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32results about How to "Broaden the absorption spectrum" patented technology

Modified carbon quantum dot loaded hollow tubular carbon nitride photocatalyst and preparation method thereof

The invention discloses a modified carbon quantum dot loaded hollow tubular carbon nitride photocatalyst and a preparation method thereof. The photocatalyst takes hollow tubular carbon nitride as a carrier and is loaded with modified carbon quantum dots; urea and melamine with a mole ratio of 1-5:1 are used to prepare the hollow tubular carbon nitride through hydrothermal and calcination. The preparation method comprises the following steps of: mixing hollow tubular carbon nitride, water and modified carbon quantum dot solution, and drying to obtain the photocatalyst. The photocatalyst has the advantages of large specific surface area, large number of pores, multiple active sites, high speed of separation and migration of photo-generated carriers, strong light absorption capacity, high photocatalytic activity, high stability, high photocatalytic efficiency and the like; the preparation method of the photocatalyst has the advantages of convenience in synthesis, simplicity in operation,no secondary pollution to the environment and the like. The photocatalyst can be widely used for treating organic pollutants in the environment and killing harmful microorganisms in the environment,and has good application value and application prospect.
Owner:HUNAN UNIV

Preparation method of single layer molybdenum disulfide and titanium dioxide nano heterojunction

The invention relates to a preparation method of a single layer molybdenum disulfide and titanium dioxide nano heterojunction. The method includes: firstly subjecting an Si/SiO2 substrate to ultrasonic cleaning, and then performing blow drying; putting a graphite boat loaded with molybdenum trioxide in a high temperature area of a chemical vapor deposition apparatus for heating, putting an Si/SiO2substrate on the graphite boat and conducting vacuum pumping; introducing a protective gas into a closed quartz tube, then performing evacuation, heating a tube furnace, raising the temperature to 700-800DEG C, conducting heat preservation for 5-20min, stopping heating, and performing cooling to room temperature to obtain flake single layer MoS2; dissolving tetrabutyl titanate in anhydrous ethanol, then adding acetyl acetone, and performing stirring at room temperature to titanium dioxide sol; immersing the flake single layer MoS2 in titanium dioxide sol, anhydrous ethanol and deionized waterin order, then using anhydrous ethanol for flushing to remove water attached to the surface, and then conducting annealing in a 500-550DEG C muffle furnace for 1-2h, thus obtaining the single layer MoS2/TiO2 nano heterojunction structure.
Owner:SHANGHAI INST OF TECH

Method for processing optical active layer of polymer solar cell and polymer solar cell manufacturing method

The invention discloses a method for processing an optical active layer of a polymer solar cell and a polymer solar cell manufacturing method. The polymer solar cell manufacturing method comprises the steps that with glass or flexible plastic serving as a substrate and a transparent conducting film serving as a front electrode, a soluble polythiophene and fullerene derivative blending system is established at indoor temperature in air to serve as the active layer, the volatilization rate of a solvent is regulated by regulating the relation among the indoor temperature, the alternative control spin-coating film formation rotating speed and the alternative control spin-coating film formation time, so that processing of the optical active layer is achieved under the condition that high-temperature heating is not needed, an optical active layer thin film obtained after processing is dried naturally in air, the polythiophene material P3HT is induced to achieve the self-assembly function, and the orderliness of the P3HT is improved. The method for processing the optical active layer of the polymer solar cell and the polymer solar cell manufacturing method have the advantages that the technology is simple, operation is easy, safety and stability are guaranteed, the cost is low, a protective gas atmosphere is not needed, heating annealing is not needed, manufacturing of the polymer solar cell can be completed in a controllable mode at room temperature, the polymer solar cell and the flexible substrate are compatible, and compared with a polymer solar cell manufactured through a conventional heating annealing and solvent annealing technology, the polymer solar cell manufactured through the method has better performance.
Owner:NINGBO UNIV

Biological detection chip, biosensor and preparation method thereof and application

The invention discloses a biological detection chip. The biological detection chip comprises a substrate, a metal array layer and a film adsorption layer which are stacked, wherein the metal array layer is positioned on the substrate and is provided with a spacing region for exposing the substrate; the film adsorption layer wraps the metal array layer and the surface of the substrate located in the spacing region, and the film adsorption layer is provided with a hydrophilic surface. Cells and organelles with biological film structures can be adsorbed by utilizing the hydrophilic surface of thefilm adsorption layer, target biomolecules are loaded on a biological film, the surface enhanced infrared absorption spectrum of the target biomolecules can be obtained, and detection and analysis ofthe target molecules are realized. The invention discloses a biosensor, which comprises the biological detection chip, is suitable for detecting film surface biomolecules with complex types, does notdestroy the molecular structure, and is suitable for research of various physiological and pathological processes, drug screening diagnosis and the like. The invention discloses a preparation methodof a biological detection chip, which is simple in preparation process and suitable for preparing the chip for detecting the biomolecules on the surfaces of various films.
Owner:SHENZHEN UNIV

