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47results about How to "Flexible process control" patented technology

Gradient-pore silicon nitride and silicon carbide combined film tube and preparation method therefor

The invention belongs to the field of porous ceramic materials and particularly relates to a gradient-pore silicon nitride and silicon carbide combined film tube and a preparation method therefor. The film tube material is prepared from silicon nitride and silicon carbide, and a gradient filtering structure is formed by a supporting body layer and a surface film layer; a supporting body is formed through combining silicon nitride produced from a reaction with coarse silicon carbide grains and has the average pore size of 10 to 80 microns, the surface film layer is formed through combining the silicon nitride produced from the reaction with fine silicon carbide grains and has the average pore size of 0.1 to 20 microns, and the overall porosity of the film tube is 35% to 50%. The preparation method sequentially comprises the steps of carrying out batching, forming the supporting body, preparing the film layer and carrying out firing, wherein the forming is carried out by adopting isostatic pressing, the forming pressure is controlled to 40MPa to 150MPa, the firing temperature is controlled to 1,400 DEG C to 1,650 DEG C, and the heat preserving time is 3 to 5 hours. The film tube can be used in an oxidative atmosphere, can also be used in a reducing atmosphere, is high in acid-alkali corrosion resistance and can be applied to the filtering and purifying of various high- and low-temperature fluids of coal gasification chemical industry, IGCC and PFBC coal-gasified power generation, high-temperature flue gas, automobile exhaust gas, water purification and the like.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Multi-channel pure silicon carbide film with asymmetric structure and preparation method for multi-channel pure silicon carbide film

The invention relates to the technical field of film separation materials and in particular relates to a multi-channel pure silicon carbide film with an asymmetric structure and a preparation method for the multi-channel pure silicon carbide film. The multi-channel pure silicon carbide film with the asymmetric structure consists of pure silicon carbide, is formed by sintering silicon carbide particles with the particle size of 0.1-100 microns and has a three-dimensional communicated gap structure; ducts form the asymmetric structure according to the sizes from small to large in the filtering direction; the aperture ratio of the film is 32-60 percent; the filtering characterization aperture range is ranged from 10-1,000nm; the film material has a tubular multi-channel structure and is formed by performing sintering for 2-4 times; a film base material is combined with a new silicon carbide in a sintering manner, which is formed by performing cracking reaction on a filtering layer serving as a silicon carbide precursor through an adhesive, and the sintering temperature is 700-1,400 DEG C. The obtained silicon carbide film has the characteristics of high filtering precision, high purity, high porosity, high intensity, large flux and long service life; the preparation method has the advantages of flexibility in control, low energy consumption, readily availability of raw materials, easiness in forming and suitability for industrial customization and can meet large-scale production.
Owner:浙江坚膜科技有限公司

Amino acid-containing condensate steam stripping system and tail gas treatment method

The invention discloses an amino acid-containing condensate steam stripping system and a tail gas treatment method for solving the problems of an existing steam stripping system that a treatment method is complex, system energy consumption is high, corrosion to pipe plates and pipelines is serious and equipment investment is high. The method comprises the steps of correspondingly feeding high temperature condensate, medium temperature condensate and low temperature condensate to a high temperature condensate stripping section, a medium temperature condensate stripping section and a low temperature condensate stripping section of a stripping tower, respectively, reducing the temperature of stripping gas at a stripping tower top to be 85-90 DEG C through an overhead condenser, and feeding into an incineration furnace, wherein the high temperature condensate stripping section is provided with a reboiler, low-pressure steam used as a heat source is used for carrying out steam stripping to the condensate, the medium temperature condensate stripping section and the low temperature condensate stripping section adopt high temperature flash gas generated by the high temperature condensate stripping section as the heat source, and low-pressure nitrogen gas is introduced for gas stripping. The process is simple, the operation can be controlled flexibly, the system stability is good, energy is saved, the consumption is reduced, the corrosion of the steam stripping system can be reduced to the maximum extent and the service life of the equipment can be prolonged.
Owner:湖北华庆石化设备有限公司

