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140results about How to "Guaranteed pH" patented technology

Conductive low-smoke zero-halogen flame retarding and oil resisting cable sheath material and preparation method thereof

The invention relates to a conductive screening material, in particular to a conductive low-smoke zero-halogen flame retarding and oil resisting cable sheath material and a preparation method thereof. The conductive screening material comprises the following basic components: 100 parts of ethylene-vinyl acetate rubber, 50-100 parts of magnesium hydroxide, 50-80 parts of conductive black, 10-30 parts of graphite powder, 5-10 parts of zinc borate, 10-25 parts of plasticizer, 2-5 parts of lubricant, 1-2 parts of antiager, 10-30 parts of flame retarding synergist, 2-3 parts of vulcanizer and 1-2 parts of vulcanization assistant. The preparation method comprises the four steps of material preparation, mixing, extrusion and tabletting. The conductive low-smoke zero-halogen flame retarding and oil resisting cable sheath material has the advantages of high conductivity, good oil resistivity, excellent flame retarding effect, no peculiar smell, easy stripping and high heat resistance level, and can pass the environment protection authentication of RoHS (Restriction of the use of certain Hazardous Substances Registration), REACH (Evaluation, Authorization and Restriction of Chemicals) and the like.
Owner:中广核三角洲(江苏)塑化有限公司

Process for abstracting high-purity hemoglobin from pig blood

InactiveCN101289493AGuaranteed pHReduce the chance of denaturation inactivationPeptide preparation methodsHigh concentrationAntioxidant
The invention relates to a method for extracting high-purity hemoglobin from pig blood, and on the condition of 2 to 6 DEG C, the following operations are carried out sequentially: first, anticoagulant pig blood is used for preparing packed red blood cells; hypotonic solution is used for dissolving packed red blood cells, in which inert gas is pumped, antioxidant is added, the pH value of the solution is adjusted and protective agent and antibacterial drugs are added, and after high-speed centrifugation, crude hemoglobin solution is obtained; toluene is added into the crude hemoglobin solution which is extracted in low temperature and the hemoglobin solution in the lower layer is extracted for dialysis; after being frozen and dried the hemoglobin solution after dialysis is then dissolved into high-concentration and small-volume liquid which is then purified by a sephadex chromatography column as a sample and high-concentration hemoglobin with even molecular weight is obtained to be frozen and dried in vacuum after being filtered for removing pyrogen so as to prepare high-concentration hemoglobin dry powder with no matrix or pyrogen. The hemoglobin obtained through the method of the invention has no matrix or pyrogen, which can be further modified to produce blood substitute safely and effectively and the operation is simple; the cost is low.
Owner:INST OF FIELD OPERATION SURGERY NO 3 MILITARY MEDICL UNIV PLA

Continuous flow method for measuring total alkaloid in tobacco or tobacco products

The invention provides a continuous flow method for measuring total alkaloid in tobacco or tobacco products. In the method, potassium thiocyanate and sodium dichloro isocyanurate are adopted to carry out reactions to generate cyanogen chloride on line. The cyanogen chloride can carry out reactions with total alkaloid (calculated in the form of nicotine) in tobacco or tobacco products to break off the pyridine rings of nicotine, and then further carries out reactions with p-aminobenzene sulfonic acid. The reaction products are measured by a chromometer at 460 nm. The method uses a buffer system to control the pH value of the reaction system in a range of 6.0 to 7.5, and the buffer system is composed of a buffer solution A and a buffer solution B. The buffer solution A is prepared by the following steps: weighing disodium hydrogen phosphate and trisodium phosphate, placing the weighed substances in a beaker, dissolving the substances with water, transferring the solution to a volumetric flask (1L), and adding water into the volumetric flask until the water reaches the scale. The buffer solution B is prepared by the following steps: weighing p-aminobenzene sulfonic acid, disodium hydrogen phosphate, sodium dihydrogen phosphate, and sodium citrate, placing the weighed substances into a beaker, dissolving the substances with water, transferring the solution to a volumetric flask (1L), and then adding water into the volumetric flask until the water reaches the scale.
Owner:CHINA NAT TOBACCO QUALITY SUPERVISION & TEST CENT

