522results about How to "Fine and uniform grain" patented technology

The invention discloses micro-alloying seamless pipeline steel and process for preparation. According to weight percentage, the range of the chemical components of the invention includes that C holds 0.08% to 0.20%, Si is equal to or less than 0.04%, Mn takes 0.60% to 1. 50%, S is equal to or less than 0.015%, P is equal to or less than 0.025%, Al is equal to or less than 0.04%, Ti is equal to or less than 0.04%, H is equal to or less than 2.5*10-4%, O is equal to or less than 25*10-4%, the rest is Fe and unavoidable foreign matters. The process for preparation comprises technique steps, including smelting, refining, continuous casting, hot rolling and slow cooling. Round steel with the size of phi 70 to 150 millimeters can be produced by the process for preparation. The seamless pipeline steel of the invention has perfect anti-sulphide stress corrosion (SSC resistance) capability and anti-HIC property. The pipeline steel which can substitute for welding pipe can be utilized in the filed of oil pipeline and the like, and the invention increases the reliability of material and adaptability of variety, in particular being adaptable for the low submarine temperature and corrosion-resistant environment and for manufacture of thick-walled tubes.

The invention discloses a thick steel plate for a nuclear power plant containment. The nuclear power plant containment is 10-60mm in thickness. The thick steel plate comprises, by mass percent, 0.06-0.15% of C, 0.10-0.40% of Si, 1.0-1.5% of Mn, 0.10-0.30% of Mo, not more than 0.012% of P, not more than 0.003% of S, 0.015-0.050% of Al, 0.20-0.50% of Ni, and at least one of not more than 0.05% of V, not more than 0.03% of Ti, not more than 0.25% of Cr, not more than 0.03% of Nb, and 0.0005-0.0050% of Ca, and the balance Fe and other inevitable impurity. Correspondingly, the invention further discloses a manufacture method of the thick steel plate for the nuclear power plant containment. The thick steel plate for the nuclear power plant containment is high in rigidity, high in toughness, fine in impact toughness of base metal and heat affected zone at low temperature, and suitable for application in the manufacture field of nuclear power plant containments.

The invention discloses a fine-grain forging method for a large-size GH690 nickel-based alloy bar billet, and belongs to the technical field of forging. By using the composite technology of ingot billet homogenization and classified forging for preparing the GH690 nickel-based alloy bar billet, the grains of the bar billet for forging can be uniform and fine, thus meeting fine-grain structure homogeneity control requirements on final large-size alloy forgings; classified repeated upsetting-stretching cogging is performed on the basis of controlling a deformation temperature and the deformation amount of each heating number, the forgings are formed by hot upsetting by virtue of end part lubrication and horizontal restrain technologies, and rapidly cooled to eliminate grain coarsening caused by deformation heat effect, and finally, the forging structures with uniform carbides and fine grains are obtained.

The invention discloses a manufacturing method for a 2xxx series ultra-large-dimension aluminum alloy round ingot, and relates to the technical field of aluminum alloy processing. The method comprises the steps of material preparation, smelting, in-furnace refining, online refining, online filtering, semi-continuous casting, homogenization heat treatment, machining and ultrasonic flaw detection. Improvements are made in the aspects of smelting, in-furnace refining, online refining, online filtering, semi-continuous casting and the like, and a method capable of improving the cast ingot quality and improving the production efficiency is provided, so that the cast ingot is fine in tissue, uniform in component and free of other metallurgical defects, and has the specification reaching phi 900 mm to phi 1,340 mm, the grain size capable of reaching a first grade, the hydrogen content not greater than 0.10 ml/100 g Al and the finished product rate reaching greater than 90%.

The invention discloses hot work die steel capable of being used for a long term at the working condition of 600-700 DEG C and belongs to the field of material and preparation. The hot work die steelcomprises the following components in percentage by mass: 0.12-0.30 of C, equal to or less than 0.5 of Si, equal to or less than 0.5 of Mn, 1.0-3.0 of Cr, 1.5-2.5 of Mo, 0.3-1.2 of W, 0.5-1.6 of Ni, 0.2-1.0 of V, 0.03-0.15% of Nb, equal to or less than 0.05 of N, equal to or less than 0.03 of S, equal to or less than 0.03 of P, equal to or less than 3.5 of (Mo+W), equal to or less than 1.0 of (Nb+V) and the balance of Fe and unavoidable impurity elements. According to the hot work die steel, low carbon is adopted to form lath martensite so as to obtain high tenacity at room temperature and lowtemperature; through alloying of Cr, W, Mo, V, Nb and the like and the thermal deformation optimization and thermal treatment technology, solution strengthening is improved and MC and M2C type carbide still keeping stability at 600-700 DEG C is formed so as to obtain high temperature strength and thermal stability of the material. Compared with the commonly used hot work die steel at present including H13, 25Cr3Mo3NiNbZr and the like, the high temperature strength at 700 DEG C of the hot work die steel is improved by 50-100%, the tempering thermal stability is improved by 50-100%, the problemabout hot work die steel used at 600-700 DEG C is better solved, and the hot work die steel has longer service life at 600 DEG C and below.