Biphase calcium phosphate (BCP) composite powder synthesized by high-temperature solid phase reaction and preparation method thereof

The invention discloses biphase calcium phosphate (BCP) composite powder synthesized by a high-temperature solid phase reaction. BCP powder is biphase composite powder prepared from hydroxyapatite (HA) and beta-tricalcium phosphate (beta-TCP), in which the molar ratio Ca/P of calcium to phosphorus is 1.5 to 1.67, wherein the value ranges of the relative mass percent of HA and beta-TCP two phases are each 1 to 99 percent; the sizes of crystalline grains of the HA and beta-TCP two phases are 20nm to 300 microns; the crystallinity is 50 to 100 percent. The invention also discloses a preparation method of the BCP composite powder synthesized by the high-temperature solid phase reaction. The BCP composite powder is prepared through the high-temperature solid phase reaction of a calcium-containing solid compound and a calcium-phosphorus solid containing compound. The BCP composite powder has the advantages that a reaction period is short; the costs of raw materials are low; the equipment investment is low; no waste gas and waste water are discharged; further, the proportion of the HA and beta-TCP two phase in the BCP powder is easily regulated and controlled at the same time; the two phases are distributed uniformly; the sizes of the crystal grains and the crystallinity are controllable; finally; the production requirement that the compression strength of BCP biphase composite ceramic is improved or a degradation speed is regulated and controlled is met.
Owner:SUZHOU DINGAN ELECTRONICS TECH

Pure foam silicon carbide support membrane tube with three-gradient pore structure and preparation method

Belonging to the field of porous ceramic materials, the invention in particular relates to a pure foam silicon carbide support membrane tube with a three-gradient pore structure and a preparation method thereof. According to the foam silicon carbide support membrane tube, a dual-gradient pore structure pure foam silicon carbide support and a surface film layer form a three-gradient filtration structure, the support is composed of a dual-gradient pore structure pure foam silicon carbide support, the average pore size of the outer layer is 300-500micrometers, the average pore size of the inner layer is 1-3mm, and the support porosity is 35-65%; the surface film layer is formed by combination of silicon carbide powder, the pore size is 50nm-20micrometers, and the film layer porosity is 35%-50%. The preparation method comprises the following steps in order: burdening, foam support molding, support sintering, film layer preparation and firing. The pure foam silicon carbide support membrane tube provided by the invention can be used in oxidizing atmosphere and reducing atmosphere, has strong acid and alkali corrosion resistance, and can be used for coal gasification chemical engineering and IGCC, PFBC coal gasification power generation, high temperature flue gas, automobile exhaust, water purification and other high and low temperature fluid filtration purification.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Pure silicon carbide filtering membrane

The invention belongs to the technical field of porous ceramic materials and their preparation and especially discloses a pure silicon carbide filtering membrane and a preparation method thereof. The pure silicon carbide filtering membrane has a high porosity, a low pressure drop, high strength, good thermal shock resistance and a high use temperature. The preparation method can be realized easily and can guarantee product performances. The pure silicon carbide filtering membrane comprises pure SiC, is a surface membrane layer obtained by pile-up and binding of fine SiC particles and has aperture sizes of 0.1 to 20 microns and membrane porosity of 25 to 50%. Fine SiC particles, silicon powder, a pore-forming additive and one or more organic resins as raw materials are prepared into a surface membrane layer by spraying or dipping and the surface membrane layer is dried and sintered to form the pure silicon carbide filtering membrane. The pure silicon carbide filtering membrane can be used in an oxidation atmosphere and in a reducing atmosphere, has strong acid corrosion and alkaline corrosion resistance, and can be used for various high / low temperature fluid filtering purification fields such as coal gasification chemical engineering, integrated gasification combined cycle (IGCC) and pressurized fluidized bed combustion (PFBC) coal gasification power generation, and high temperature flue gas, automobile exhaust and water purification.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Dual-gradient pore-structure sialon and silicon carbide combined membrane tube and preparation method thereof