Sieve-plate tower used for sintering machine flue gas desulfurization and desulfurization process thereof

The invention discloses a sieve-plate tower used for sintering machine flue gas desulfurization and a desulfurization process thereof, and belongs to the field of resource and environment protection. The device comprises an absorption tower, wherein the absorption tower is provided with a flue gas inlet, a flue gas outlet and a desulfurizer inlet, a demisting layer, a spraying layer, a sieve plate and a pulp chest are sequentially arranged in the absorption tower from top to bottom, the desulfurizer inlet is positioned above the flue gas inlet, the sieve plate is positioned between the desulfurizer inlet and the flue gas inlet, an overflow weir is arranged above the sieve plate, the sieve plate is divided into an overflow area and a gas liquid contact area by the overflow weir, sieve pores of the sieve plate are arranged in the gas liquid contact area, the gas liquid contact area is positioned at one side of the sieve plate close to the desulfurizer inlet, and an overflow pipe is arranged under the overflow area. The desulfurization process comprises the following steps that: sintering machine flue gas enters the absorption tower to be reacted with the desulfurizer at the gas liquid contact area and then is discharged after sulfur dioxide is removed, and desulfurized pulp generated by the reaction of the flue gas and the desulfurizer overflows into the pulp chest of the absorption tower. The invention is used for removing the sulfur dioxide in the sintering machine flue gas, the flue gas desulfurization efficiency is improved, and the desulphurization energy consumption is reduced.
Owner:ZHEJIANG TIANLAN ENVIRONMENTAL PROTECTION TECH

Method for preparing metal organic framework material

The present invention discloses a method for preparing a metal organic framework material. The method comprises: (1) preparing a metal precursor solution A; (2) preparing an organic ligand solution B; (3) respectively conveying the solutions A and the solution B into a micro-channel reactor module I to carry out in-situ generation of a MOFs crystal seed, carrying out a reaction for a certain time, and conveying the material liquid into a module II; (4) conveying the solution B into the module II when the material liquid enters the module II, carrying out crystal seed induction synthesis, carrying out a reaction for a certain time, and conveying the material liquid into a module III; (5) conveying a solvent C into the module III when the obtained material liquid enters the module III, and carrying out a solvent activation reaction; and (6) carrying out solid-liquid separation on the obtained suspension, washing the solid by using ethanol, and drying to obtain the product. According to the present invention, the multi-module micro-channel reactor is used, the MOFs crystal seed is subjected to in-situ generation in the module I, the crystal seed induction synthesis is performed in the module II, and the solvent activation reaction is completed in the module III, such that the advantages of simple and fast preparation process, narrow product particle size distribution, good dispersion and the like are provided.
Owner:CHINA PETROLEUM & CHEM CORP +1

Compound orthophaladetyde phenyl ammonium chloride disinfectant and preparation method thereof

The invention relates to a compound orthophaladetyde phenyl ammonium chloride disinfectant and a preparation method thereof. The compound orthophaladetyde phenyl ammonium chloride disinfectant comprises the following components by weight: 0.2-1 wt% of orthophaladetyde, 0.05-0.5 wt% of phenyl ammonium chloride, 0.1-1 wt% of dipotassium phosphate, 0.1-1 wt% of monopotassium phosphate, 0.1-0.3 wt% of sodium polyacrylate, 0.05-0.2 wt% of antioxidant, 0.01-0.1 wt% of disodium ethylene diamine tetraacetic acid and the balance of water. The preparation method of the compound orthophaladetyde phenyl ammonium chloride disinfectant comprises the following steps of: adding the orthophaladetyde into water according to the content and components, and stirring for dissolving; adding the dipotassium phosphate, the monopotassium phosphate, the sodium polyacrylate, the antioxidant and the disodium ethylene diamine tetraacetic acid in sequence, and stirring for dissolving; and adding the phenyl ammonium chloride, and stirring for dissolving to obtain the compound orthophaladetyde phenyl ammonium chloride disinfectant. The disinfectant is applicable to the high-level disinfection of thermolabile medical apparatus and instruments. The disinfectant has no pungent smell, safety, low toxicity, stable properties and convenient use.
Owner:SHANGHAI LIKANG DISINFECTION HIGH TECH