The invention relates to a production method of 3003-brand cathode aluminum foil, which includes the following steps: a. raw materials are refined and rolled into a blank with the thickness of 6.5 mm to 8.5 mm; b. the blank obtained in step a is rolled into the blank with the thickness of 3.5 mm to 4.3 mm in a cooling mode to be uniformly annealed; c. the uniformly-annealed blank is rolled into the blank with the thickness of 0.3 mm to 0.5 mm in a cooling mode to be recrystallized and annealed; and d. the recrystallized-and-annealed blank is rolled into the 3003-brand cathode aluminum foil with the required thickness. The method of the invention enables the cost to be lower and the product quality to be better, the specific capacitance of the product is increased to be higher than 530 microfarads /cm<2>, and the highest specific capacitance can be 560 microfarads /cm<2>. The invention greatly improves the product competitive strength, reduces the disparity with abroad products, and makes a contribution for the trade progress.

The invention discloses sulphuric acid dew point corrosion resisting steel and a method for producing the same by continuously casting and rolling a thin steel billet with an electric furnace. The molten steel comprises the following chemical components by weight percent: 0.03-0.08 percent of C, 0.10-0.45 percent of Si, 0.40-1.0 percent of Mn, 0.025 percent of P or less, 0.035 percent of S or less, 0.15-0.50 percent of Cu, 0.40-1.0 percent of Cr, 0.02-0.15 percent of Sb, 0.04-0.30 percent of Ni and 0.01-0.05 percent of Ti and also comprises 100ppm of N or less. The thin steel billet is continuously cast at the speed of 3.5-5.5m/min, and the cast thin steel billet is placed in the electric furnace of 900-1050 DEG C, soaked at 1100-1200 DEG C, rolled at 1040-1120 DEG C, finally rolled at 850-920 DEG C and winded at 550-650 DEG C. The Cu-Cr-Sb composite micro-alloyed sulphuric acid dew point corrosion resisting steel having good mechanical performance, welding performance and corrosion resisting performance can be produced by continuously casting and rolling the thin steel billet with the electric furnace.

The invention provides a method for preparing 24CrNiMo bainite alloy steel by using a selective laser melting technology. The method includes the steps that a laser device is used for conducting scanning on 24CrNiMo alloy steel power which is spread out on a base plate according to a preset selective laser melt scanning route till the power melts. According to the method, by optimizing technology parameters, taking use of the effects of alloy elements such as C, Cr, Ni, Mo, the bainite alloy steel which is uniform in microstructure is obtained at a high selective laser melting cooling speed, the average micro-hardness of the obtained bainite microstructure reaches 330-346 HV, the tensile strength is 962-978 Mpa, the elongation ratio is 16.4-17.6%, the product of tensile strength and elongation reaches 16.1-16.9 Gpa%, and the microstructure has excellent matched strength and toughness. The method and the technology are mainly applied to selective laser melting manufacture of 24CrNiMo alloy steel high speed rail brake discs.

A La-doped strontium titanate (SrTiO3)-based oxide thermoelectric material and a preparation method thereof, belonging to the technical field of energy materials. The method is divided into two parts of powder synthesis and forming of bulk materials. The powder synthesis adopts the sol-gel method, takes tetrabutyl titanate, strontium nitrate and lanthanum nitrate as raw materials, takes deionized water and ethanol as solvents and takes acetic acid and glycerol as a catalyst and a chelating agent to prepare SrTiO3 gel with different La doping amount, and the temperature is kept at the temperature of 500-560 DEG C for 1-2 hours to obtain precursor powder. The bulk forming adopts the spark plasma sintering method, and the sintering conditions are as follows: the vacuum degree is 2-10Pa, the pressure is 40-50MPa, the heating rate is 100 DEG C/min, the sintering temperature is 900-1000 DEG C, and the holding time is 5-10min. The method synthesizes the La-doped SrTiO3-based bulk thermoelectric material with high chemical homogeneity, uniform and fine grains and single-phase perovskite structure under the conditions of lower reaction temperature and shorter reaction time. The preparation method has the advantages of simple and convenient process, short synthesis and forming time, and the like.