The invention relates to the field of porous ceramic materials, and specifically relates to a dual-gradient pore-structure sialon and silicon carbide combined membrane tube and a preparation method thereof. The membrane tube material is composed of sialon and silicon carbide. The membrane tube has a dual-gradient filtering structure composed of a support body layer and a surface membrane layer. The support body layer is composed of a combination of sialon produced through a reaction and coarse silicon carbide grains, and has an average pore size of 10-50mum. The surface membrane layer is composed of a combination of sialon produced through a reaction and fine-particle silicon carbide grains, and has an average pore size of 0.1-5mum. An overall porosity of the membrane tube is within a range of 40-50%. The preparation method of the membrane tube sequentially comprises the steps of material preparation, support forming, membrane layer preparation and firing. Isostatic pressing is adopted in the forming step, wherein a forming pressure is controlled at 100-150MPa. The firing temperature is controlled at 1650-1850 DEG C, and a temperature maintaining time is 3-5h. The method is easy to realize. With the method, product performance can be ensured. The membrane tube provided by the invention has the advantages of high application temperature, high acid corrosion resistance and high alkali corrosion resistance. The membrane tube can be used in filtration purification of various fluids with high temperature or low temperature, such as high-temperature high-press gas filtration dedusting, water purification and the like.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Preparation method of porous silicon carbide ceramic support body

The invention discloses a preparation method of a porous silicon carbide ceramic support. The preparation method comprises the following steps: uniformly mixing mixed silicon carbide powder, silicon dioxide powder, a foaming agent, a dispersing agent and a thermosetting polymer emulsion used as main raw materials to obtain high-solid-content silicon carbide slurry, and then pouring, and carrying out pressureless sintering molding to obtain the porous silicon carbide ceramic support, wherein the mixed silicon carbide powder is formed by mixing large-particle-size silicon carbide powder and small-particle-size silicon carbide powder. The porous silicon carbide ceramic support body has the advantages of high strength, high temperature resistance, acid and alkali corrosion resistance and the like, ceramic matrixes of separation membrane materials with different specifications and different shape structures can be designed according to process requirements, and the porous silicon carbide ceramic support body can also be independently used as a separation filtering material of large-particle substances; and the related preparation method is simple, flexible in process control, relativelylow in cost and short in molding process period, and has important application and popularization values.
Owner:WUHAN INSTITUTE OF TECHNOLOGY

Method for preparing blast furnace blowing semicoke from low-rank coal based on high-pressure hydrothermal reaction

The invention relates to a treatment method for dehydrating and upgrading high-moisture and high-volatile low-rank coal, and discloses a method for preparing blast furnace blowing semicoke by upgrading low-rank coal based on a high-pressure hydrothermal reaction, wherein the method comprises four steps of low-rank coal pretreatment, high-pressure hydrothermal upgrading, waste heat recycling and upgraded semicoke dehydration and drying. According to the method, low-heat-value low-rank coal is converted into high-quality blast furnace blowing upgrading semicoke by utilizing a high-pressure hydrothermal reaction upgrading technology, wherein the moisture content of the semicoke air drying base is less than 6%, the volatile component content is less than 25%, the Hardgrove grind ability indexis greater than 60, the high-order heat generation value is greater than 24000 kJ/kg, soluble potassium salt, sodium salt and sulfate components in ash are dissolved out, the organic sulfur in coal iseffectively separated out, and the upgraded semicoke can meet the performance index requirements of coal for blast furnace blowing; and the method provided by the invention effectively solves the problems of high water content, high volatile component content, low heat value and high harmful element content of blast furnace blowing of low-rank coal, and provides a clean, efficient, low-energy-consumption and high-added-value low-rank coal upgrading utilization method.
Owner:UNIV OF SCI & TECH BEIJING

