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Surface modified nano ferroferric oxide Fenton catalyst and preparation method thereof

The invention discloses a surface modified nano ferroferric oxide Fenton catalyst and a preparation method thereof. The preparation method of the surface modified nano ferroferric oxide Fenton catalyst comprises the following steps: firstly preparing high dispersibility nano ferroferric oxide by adopting a coprecipitation method, and then carrying out surface modification on the nano ferroferric oxide by adopting a hydrolysis method. Organic acid salt and a non-ionic surface active agent are added when the coprecipitation method is adopted for preparing ferroferric oxide particles, so that the quantity of inorganic matters deposited on the surfaces of the ferroferric oxide particles is low, enrichment of reaction substrate and charge transfer on the surfaces of the ferroferric oxide particles can be enhanced, good catalytic efficiency can be realized at room temperature in a larger pH range, and the surface modified nano ferroferric oxide Fenton catalyst can be used for advanced oxidation treatment of dye sewage, organic pollutant sewage, pesticide sewage and the like. Therefore, the preparation method of the surface modified nano ferroferric oxide Fenton catalyst has the characteristics of simplicity in operation, mild conditions, adaptability to large-scale preparation and the like, cost for obtaining the product is low, and the obtained product can be widely and more easily popularized.
Owner:SOUTHWEST UNIVERSITY FOR NATIONALITIES

Method of preparing traditional Chinese medicine preparation for treating melancholia and anxiety neurosis

InactiveCN101244208ASignificant insomniaSignificant depressionNervous disorderUnknown materialsAngelica Sinensis RootAdditive ingredient
The invention relates to a preparation method of Chinese herbal medicine preparation for treating depression and anxiety disorder, having the materials of roasted milkvetch root, Largehead Atractylodes Rhizome, Rhizoma Gastrodiae, medlar, Prepared Rehmannia Root, root of herbaceous peony, danshen root, angelica sinensis, Szechwan Lovage Rhizome, Epimedium Herb, semen zizyphi spinosae, polygalae, pachyma cocos, medicinal glue, American ginseng and Hairy Antler. The water volume of water decoction, extraction time and extraction times of the roasted milkvetch root, Largehead Atractylodes Rhizome, Rhizoma Gastrodiae, medlar, Prepared Rehmannia Root, root of herbaceous peony, danshen root, angelica sinensis, Szechwan Lovage Rhizome, Epimedium Herb, semen zizyphi spinosae, polygalae, pachyma cocos are preferred by adopting orthogonal test in the invention, which remain every component of medicinal materials having effect on the indications to the utmost extent; simultaneously the extraction of ineffective ingredient is reduced; the concentration is processed, and the active ingredient is not lost; the cost is lowered; the medicinal glue, American ginseng and Hairy Antler are ground, and the raw powder is used as medicines. The capsules prepared by the preparation method of Chinese herbal medicine preparation has the advantages of convenient administration, small administration dosage, easy discharge of the drug active ingredient, rapid absorption, increased bioavailability and fully exerted drug efficacy.
Owner:HOSPITAL NO 3 CPLA

Gradient preparation method of ultrahigh barley malt syrup

The invention belongs to the technical field of barley malt syrups, and particularly relates to a gradient preparation method of ultrahigh barley malt syrup. The method includes the steps: placing starch into ethanol water solution, performing ultrasonic stirring and hermetically pressurized reaction, and rapidly releasing pressure and then filtering mixture to obtain refined starch solution afterstanding and reacting; adding pullulanase and beta-amylase and pullulanase and maltase into citric acid-sodium citrate buffer solution to obtain first enzymolysis liquid and second enzymolysis liquid, adding the first enzymolysis liquid and the second enzymolysis liquid into a double-layer reaction kettle, slowly adding the refined starch solution, performing microwave reaction and stirring and heating reaction, mixing mixture after reaction, and performing standing and reacting to obtain enzymatic liquid; performing heating, enzyme deactivation and pressure reducing distillation on the enzymatic liquid, and filtering mixture by a micro-porous film to obtain the ultrahigh barley malt syrup. The method solves the problems that an existing process is high in production cost and easily pollutes environment, the method is simple and easy in process, good in stability and suitable for industrial production, and waste gas and waste water are omitted.
Owner:无锡甜丰食品有限公司