Assembly type grass-planted concrete precast block and construction method of ecological bank adopting same

The invention discloses an assembly type grass-planted concrete precast block and a construction method of an ecological bank adopting the same. The assembly type grass-planted concrete precast blockis composed of a convex block body and concave block bodies, wherein the convex block body and the concave block bodies are connected into a whole, the convex block body is located in the middle, theplurality of concave block bodies are arranged next to the convex block body, and the convex block body and the concave block bodies are made of ecological concrete with ecological holes; greening soil coverings suitable for the growth of herbaceous plants are laid on the upper surface of the convex block body and the upper surfaces of the concave block bodies respectively, the herbaceous plants take roots on the greening soil coverings and in the convex block body and the concave block bodies; and the concrete precast blocks can be spliced and clamped together. Meanwhile, the invention provides a construction method of the ecological bank adopting the assembly type grass-planted concrete precast block according to the characteristics of the assembly type grass-planted concrete precast block. The assembly type grass-planted concrete precast block has the advantages that the structure is reasonable, the coverage rate of the planted-grass is high and the construction is convenient and rapid; and the assembly type grass-planted concrete precast block can be used for ecological protection of medium and small rivers, and can also be used for ecological protection of channels, lakes, reservoirs and ponds.
Owner:NANCHANG INST OF TECH

O-phthalaldehyde disinfectant and preparation method thereof

The invention relates to an o-phthalaldehyde disinfectant and a preparation method thereof. The o-phthalaldehyde disinfectant comprises the following components in percentage by weight: 0.2 to 1 percent of o-phthalaldehyde, 0.1 to 0.5 percent of salicylic acid, 0.5 to 1.5 percent of dodecyldimethylbenzylammonium chloride, 1 to 10 percent of ethanol, 0.1 to 1 percent of disodium hydrogen phosphate, 1 to 10 percent of ethanol, 0.1 to 1 percent of sodium dihydrogen phosphate, 0.1 to 0.5 percent of inhibitor, 0.01 to 0.1 percent of ethylene diamine tetraacetic acid and the balance of water. The method for preparing the disinfectant comprises the steps of: adding the o-phthalaldehyde into the ethanol according to the content and component, stirring and mixing the materials; adding water into the materials and stirring the mixture; and adding the dodecyldimethylbenzylammonium chloride, the disodium hydrogen phosphate, the sodium dihydrogen phosphate, the inhibitor and the ethylene diamine tetraacetic acid into the mixture in sequence and stirring the mixed solution to allow the added materials to dissolve to obtain the o-phthalaldehyde disinfectant. The disinfectant has the advantages of no pungent smell, safety, low toxicity, stable property and convenient use, can be used for high-level disinfection of the heat-labile medical equipment and is particularly applicable to an endoscope automatic washing and disinfecting machine to perform high-level disinfection on an endoscope.
Owner:SHANGHAI LIKANG DISINFECTION HIGH TECH

Detecting method of specific capacity of negative electrode material of lithium ion battery after circulation

The invention discloses a detecting method of specific capacity of negative electrode material of a lithium ion battery after circulation. The detecting method comprises the following steps: 1) discharging the lithium ion battery after circulation, then dismantling the battery and taking out a negative electrode plate; 2) washing the negative electrode plate a plurality of times immediately using organic solvent and drying, then putting the negative electrode plate in acidic solution and dipping sufficiently, enabling a negative electrode membrane on the negative electrode plate to fall in the acidic solution; 3) taking out a current collector of the negative electrode plate, then carrying out solid-liquid separation upon the acidic solution in which the negative electrode membrane is dissolved, obtaining solid substance, washing the solid substance repeatedly using de-ionized water till the pH value of filtrate is 6-7, drying in vacuum condition, then grinding and sieving, obtaining graphite powders; and 4) making the lithium ion battery by using the graphite powders as negative electrode material, stewing for two hours and then measuring the specific capacity of the lithium ion battery. In comparison with the prior art, the detecting method has the advantages of low requirement on the environment and high accuracy.
Owner:DONGGUAN AMPEREX TECH

