, a chute draught fan, a rotary feeder, a sluice valve, a rotary kiln, a water-cooling stirring tank, a burner, a hot wind mixing chamber, a high-temperature draught fan, a cyclone dust remover, a bag-type dust remover, a chain-type conveyor, a burner and a pre-reduction system. The preparation method and the device allow the heat transfer area of the ore powder to be large, enable each particle to be uniformly and fully subjected to a chemical reaction, have short reaction time, and have high utilization rate of the lateritic nickel ore.
Owner:WUHAN BUILDING MATERIAL IND DESIGN & RES INST

Blowing-type induction melting furnace

The invention provides a blowing-type induction melting furnace which comprises a furnace body, an air brick, a mechanical stirring system, a blowing system and an induction system, wherein the furnace body and a refractory crucible of the induction system form a molten pool; the inner wall of the furnace body and the induction system are partitioned and sealed through a thermal insulation material; the air brick is arranged at the bottom part or the side wall of the furnace body, directly passes through the furnace body and is communicated with the induction system and the molten pool; the mechanical stirring system comprises a mixing propeller and a control box; the mixing propeller is inserted into the molten pool and controls the rotating speed when working through the control box; the blowing system comprises a gas source and a high-pressure carrier gas transmission pipeline, and is connected with the bottom part of the furnace body through the high-pressure carrier gas transmission pipeline; an air outlet of the pipeline is opposite to the air brick; the induction system comprises an induction coil, an electromagnetic induction body, the refractory crucible and the thermal insulation material; the induction coil is in tight contact with the thermal insulation material on the inner wall of the furnace body; the thermal insulation material is arranged between the induction coil and the electromagnetic induction body; and the refractory crucible is located on the innermost layer.
Owner:NORTHEASTERN UNIV

Preparation technique of methanol by lignite gasification and special equipment thereof

The invention relates to a process for preparing methanol from brown coal in gasification, which is characterized in that: the brown coal is crushed to brown coal powder of less 8; the brown coal powder is arranged into a totally-enclosed processing warehouse for being dried, and then is delivered into a direct-injection fluidization and gasification gas furnace in inside and outside cycle; the air and vapor are mixed to prepare the gasification agent with rich oxygen by adopting a transformation oxygen-enrichment adsorption process unit; the gasification agent is delivered into a furnace from the bottom of the direct-injection fluidization and gasification gas furnace in inside and outside cycle; and the clean water is sprayed into the furnace from the bottom. The fully mixed material in the furnace is implemented on high temperature and high pressure, so that which is cracked to generate the air with rich methanol, further, the high-purity methanol can be generated when the air with rich methanol is processed through separation, desulfurization, decarbonization and purification. The adaptability of low-quality feed coal can be expanded by taking the low-quality as raw material according to the process for preparing methanol, thereby the utilization rate of the desulfurization and gasification on the feed coal can be improved; the energy consumption can be lowered, the environmental quality can be improved; and the economical efficiency is stronger. The invention also provides special equipment so as to meet the needs of the process.
Owner:单晓强 +2

Production method for barium stearate

InactiveCN103694100AAvoid clumpingTo prevent the disadvantages of unqualified high free acid contentOrganic compound preparationCarboxylic acid salt preparationChemical reactionWastewater
The invention discloses a production method for barium stearate. The production method comprises the following steps: 1) adding water into a reactor and starting stirring and heating; 2) with water as a reaction dispersion medium and under the conditions of stirring and heating, adding powdery barium hydroxide at normal pressure so as to form a barium hydroxide suspension, then adding subparticle stearic acid while stirring when temperature reaches 50 to 60 DEG C, stopping heating when temperature reaches 65 to 66 DEG C and carrying out a reaction for 20 to 30 min when temperature rises to 69 to 70 DEG C caused by reaction exotherm; and 3) subjecting a reaction product to filtering separation, drying and crushing so as to obtain a barium stearate product. The production method provided by the invention realizes a complete chemical reaction of stearic acid with barium hydroxide under the reaction condition that a catalyst is not added and has low requirements on equipment; process flow is simple; the reaction medium water can be cyclically used, so no waste water is discharged, causing no pollution to the environment; reaction temperature is low, and little energy is consumed; no catalyst is needed, and production cost is reduced.
Owner:GUANGZHOU VOCATIONAL COLLEGE OF SCI & TECH