Cyclone overflow pulp classification system and pulp classification process

ActiveCN105214833AHigh recovery rateThe grading process is simple and reliableSolid separationRotary centrifugesCycloneSlag
The invention relates to a cyclone overflow pulp classification system and a pulp classification process. Pulp enters a first-grade cyclone for centrifugal separation; particles larger than 74 microns are discharged from a sand settling port of the first-grade cyclone; particles smaller than 74 microns are discharged from an overflow port of the first-grade cyclone; after the particles are cached by a buffer tank, the particles are fed from a first-grade slurry pump to a second-grade cyclone for centrifugal separation; particles larger than 37 microns are discharged from a sand settling port of the second-grade cyclone; particles smaller than 37 microns are discharged from an overflow port of the second-grade cyclone for removing large residues by a 0.5 mm slag separation sieve; after the pulp removed away the large residues enters a stirring tank for uniform stirring, the pulp is fed from a second-grade slurry pump to a 0.8 mm filter for impurity removal; the pulp, with impurities removed away, enters an inclined disc classifier for classification; settled sand of the classifier is discharged from a bottom flowing discharge port of the inclined disc classifier; and an overflow of the classifier is discharged from an overflow discharge port of the inclined disc classifier for entering a tailing. The classification system and process can improve the recovery rate of targeted ores to promote the economic benefit.
Owner:MYANDE GRP CO LTD

Surface-modified nanometer ferric oxide Fenton catalyst and preparation method thereof

The invention discloses a surface modified nano ferroferric oxide Fenton catalyst and a preparation method thereof. The preparation method of the surface modified nano ferroferric oxide Fenton catalyst comprises the following steps: firstly preparing high dispersibility nano ferroferric oxide by adopting a coprecipitation method, and then carrying out surface modification on the nano ferroferric oxide by adopting a hydrolysis method. Organic acid salt and a non-ionic surface active agent are added when the coprecipitation method is adopted for preparing ferroferric oxide particles, so that the quantity of inorganic matters deposited on the surfaces of the ferroferric oxide particles is low, enrichment of reaction substrate and charge transfer on the surfaces of the ferroferric oxide particles can be enhanced, good catalytic efficiency can be realized at room temperature in a larger pH range, and the surface modified nano ferroferric oxide Fenton catalyst can be used for advanced oxidation treatment of dye sewage, organic pollutant sewage, pesticide sewage and the like. Therefore, the preparation method of the surface modified nano ferroferric oxide Fenton catalyst has the characteristics of simplicity in operation, mild conditions, adaptability to large-scale preparation and the like, cost for obtaining the product is low, and the obtained product can be widely and more easily popularized.
Owner:SOUTHWEST UNIVERSITY FOR NATIONALITIES

Chlorogenic acid purifying and concentrating method

The invention relates to the field of purification of chlorogenic acid and discloses a chlorogenic acid purifying and concentrating method. The chlorogenic acid purifying and concentrating method comprises the following steps: (1) ultra-filtering a crude chlorogenic acid extract; (2) transferring an ultra-filtered thin solution to a fresh water tank, transferring an ultra-filtered concentrated solution to a percolation tank, adding water into the percolation tank to obtain a percolate; ultra-filtering the percolate again, transferring the ultra-filtered thin solution subjected to ultrafiltration again into the fresh water tank, and transferring the ultra-filtered concentrated solution subjected to ultrafiltration again to the percolation tank, and circulating in turn; and (3) conducting reverse osmosis treatment on the ultra-filtered thin solution, enabling a reverse osmosis thin solution to enter the fresh water tank again, and collecting a reverse osmosis concentrated solution. The method adopts the mode of combination of a tubular ultrafiltration membrane and a reverse osmosis membrane, the chlorogenic acid extract is purified and concentrated, on the basis of guaranteeing the purity of an obtained chlorogenic acid extract concentrated solution, the whole process is high in efficiency, the energy consumption is low, the cost is reduced, and no extra pollutants are produced in the whole process.
Owner:HANGZHOU RUINA MEMBRANE ENG
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