Pure SiC membrane tube support and preparation method thereof

The invention belongs to the technical field of porous ceramic materials and their preparation and especially discloses a pure SiC membrane tube support and a preparation method thereof. The pure SiC membrane tube support comprises pure SiC, is obtained by pile-up and binding of crude SiC particles having sizes of 5 to 400 microns, and has an uniform communicated aperture structure having an average aperture size of 5 to 120 microns and integral porosity of 25 to 50%. The preparation method comprises that crude SiC particles, crude silicon oxide particles or silicon powder as basic materials and one or more polymers as binders are mixed; the mixture is pressed into a support by a cold isostatic pressing sheath; and the support is sintered into the pure SiC membrane tube support. The pure SiC membrane tube support can be used in an oxidation atmosphere and in a reducing atmosphere, has strong acid corrosion and alkaline corrosion resistance, and can be used for various high / low temperature fluid filtering purification fields such as coal gasification chemical engineering, integrated gasification combined cycle (IGCC) and pressurized fluidized bed combustion (PFBC) coal gasification power generation, and high temperature flue gas, automobile exhaust and water purification.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Gradient-porosity pure silicon carbide membrane tube

The invention belongs to the technical field of multipore ceramic materials and preparation thereof, and particularly relates to a gradient-porosity pure silicon carbide membrane tube and a preparation method thereof. The gradient-porosity pure silicon carbide membrane tube consists of pure SiC; a gradient filter structure consists of a supporting body layer and a surface membrane layer, wherein the supporting body is formed by stacking and combining roughly granular SiC, and the average aperture is 5-120 mu m; the surface membrane layer is formed by stacking and combining finely granular SiC, and the aperture is 0.1-20 mu m; and the whole porosity of the membrane tube is 25-50%. The preparation method comprises burdening, forming the supporting body, preparing the membrane layer and sintering, wherein forming is performed under equal static pressure; the forming pressure is controlled between 40 and 150MPa; the sintering temperature is controlled between 1,500 and 2,400 DEG C; and heat is preserved for 0.5-5 hours. The method is easy to implement, and the performance of a product can be guaranteed. The gradient-porosity pure silicon carbide membrane tube can be used under an oxidization atmosphere and a reduction atmosphere, is high in acid and alkaline corrosion resistance and can be applied to gas chemical engineering and integrated gasification combined cycle (IGCC) and pressurized fluidized bed combustion (PFBC) power generation and used for filtering and purifying various types of high- and low- temperature fluid, such as high-temperature flue, automobile tail gas, water and the like.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Method and system for producing sandy aluminum oxide through three-section seed decomposition

The invention relates to a method for producing sandy aluminum oxide through three-section seed decomposition in a process of producing aluminum oxide with a Bayer process or in a Bayer process part of a combined process. The method for producing the sandy aluminum oxide through three-section seed decomposition comprises the steps of: mixing fine fluid with seeds; feeding into a first-section decomposition groove; discharging; performing first-stage cooling; feeding into a second-section decomposition groove; forming a necessary gravity fractionation layer in the decomposition groove by controlling proper stirring intensity; and drawing out coarse particles from the bottom of the groove and taking the coarse particles as aluminum hydroxide products; performing second-stage cooling on overflow containing fine particles at the upper part; feeding into a third-section decomposition groove; separating the underflow; performing seed filtering and washing processes; mixing the filtered seeds with the fine fluid; returning to the first-section decomposition groove; and performing an oxalate removing process on a seed washing solution after the seeds are washed. According to the method and system provided by the invention, by adoption of the three-section decomposition technology, the positions of the products to be output and the seeds are respectively arranged in the first-section and third-section decomposition grooves, so that the aims of obtaining high-quality aluminum hydroxide product, realizing high yield and flexible process control and facilitating the removal of oxalate are achieved.
Owner:中铝国际技术发展有限公司

Method for producing at least one air product, air separation system, method and device for producing electrical energy