Online rapid pickling device and method for condenser in power plant

ActiveCN104596350ASimple structureReduced positioning accuracy requirementsFlush cleaningPropellerEngineering
The invention discloses an online rapid pickling device and method for a condenser in a power plant. The online rapid pickling device comprises a pickling liquid distribution device and a servo motor which are arranged outside a condenser water chamber, wherein an underwater positioning device for accurately positioning and a rapid filler for injecting pickling liquid are arranged in the condenser water chamber; the servo device is connected with the underwater positioning device; the pickling liquid distribution device is connected with the rapid filler; the servo device is used for transmitting a command to an underwater vertical positioning device in order to drive the rapid filler on a vertical coupler support to arrive at a specified area; a propeller on the support is used for driving the rapid filler to move forwards to be in hermetical butt joint with a condenser tube plate; the liquid distribution device is used for supplying pickling liquid to the rapid filler; the rapid filler is used for filling the pickling liquid into a plurality of rows of condenser heat exchange tubes in a covered area; after set cleaning and soaking time is reached, the rapid filler is separated from the condenser tube plate under the driving action of the propeller, and moves to a next area according to a set program for cleaning continually. By adopting the online rapid pickling device and method, the cleaning time is shortened greatly, the equipment running reliability is enhanced, and the cleaning cost of the condenser is lowered.
Owner:徐州比此智能科技有限公司

Method for pre-treating complex indium-containing smoke dust by microwave roasting

The invention provides a method for pre-treating complex indium-containing smoke dust by microwave roasting. The method comprises the following steps of: uniformly mixing the complex indium-containing smoke dust with concentrated sulphuric acid, and then roasting the mixture for 0.5 hour to 3 hours at 100 DEG C to 250 DEG C under the condition with microwave powder or 300W-500W to obtain a roasted product; crushing the roasted product, stirring and soaking the crushed rotated product in a sulphuric acid solution for 0.5 hour to 2 hours at 23 DEG C to 50 DEG C, so as to obtain leachate and leached residue by carrying out solid-liquid separation, wherein the leaching efficiency of easy-soluble valuable metals such as indium, zinc and the like in the materials is higher than 95%; and extracting the indium in the complex indium-containing smoke dust by leafing most of the metals such as lead, iron and the like in the slag. The method disclosed by the invention has the technical characteristics of being high in metal leaching efficiency, small in reagent consumption amount, short in treatment time, low in energy consumption, concentrated in valuable metals. Most of the metals such as the lead, the iron and the like are left in the slag, so that beneficial conditions are created for the subsequent indium treatment process.
Owner:KUNMING UNIV OF SCI & TECH

Online precision chemical descaling device and method of industrial tube nest type water cooler

The invention discloses an online precision chemical descaling device and method thereof of an industrial tube nest type water cooler. A descaling agent distribution device and a servo control device are arranged outside a water chamber of the water cooler, an underwater positioning device and a descaling agent injection device are mounted in the water chamber of the water cooler, the underwater positioning device is connected with the servo control device through a waterproof cable, the descaling agent distribution device is connected with the descaling agent injection device through a guide tube, the servo control device transmits commands to the underwater positioning device, descaling agent injection nozzles on a driving support and orifices of cooler heat exchange tubes are docked, and the descaling agent distribution device supplies descaling agent to the descaling agent into the descaling agent injection nozzles. After set washing and soaking time is up, the descaling agent injection nozzles are separated from docking with the orifices of the cooler heat exchange tubes under drive of the servo control device and automatically move to inlets of the next group of cooler heat exchange tubes. On the premise of zero emission, reliability of operating of the equipment is improved, cleaning cost of the cooler is greatly reduced, and cleaning effect is greatly improved.
Owner:徐州比此智能科技有限公司

Zero emission treatment system and zero emission treatment method for desulfurization waste water from ultra-supercritical circulating fluid bed (CFB) boiler