Preparation method and application of silver/silver halide-loaded mesoporous titanium dioxide microsphere

The invention provides a preparation method of a silver / silver halide-loaded mesoporous titanium dioxide microsphere. The preparation method comprises the following steps: mixing a proper amount of tetrabutyl titanate and diethylene glycol, and carrying out stirring at 25 DEG C for 8 hours; dropwise adding a mixture obtained in the previous step into acetone and continuing stirring to obtain a white precipitate; heating the collected white precipitate at 550 DEG C for 8 hours to obtain anatase titanium dioxide microspheres; weighing a proper amount of the titanium dioxide microspheres, dispersing the titanium dioxide microspheres in 20 mL of pure water, carrying out stirring for 1 h, dropwise adding a proper amount of hexadecyl trimethyl ammonium halide, and continuing stirring for 1 h; adding a silver nitrate solution, and continuing stirring for 1-2 hours; after illuminating for 30 minutes, centrifugally collecting a precipitate, and cleaning the precipitate with pure water to obtaina sample; and drying the sample at 60 DEG C, and then heating the sample for 8 hours in a nitrogen atmosphere at 300 DEG C to obtain the silver / silver halide-loaded mesoporous titanium dioxide microsphere. The titanium dioxide microsphere prepared by the method can be used as an effective visible-light-induced photocatalyst for catalytically decomposing formaldehyde.
Owner:常州良福朗清生物科技有限公司

Modified carbon quantum dot supported hollow tubular carbon nitride photocatalyst and preparation method thereof

The invention discloses a modified carbon quantum dot loaded hollow tubular carbon nitride photocatalyst and a preparation method thereof. The photocatalyst takes hollow tubular carbon nitride as a carrier and is loaded with modified carbon quantum dots; urea and melamine with a mole ratio of 1-5:1 are used to prepare the hollow tubular carbon nitride through hydrothermal and calcination. The preparation method comprises the following steps of: mixing hollow tubular carbon nitride, water and modified carbon quantum dot solution, and drying to obtain the photocatalyst. The photocatalyst has the advantages of large specific surface area, large number of pores, multiple active sites, high speed of separation and migration of photo-generated carriers, strong light absorption capacity, high photocatalytic activity, high stability, high photocatalytic efficiency and the like; the preparation method of the photocatalyst has the advantages of convenience in synthesis, simplicity in operation,no secondary pollution to the environment and the like. The photocatalyst can be widely used for treating organic pollutants in the environment and killing harmful microorganisms in the environment,and has good application value and application prospect.
Owner:HUNAN UNIV

Titanium dioxide-based nano-composite photocatalyst for photocatalytic degradation under visible light irradiation and application of titanium dioxide-based nano-composite photocatalyst

The invention discloses a titanium dioxide-based nano-composite photocatalyst for photocatalytic degradation under visible light irradiation and application of the titanium dioxide-based nano-composite photocatalyst. The preparation method of the titanium dioxide-based nano-composite photocatalyst comprises the following steps: dissolving a titanium-containing precursor into a solvent to obtain a titanium-containing solution, then adding a silicon-containing compound and uniformly stirring, and finally adding rare earth salt and dissolving to obtain a mixed solution; and carrying out a hot-pressing reaction on the mixed solution under a closed condition, cooling to room temperature after the reaction is completed, carrying out suction filtration to obtain a solid, and drying the solid to obtain the titanium dioxide-based nano composite photocatalyst. The doping amount of the rare earth in the titanium dioxide-based nano composite photocatalyst accounts for 0.2-2.0 mol%, and the doping amount of the silicon accounts for 5.0-20 mol%. The rare earth, the silicon oxide and other components are doped into the nano titanium dioxide crystal, so that on one hand, the specific surface area of the composite photocatalyst is remarkably increased, and on the other hand, the light absorption spectrum of the photocatalyst is expanded to a visible light region, and the performance of removing VOCs (volatile organic compounds) such as formaldehyde is greatly improved.
Owner:UNIV OF JINAN
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