The invention relates to a method for producing at least one air product, wherein an air separation system (100) is used which has a primary air compressor (10), a primary heat exchanger (20) and a distillation column system (30), and which comprises a first and a second operation mode, wherein, in the first operating mode, at least one liquid air product (LIN, LOX) produced in the distillation column system (30) is saved and, in the second operating mode, the at least one air product (LIN, LOX, LAIR) saved in the first operating mode and / or at least one additional liquid air product is supplied to the distillation column system (30). The method is characterized in that, in the second operating mode, at least one gaseous pressure flow (b - g) at a temperature level which lies below a hot-side temperature of the primary heat exchanger (20) is supplied to a cold compressor (45), compressed in the cold compressor (45) from a first above-atmospheric pressure level to a second above-atmospheric pressure level, and is supplied to at least one distillation column (31, 32) of the distillation column system (30) at the second above-atmospheric pressure level. The invention further relates to a corresponding air separation system (100) and to a method and to a device for producing electrical energy.
Owner:LINDE AG

System and method for producing fuel chemicals by conducting solar high-temperature thermal-coupling on methane

The invention provides a system and method for producing fuel chemicals by conducting solar high-temperature thermal-coupling on methane. The method includes the steps of introducing CO2-enriched gasinto a first high-temperature thermochemical reactor, carrying out a thermochemical decomposition reaction to produce a gas mixture of CO and CO2 and first oxygen under irradiation of first sunlight,and making the gas mixture of CO and CO2 sequentially pass a first temperature reducing device and a CO2 removal device to become CO-enriched gas; introducing water vapor into a second high-temperature thermochemical reactor, carrying out a thermochemical decomposition reaction to produce a gas mixture of water vapor and H2 and second oxygen under irradiation of second sunlight, and making the gasmixture of water vapor and H2 sequentially pass a second temperature reducing device and a dewatering device to become H2-enriched gas; after mixing methane-enriched gas with the first oxygen and thesecond oxygen, carrying out a reaction in a methane partial-oxidation reactor to produce synthesis gas; mixing the synthesis gas, the CO-enriched gas and the H2-enriched gas to be introduced into a fuel chemical synthesis tower for reacting to obtain the fuel chemicals.
Owner:SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI +1

A composite preparation process and equipment for semi-solid metal paste

The invention discloses a composite preparation process and composite preparation equipment for semisolid metal slurry. A weak electromagnetic stirring device and a mechanical stirring device are compounded together to prepare the semisolid metal slurry. Compared with an existing semisolid metal slurry preparation technique, the compound preparation process has the advantages that 1, compared witha rotary magnetic field electromagnetic stirring method, the electromagnetic field can be fully covered to avoid a skin effect and the needed energy consumption is low; 2, compared with a weak electromagnetic stirring method, the stirring force of alloy slurry is enhanced, the time needed to obtain the semisolid metal slurry is shortened, and the efficiency is improved; 3, compared with a mechanical stirring method, no mechanical stirrers are available, so that the defects that the stirrer is corroded and the alloy slurry is polluted are overcome, and meanwhile, the temperature of the slurryis controllable; 4, the composite preparation equipment is simple in structure, low in cost, flexible to control process and convenient to operate; and 5, the composite preparation process solves theproblem of low preparation efficiency of the semisolid slurry in large structural part production in production of large structural parts, the weights of which are over 5 Kg.
Owner:XI AN JIAOTONG UNIV

Amino acid-containing condensate steam stripping system and tail gas treatment method

The invention discloses an amino acid-containing condensate steam stripping system and a tail gas treatment method for solving the problems of an existing steam stripping system that a treatment method is complex, system energy consumption is high, corrosion to pipe plates and pipelines is serious and equipment investment is high. The method comprises the steps of correspondingly feeding high temperature condensate, medium temperature condensate and low temperature condensate to a high temperature condensate stripping section, a medium temperature condensate stripping section and a low temperature condensate stripping section of a stripping tower, respectively, reducing the temperature of stripping gas at a stripping tower top to be 85-90 DEG C through an overhead condenser, and feeding into an incineration furnace, wherein the high temperature condensate stripping section is provided with a reboiler, low-pressure steam used as a heat source is used for carrying out steam stripping to the condensate, the medium temperature condensate stripping section and the low temperature condensate stripping section adopt high temperature flash gas generated by the high temperature condensate stripping section as the heat source, and low-pressure nitrogen gas is introduced for gas stripping. The process is simple, the operation can be controlled flexibly, the system stability is good, energy is saved, the consumption is reduced, the corrosion of the steam stripping system can be reduced to the maximum extent and the service life of the equipment can be prolonged.
Owner:湖北华庆石化设备有限公司