The invention discloses a zero emission treatment system and a zero emission treatment method for desulfurization waste water from an ultra-supercritical circulating fluid bed (CFB) boiler. The zero emission treatment system comprises a chemical pretreatment system, a membrane filtration system, an electrodialysis system, a desulfurization waste water preheating system, a desulfurization waste water evaporator, a solid-liquid separation device and a vapor condensation device. High-temperature flue gas at an exit position of a cyclone separator of the ultra-supercritical CFB boiler is used as aheat source to evaporate and crystallize the desulfurization waste water, superheated steam at an inlet header of a rear platen superheater of the super-supercritical CFB boiler is used as a heat source for the preheated desulfurization waste water, and the membrane filtration system provided with a microfiltration device and the electrodialysis system used for concentration reduction are additionally arranged, so that the defects of high energy consumption and high equipment investment cost of the existing multi-effect evaporation technology are overcome, the desulfurization efficiency can be improved, equipment scaling is effectively avoided, system handling load is reduced, economic benefit is significantly improved, the energy is saved, and the operating cost is reduced.
Owner:XI AN JIAOTONG UNIV

Isothermal self-compensating type liquid level adjusting water bath kettle

InactiveCN105498882ARealize the function of automatic water replenishment (water with the same water temperature)Added automatic compensation functionWater/sand/air bathsTemperature controlWater baths
The invention relates to an isothermal self-compensating type liquid level adjusting water bath kettle which comprises a water bath kettle body, a first temperature controller for controlling the temperature of a water bath area of the water bath kettle, and a water supplementing tank, a first liquid level controller (1), a second liquid level controller (2) and a second temperature controller, wherein the water bath kettle body is arranged in the water supplementing tank, a liquid level water supplementing area (7) is arranged between the inner wall of the water supplementing tank and the outer wall of the water bath kettle body, the first liquid level controller (1) is arranged at a lower part of the water bath kettle body and is used for control water input when the liquid level of a water bath kettle water bath area (6) is too low, the second liquid level controller (2) is arranged at an upper part of the water supplementing tank and is used for control water input when the liquid level of the liquid level water supplementing area (7) is too low, and the second temperature controller is used for controlling the temperature of the liquid level water supplementing area (7) to keep consistent with the temperature of the water bath kettle water bath area (6). The isothermal self-compensating type liquid level adjusting water bath kettle can realize the function of unmanned water self-compensation (water at the same temperature).
Owner:TIANJIN ENVIRONMENT MONITORING CENT

Chemical reaction kettle with automatic temperature changing function

The invention belongs to the technical field of reaction kettles, and particularly discloses a chemical reaction kettle with an automatic temperature changing function. The chemical reaction kettle comprises a base, an electric heating wire plate, a lithium battery, a kettle body, a control box, a control panel, a displayer, an indicator lamp, a timer, a buzzer, a cooling pipe, a fixing ring, a temperature sensor, a top cover, a fixing pipe, a slider, a connecting rod, a movable frame, a rack plate, a fixing plate, a half gear, a first motor, an arc-shaped groove, a second motor, a fixing block, a stirring shaft, a stirring plate and side holes. The chemical reaction kettle is reasonable in structure; the temperature in the kettle body is detected through the temperature sensor, the temperature in the kettle body is displayed on the displayer, the kettle body is heated through the electric heating wire plate, the temperature in the kettle body is raised, cold water is guided into the cooling pipe for cooling the interior of the kettle body, the heating time and cooling time are calculated through the timer, temperature changing is more accurate, the heating or cooling state is displayed through the indicator lamp, and workers are reminded through the buzzer.
Owner:陆挚译

Multi-step preparation chemical reaction device

The invention belongs to the technical field of chemical reaction, and provides a multi-step preparation chemical reaction device, which includes a box, at least two primary reaction devices and a secondary reaction device are arranged in the box; the primary reaction device includes a primary reaction Pool and electromagnetic stirrer, thermocouples and heating rods are respectively arranged on both sides of the primary reaction pool, at least two injectors and a condenser are provided in the primary reaction pool; the secondary reaction device is arranged under the primary reaction device, The secondary reaction device comprises a secondary reaction pool, which is also provided with a thermocouple and a heating rod, and the secondary reaction pool is provided with a stirring device and a condensation pipe; the outlet end of the discharge pipe extends into the secondary reaction pool, It also includes a tail gas absorption bottle, the injector is provided with a funnel, a metering tube, a feeding tube and a recovery tube are arranged under the funnel, and a recovery bottle is arranged under the recovery tube. The multi-step preparation chemical reaction device provided by the invention has the advantages of simple operation, easy cleaning, rapid multi-step reaction and recovery of redundant reaction reagents.
Owner:廖允泰

