The application provides a kind of alkali
copper combined impregnated
activated carbon for protecting CNCl / HCN and
organic vapor and a preparation method, first, peach shell
activated carbon with certain pore structure is selected, then impregnated in two steps, first,
sodium alkali is impregnated into the inside of
activated carbon carrier channel, then
active component copper is impregnated into the inside of activated carbon carrier channel, wherein the
oxide generated by
thermal decomposition of Cu, Mo bimetallic impregnation solution has strong adsorption capacity for
cyanide, the presence of alkali can promote the
hydrolysis reaction of
cyanogen chloride, and the
hydrolysis product of adsorbed
cyanogen chloride is
hydrochloric acid. The unique pore structure of activated carbon and alkaline pretreatment are beneficial to the adsorption of DMMP
organic vapor. The application first uses vacuum ultrasonic impregnation and
water vapor activation to load the precursors of alkali and
copper into the inside of
macropore of activated carbon in turns, which not only makes the surface of impregnated carbon alkaline, but also makes the
active component fully absorbed and dispersed in the channel of activated carbon.