A dual gradient pore structure Sialon bonded silicon carbide membrane tube and its preparation method

The invention relates to the field of porous ceramic materials, and specifically relates to a dual-gradient pore-structure sialon and silicon carbide combined membrane tube and a preparation method thereof. The membrane tube material is composed of sialon and silicon carbide. The membrane tube has a dual-gradient filtering structure composed of a support body layer and a surface membrane layer. The support body layer is composed of a combination of sialon produced through a reaction and coarse silicon carbide grains, and has an average pore size of 10-50mum. The surface membrane layer is composed of a combination of sialon produced through a reaction and fine-particle silicon carbide grains, and has an average pore size of 0.1-5mum. An overall porosity of the membrane tube is within a range of 40-50%. The preparation method of the membrane tube sequentially comprises the steps of material preparation, support forming, membrane layer preparation and firing. Isostatic pressing is adopted in the forming step, wherein a forming pressure is controlled at 100-150MPa. The firing temperature is controlled at 1650-1850 DEG C, and a temperature maintaining time is 3-5h. The method is easy to realize. With the method, product performance can be ensured. The membrane tube provided by the invention has the advantages of high application temperature, high acid corrosion resistance and high alkali corrosion resistance. The membrane tube can be used in filtration purification of various fluids with high temperature or low temperature, such as high-temperature high-press gas filtration dedusting, water purification and the like.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Method for realizing flexible process control of atomic layer deposition coating equipment

The invention relates to a method for realizing flexible process control of atomic layer deposition coating equipment. The flexible process control is realized by making a process file for controllinga film forming process of the atomic layer deposition coating equipment. The method comprises the following steps of: recording process information in a process text file mode, wherein the process information can be adjusted by modifying a self-defined text in the process text file; compiling the process text file through a compiler, and converting the process text file containing the process information into a rule file which accords with a program definition of a controller; and identifying and processing the rule file through the controller, and controlling the working state of the atomiclayer deposition coating equipment according to the rule file, so that the atomic layer deposition coating equipment executes the process information contained in the rule file. The method has the advantages that: a process worker directly modifies the process file without modifying a control program, so that error hidden dangers generated in the communication process are avoided, the design and test time of the control program is saved, and the process development efficiency is improved.
Owner:OPTORUN SHANGHAI CO LTD

Method for producing phosphoric acid by using (93-98)% concentrated sulfuric acid to extract phosphate rock and its equipment

The present invention proposes a method and equipment for extracting phosphate rock with 93%-98% concentrated sulfuric acid to produce phosphoric acid. Sulfuric acid and phosphate rock pulp are respectively added to two series-connected cylindrical reaction tanks of equal volume according to a certain ratio. The reaction tank is equipped with several sulfuric acid distributors and surface coolers, as well as a single central stirring paddle with large circulation. The cold air passes over the surface of the slurry thrown by the surface cooler and the sulfuric acid distributor, and the cold air is heated and humidified, thereby taking away the water vapor and removing the heat of reaction. The extraction reaction is carried out in two reaction tanks at the same time, and the operating conditions of the two tanks can be controlled separately, which is more conducive to the decomposition of phosphate rock and the coarse crystallization; the sulfuric acid is easy to disperse and more uniform under the sprinkler of the sulfuric acid distributor, and will not produce local A lot of SO 4 2- excess. The invention has strong adaptability to phosphate rock and can effectively improve the P 2 o 5 Improve the extraction rate, improve the crystallization of calcium sulfate dihydrate, and improve the filtration strength.
Owner:EAST CHINA ENG SCI & TECH
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