The invention relates to a method for preparing a high performance magnesium alloy sheet, which belongs to the technical field of magnesium alloy preparation. The method is characterized by comprising: firstly, smelting out a magnesium alloy fused mass conforming to the requirements on components and then, adopting a double-roller rolling mill to produce rolling sheet blanks; heating the rolling sheet blanks to a set temperature so as to carry out hot rolling and matching with intermediate annealing in the hot rolling process so as to ensure that the sheets have perfect recrystallization and eliminate processing hardening; and subsequently, thermally rolling the hot rolled sheets to the needed thickness and carrying out final annealing on the magnesium alloy sheets so as to obtain the high performance magnesium alloy sheets with fine and uniform crystal grains. The prepared magnesium alloy sheets have the advantages of higher tensile strength, yield strength and elongation.

The invention discloses an abrasion-proof and corrosion-resistant nickel-based alloy wire and a preparation method thereof. The alloy wire comprises the following components: 17-21% of C, 20-25% of Co, 1.8-2.2% of W, 6.4-9.5% of Mo, 1.4-1.8% of Al, 3.2-4.5% of Ti, 0.1-0.5% of Nb, 0.1-0.5% of Hf, 1.2-1.8% of Ta, 0.03-0.06% of Re, 0.01-0.05% of Ce, 0.02-0.1% of C, 0.005-0.015% of B, 0.02-0.07% of Zr, 0.005-0.008% of Mg, and the balance Ni. The preparation technology of the alloy comprises the steps of vacuum smelting, remelting, forging, hot rolling, drawing, solid solution treatment and aging treatment, namely, raw materials are prepared and smelted based on mass percent and then smelted; the smelted materials are forged and rolled into obtain alloyed wire rods; the alloyed wire rods are drawn at a plurality of times to obtain phi 0.05-0.4mm alloy wires; finally the alloy wires are subjected to solid solution treatment and aging treatment. The abrasion-proof and corrosion-resistant nickel-based alloy wire can be used as a brush wire material for brush sealing of an aircraft engine, a gas turbine, etc., thus the brush sealing effect can be effectively improved, and the service life can be prolonged.

The invention provides a vacuum freeze dryer which comprises a material box, a water catching bin, a refrigerating unit, a heater, a vacuum pump and a control device. The material box is communicated with the water catching bin. The water catching bin is connected with the vacuum pump. The refrigerating unit and the heater are arranged outside the material box. The control device controls the refrigerating unit, the heater and the vacuum pump. The material box is internally provided with a refrigerating pipe and a heating pipe at the same time, and the refrigerating pipe and the heating pipe are used for freezing and drying materials respectively. The inner wall of a material frame and the inner wall of the material box are each provided with a temperature sensor, and the temperature sensors monitor the temperature of the material frame and the temperature of the material box. Materials inside a material bottle are frozen in advance to reach the eutectic point approximately, then the temperature is decreased rapidly, and the materials pass through the eutectic point within the short time as little as possible, so that the grain size of crystals is effectively controlled, the fine freeze-drying powder is obtained, and the freeze-dried powder product quality is improved. The freezing cavity and the drying cavity are integrated, the technological steps are simplified, the occupied space is small, and refrigerating and heating are uniform.

The invention relates to a preparation method of zirconium carbide ceramics powder; the method for rapidly preparing zirconium carbide ceramics powder is characterized in that: the method comprises the following steps: 1) raw material selection: the raw materials are selected according to 12:4-12:5 of mass ratio of zirconium propoxide solution and sugar and 8:32:1:1-8:64:2:4 of volume ratio of zirconium propoxide solution, normal propyl alcohol, chelant-acetic acid and water; the solvent acetic acid is selected according to (7-8)g:50ml of proportion of the sugar and the solvent acetic acid; 2) the preparation of dried gel power; 3) preparation of precursor powder; 4) heat treatment of the precursor powder; carbothermal reduction reaction is carried out under the conditions of high heating rate and short temperature preservation time, the synthesizing process of the zirconium carbide powder is shortened into dozens of minutes even several minutes, so as to obtain high-purity and refined zirconium carbide ceramics powder with good sintering character; single zirconium carbide phase can be analyzed by X-ray diffraction, the oxygen content in the product is 0.5-3 percent, and the free carbon content is from 0.2 to 2 percent; the crystal particles are uniform and tiny, and the mean grain size is less than 500nm.