Method for preparing manganese sulfate by using manganese dioxide ore pulp to absorb sulfur dioxide in flue gases

ActiveCN102815750BLess solidMeet the requirements of flue gas desulfurizationChemical industryManganese sulfatesManganese sulphateFlue gas
The invention discloses a method for preparing manganese sulfate by absorbing sulfur dioxide in flue gas with manganese dioxide ore pulp, comprising the following steps: performing wet ball milling on manganese dioxide ore and grading to obtain initial ore pulp, and the particle size of the ore material in the initial ore pulp is less than 149 μm, the initial pulp is crushed by a vertical stirring mill to obtain a reaction pulp, and 90% of the particle size of the mineral material in the reaction pulp is below 50 μm; add a manganese sulfate solution containing Fe3+ and / or Fe2+ to the obtained reaction pulp, and then make the reaction pulp Absorption reaction with high-temperature flue gas containing sulfur dioxide, the reaction temperature is controlled at 90 ° C ~ 95 ° C; after the completion of the absorption reaction, the reaction product is subjected to solid-liquid separation, iron and heavy metal removal, and then concentrated and crystallized under normal pressure to obtain monohydrate Manganese sulfate. The method of the invention has the advantages of energy saving and environmental protection, high resource utilization rate, high product added value, good flue gas desulfurization effect, continuous and thorough reaction, low cost and the like.
Owner:GUIZHOU DALONG HUICHENG NEW MATERIAL CO LTD

Novel semi-ecological sewage treatment process

The invention discloses a new process for semi-ecological sewage treatment, which comprises a sewage treatment tank, a sewage storage room is arranged at the lower part of the sewage treatment tank, a support layer is set above the sewage storage room, a filter material layer is provided above the support layer, and a filter material layer is arranged above the support layer. The material layer includes a filter layer and an organism ecological treatment layer. An aeration pipe is provided at the bottom of the sewage holding room. The bottom of the sewage holding room is also connected to a water inlet pipe. The other end of the water inlet pipe is connected to a sewage separator. The sewage separator includes a separation device and Circulating water treatment device. By combining physical purification and biological purification, the present invention avoids the problem of long purification time in the simple ecological treatment of sewage, and at the same time avoids the excessive pollution of sewage entering the ecological sewage treatment pool, which will cause the microorganisms to be in the sewage The environment is harsh, which leads to low sewage treatment efficiency, poor water quality after treatment, and the phenomenon that the water cannot be completely up to standard, which can ensure that the sewage can be completely purified.
Owner:王攀

Production method for barium stearate

InactiveCN103694100BAvoid clumpingTo prevent the disadvantages of unqualified high free acid contentOrganic compound preparationCarboxylic acid salt preparationChemical reactionReaction temperature
The invention discloses a production method for barium stearate. The production method comprises the following steps: 1) adding water into a reactor and starting stirring and heating; 2) with water as a reaction dispersion medium and under the conditions of stirring and heating, adding powdery barium hydroxide at normal pressure so as to form a barium hydroxide suspension, then adding subparticle stearic acid while stirring when temperature reaches 50 to 60 DEG C, stopping heating when temperature reaches 65 to 66 DEG C and carrying out a reaction for 20 to 30 min when temperature rises to 69 to 70 DEG C caused by reaction exotherm; and 3) subjecting a reaction product to filtering separation, drying and crushing so as to obtain a barium stearate product. The production method provided by the invention realizes a complete chemical reaction of stearic acid with barium hydroxide under the reaction condition that a catalyst is not added and has low requirements on equipment; process flow is simple; the reaction medium water can be cyclically used, so no waste water is discharged, causing no pollution to the environment; reaction temperature is low, and little energy is consumed; no catalyst is needed, and production cost is reduced.
Owner:GUANGZHOU VOCATIONAL COLLEGE OF SCI & TECH
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