Method for preparing nanoscale Cu-based metal organic framework material

The invention discloses a method for preparing a nanoscale Cu-based metal organic framework material. The method includes the steps: (1) preparing a copper precursor solution A; (2) preparing an organic ligand solution B; (3) sending the solution A and the solution B into a micro channel reactor module I at a certain flow speed, generating a Cu-MOFs crystal seed in situ, and after the reaction is carried out for a certain time, sending the product material liquid into a module II; (4) when the product material liquid enters the module II, sending the solution B into the module II at a certain flow speed, carrying out crystal seed induced synthesis reaction, and after the reaction is carried out for a certain period of time, sending the product material liquid into a module III; (5) allowing the material liquid prepared in the step (4) to enter the micro channel reactor module III, and carrying out secondary crystallization reaction to synthesize a Cu-MOFs material; and (6) carrying out solid-liquid separation of the Cu-MOFs suspension prepared in the step (5), and allowing the filtrate to return to the micro channel reactor module II at a certain flow speed to participate in secondary crystallization reaction; and washing the solid with ethanol, and drying to obtain the product. The Cu-MOFs material is prepared by a multi-module micro channel reactor, and the method has the advantages of simple and fast preparation process, good product performance and the like.
Owner:CHINA PETROLEUM & CHEM CORP +1

Thallium-containing wastewater adsorption material and preparation method thereof

The invention provides a thallium-containing wastewater adsorption material and a preparation method thereof. The adsorption material comprises the following raw material components: chloromethyl polystyrene microspheres and thiourea. The chloromethyl polystyrene microspheres comprise the following raw materials: polystyrene microspheres, an organic solvent and tin tetrachloride. The preparation method comprises the following steps: 1, preparing polystyrene microspheres; step 2, preparing chloromethyl polystyrene microspheres; step 3: preparation of the adsorption material: adding the chloromethyl polystyrene microspheres and thiourea into absolute ethyl alcohol according to a mass ratio of 1:2, carrying out heating reflux for 2 hours to prepare an intermediate mixed solution, hydrolyzingthe intermediate mixed solution for 12 hours by using a 50% sodium hydroxide solution under the protection of nitrogen to prepare a mixed solution, and cooling the mixed solution, alternately cleaningthe mixed solution by using distilled water and a 2 mol/L hydrogen chloride aqueous solution, and drying the mixture to prepare the adsorption material. The adsorption material can be used for treating the concentration of thallium in wastewater to be less than 5 [mu] g/L and ensures that the thallium-containing wastewater reaches the industrial discharge standard.
Owner:湖南省环境保护科学研究院

Preparation method for high-activity metal organic framework material

The invention discloses a preparation method for a high-activity metal organic framework material. The method includes the steps: (1) preparing a metal precursor solution A; (2) preparing an organic ligand solution B; (3) sending the solution A and the solution B into a micro channel reactor module I, and generating an MOFs crystal seed in situ; (4) dissolving a metal in a state of metal powder, nano oxide or metal salt to obtain a solution C, when the material liquid obtained in the step (3) enters a module II, sending the solution C into the module II, and carrying out a metal ion in-situ synthesis reaction; (5) allowing the material liquid of the step (4) to enter a module III, sending the solution B into the module III, and carrying out crystal seed induced synthesis; (6) when the material liquid of the step (5) enters a module IV, sending a light reduction sacrificial agent D into the module IV; (7) when the material liquid obtained in the step (6) enters a module V, carrying out metal reduction reaction by sun illumination; and (8) carrying out solid-liquid separation, washing, and drying to obtain the product. The MOFs material prepared by the multi-module micro channel reactor has the advantages of simple and fast preparation process and good product activity.
Owner:CHINA PETROLEUM & CHEM CORP +1
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