A wide-temperature, high-frequency and low-loss manganese-zinc soft magnetic ferrite material comprises a main component, an auxiliary component A and an auxiliary component B, wherein, according to weight percentage, the main component comprises Fe2O3, MnO and ZnO; based on the weight of the main component, the auxiliary component A comprises at least two of CaCO3, V2O5, TiO2 and Co3O4, and the auxiliary component B comprises at least three of CaCO3, Nb2O5, TiO2, Co3O4, CuO, MoO and SiO2; the SiO2 amount in the auxiliary component B is determined according to the total amount of SiO2 impurities in the main component so as to ensure that in the whole material, the SiO2 amount is 0.025-0.035% of the total weight of the main component. A preparation method of the wide-temperature, high-frequency and low-loss manganese-zinc soft magnetic ferrite material sequentially comprises the following steps: performing component analysis on the main component, primarily dosing, primarily sanding, presintering, secondarily dosing, moulding and sintering. The wide-temperature, high-frequency and low-loss manganese-zinc soft magnetic ferrite material has excellent working performance under the conditions of 500KHz and 50mT and within the temperature range from -20 DEG C to 120 DEG C, has relatively low loss, saves more energy than the conventional material, and has lower standby loss at low temperature and room temperature.

The invention relates to a preparation method of an ultrahigh-purity aluminum target. The preparation method comprises the following steps: (1) the surface of an ultrahigh-purity aluminum ingot with a purity of higher than 99.999 wt% is milled to remove an oxide layer thereof; (2) the ingot is heated to 230-400 DEG C; (3) the hot rolling of 10-20 passes is performed for the heated ingot; the single-pass reduction is controlled within 20-60 mm; and the final rolling temperature in final pass is controlled below 350 DEG C; (4) the annealing treatment with a temperature of 200-300 DEG C and an insulation time of 1-2 h is performed for a hot-rolled aluminum plate; and (5) the plate is straightened for milling to obtain the ultrahigh-purity aluminum target with average grains of 80-150 microns. The preparation method can prepare the target with high purity, fine and uniform grains and consistent texture orientation to satisfy the use requirements of PVD; and meanwhile, the preparation method is simple in process, easy to operate and convenient for large-scale industrial production, effectively reduces the energy consumption, and reduces the cost.

The invention belongs to the technical field of cold rolled steel and discloses zinc-plated double-phase steel and a production method of the zinc-plated double-phase steel. The zinc-plated double-phase steel comprises, by weight percentage, 0.085%-0.115% of C, 0.15%-0.24% of Si, 1.45%-1.55% of Mn, not larger than 0.015% of P, not larger than 0.005% of S, 0.025%-0.065% of Alt, 0.14%-0.24% of Cr, 0.24%-0.29% of Mo, not larger than 0.006% of N and the balance Fe and other inevitable impurities. The production method includes the steps of KR desulfuration, converter steelmaking, LF+RH refining treatment, RH calcium treatment, continuous steel casing, billet heating, rough rolling, finish rolling, laminar cooling and winding; unwinding, acid pickling, cold continuous rolling and winding; and unwinding, cleaning, annealing, zinc plating, finishing and winding. Through composition design and process control, the zinc-plated double-phase steel is suitable for annealing production lines having the rapid cooling segment or not.

The invention discloses a cogging method for a large GH4738 high-temperature alloy ingot. According to the method, a bar billet with even and fine grains is obtained through multiple times of heading, drawing, forging and cogging conducted on a homogenized alloy steel ingot, so that the requirement for control over homogeneity of the fine-grained microstructure of the large-size alloy forge piece is met. In the forging and cogging control process, the cogging temperature, deformation amount and deformation speed are strictly controlled, heading, drawing and cogging are conducted repeatedly, forging is conducted by the adoption of glass lubricants and a coating insulation mode, and finally the bar billet of the even fine-grained microstructure is obtained. The cogging method can be applied to cogging and forging of the large GH4738 nickel-based high-temperature alloy ingot to produce the fine-grained bar billet.

The invention relates to a multi-pass drawing process method for manufacturing magnesium and magnesium alloy filaments. The prior production method has many middle annealing times, low production efficiency, low yield of a finished product, and high cost. The multi-pass drawing process method for manufacturing the magnesium and the magnesium alloy filaments comprises: a raw material of a fine crystal magnesium or magnesium alloy wire material with diameter of between phi 2 and 3 is selected; the raw material and a wire drawing mould are lubricated through a grease-type lube and are subjected to cold drawing for 5 to 12 times, and the cold drawing speed is between 120 and 150 mm/s; the raw material is recrystallized and annealed, the annealing temperature is between 400 and 420 DEG C, and the annealing time is between 1 and 3 minutes; and the process is repeated till the process is finished. The method is used for manufacturing the magnesium and the magnesium alloy filaments.

The invention relates to the manufacturing field of steel for a chrome-molybdenum heat resistant pressure container, in particular to a steel plate for a high toughness 15CrMoR pressure container. The steel plate is prepared by the following components in percentage by mass: 0.14-0.18% of C (Carbon), 0.15-0.40% of Si (Silicon), 0.45-0.70% of Mn (Manganese), no more than 0.020% of P (Phosphorus), no more than 0.005% of S (Sulfur), 0.90-1.10% of Cr (Chromium), 0.45-0.60% of Mo (Molybdenum) and the balance of Fe (Ferrum) and inevitable impurities. The steel plate for the high toughness 15CrMoR pressure container, provided by the invention, has the advantages as follows: (1) as impact toughness of 15CrMoR is high, low temperature impact performance is that transverse impact is not less than 80 J at -40 DEG C and far higher than the nationally specified transverse impact; (2) pure steel quality and low content of harmful elements such as S and the like; (3) as refined grain elements, such as Nb, V, Ti and the like, are not added, cost is greatly saved; and (4) when a requirement on low temperature toughness is satisfied, good conventional properties and good high-temperature tensile properties are obtained.

The invention discloses a rare earth treated normalized Q460GJ steel plate for buildings and a production method of the steel plate, and belongs to the technical field of steel for buildings. The steel plate comprises chemical components in percentage by weight as follows: 0.17-0.19% of C, 0.35-0.45% of Si, 1.50-1.60% of Mn, <=0.015% of P, <=0.010% of S, 0.03-0.04% of Nb, 0.05-0.06% of V, 0.01-0.02% of Ti, 0.2-0.3% of Ni, 0.020-0.040% of Als, 0.0010-0.0020% of rare earth La and the balance of Fe and impurities. The production method comprises the following steps: step I, smelting; step II, continuous casting; step III, heating; step IV, rolling and cooling; and step V, normalizing heat treatment. Therefore, the steel plate for buildings can be obtained, and the steel plate is in a metallographic structure of ferrites and pearlites with fine and uniform crystalline grains.

The invention relates to a high-strength thick steel plate with an excellent crack-arrest property. The steel plate has the following characteristics: a wide-plate tensile value Kca for determining the crack-arrest property is larger than 6000 N/mm<1.5>; yield strength at the positions, which are respectively 1/4 and 1/2 the thickness of the steel plate away from the surface of the steel plate, isno less than 460 MPa; tensile strength is 570 to 720 MPa; Charpy impact energy at minus 40 DEG C is no less than 200 J; and a zero-ductility transition temperature is less than minus 60 DEG C. The steel plate provided by the invention comprises the following components by weight: 0.04 to 0.16% of C, 0.1 to 0.5% of Si, 0.9 to 1.6% of Mn, 0.1 to 0.3% of Cu, 0.2 to 0.9% of Ni, no more than 0.02% ofP, no more than 0.02% of S, 0.01% to 0.05% of Als, 0.002 to 0.010% of N, 0.02% to 0.05% of Nb and 0.01 to 0.03% of Ti, with the balance being Fe and unavoidable impurities. According to the invention,through optimization of chemical components of a high-strength steel plate and adoption of controlled rolling and controlled cooling processes for controlling the microscopic structure and grain sizein a plate thickness direction, the crack-arrest steel plate with high yield and stable strength and toughness is obtained. The high-strength thick steel plate provided by the Invention is used as container vessel steel, and has the characteristics of excellent crack-arrest toughness, high yield strength, excellent low-temperature toughness and large thickness.