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96results about How to "Reduce intermediate steps" patented technology

Primary concentration and purification method for trioxymethylene after synthesizing

The invention discloses a new method for preliminary concentration and purification of paraformaldehyde after synthesis, which belongs to the technical field of concentration and purification of crude paraformaldehyde. The mixture is sent to the rectification tower for rectification; the top product obtained after rectification enters the condenser, and enters the absorption tower after cooling; the rectification tower still liquid returns to the paraformaldehyde synthesis reactor; after being absorbed by the absorption tower, the absorption tower The top gas and the bottom product enter the pre-concentration tower together for rectification treatment, and the solution obtained at the bottom of the pre-concentration tower is used as the reflux of the synthesis rectification tower and the absorption liquid of the absorption tower; The top product is sent to the concentration tower for concentration, and formaldehyde solution is obtained at the bottom of the concentration tower; the top product obtained from the concentration tower enters the light component removal tower, and the top of the light component removal tower obtains combustible waste liquid, and the bottom of the tower obtains 30-90% aqueous solution of paraformaldehyde. The invention has large output and low operation cost.
Owner:ZHEJIANG SANPO POLYMER

Safe soil on-site remediation integrated device

The invention discloses a safe soil on-site remediation integrated device. The invention belongs to the field of soil remediation. The device comprises a moving vehicle, a telescopic rod is arranged at the front end of the moving vehicle, a coulter is mounted at the bottom end of the telescopic rod, a rotating platform is arranged on the moving vehicle, a mechanical excavating arm is arranged on alifting column, an excavator bucket is mounted on the mechanical excavating arm, a treatment box is arranged on the moving vehicle, a partition plate is arranged in the treatment box, a water tank isarranged on the side wall of the treatment box, a water pipe is arranged on the water tank, a spraying disc is arranged at the outlet end of the water pipe, a sterilizing lamp is arranged on the inner wall of the treatment box, a strain adding pipe is arranged at the top end of the treatment box, an air injection tank is installed on the moving vehicle, a rotary drum is arranged in the treatmentbox, and multiple overturning plates are evenly arranged on the outer wall of the rotary drum. Office remediation is directly carried out on site, soil does not need to be dug out and transported, intermediate steps are saved, time and labor are saved, the soil remediation effect and efficiency are improved, harmful substances in soil are conveniently removed, soil remediation is facilitated, safety is improved, and use is convenient.
Owner:默晓辉

Biotin derivative of phenylephrine and preparation method and application thereof

The invention discloses a biotin derivative of phenylephrine and a preparation method and application thereof. The method includes: firstly, the synthetization of double-different-end polyethylene glycol; and secondly, the synthetization of piperazine derivative of phenylephrine; and thirdly, the synthetization of biotinylation of piperazine derivative of phenylephrine. The biotin derivative of phenylephrine and preparation method and application thereof discloses the application of the biotin derivative of phenylephrine as a fluorescence probe. The method firstly synthetizes the biotin derivative capable of being used to be connected with the biotin derivative of phenylephrine of alpha I adrenergic receptor agonist of streptavidin quantum dots, reserves the pharmaceutical activity part of the biotin derivative, and provides a tool for the future application of quantum dots in the research field of alpha I adrenergic receptor. Using PEG to connect alpha I adrenergic receptor agonist with biotin, the nonspecific adsorption of quantum dots and the steric hindrance generated after connected with the agonist are reduced. Because of continuous charging, the method is simple and effective, simple in operation, and good in purification effect. The structural formula is shown in the description, and n=25-60.
Owner:SHANDONG UNIV

Iron lithium fluoride battery anode material prepared by nitrogen-doped silicon carbide-assisted solid phase one-step process and preparation method

The invention discloses an iron lithium fluoride battery anode material prepared by a nitrogen-doped silicon carbide-assisted solid phase one-step process and a preparation method. The preparation method is characterized in that nitrogen-doped silicon carbide is adopted as a ball milling auxiliary, a conductive agent and a surface modifier at the same time in a preparation process; after the ball milling of a certain period of time and thermal treatment by a high-energy ball mill, the raw material is directly supplied to a battery production enterprise for coating production, thereby greatly reducing the intermediate steps, lowering the production cost and avoiding any waste liquid; the prepared FeF3 anode material has a stable capacity over 200mAh.g<-1> and a good multiplying power feature; iron salt containing crystal water and ammonium fluoride at a molar ratio of 1.0:(3.0-3.6), 3-15% of nitrogen-doped silicon carbide by weight and 0.5-3.0% of auxiliary by weight are subjected to normal-temperature ball milling for 5-20 hours under the atmosphere protection in the high-energy ball mill; then the material is taken out and heated to 300-450 DEG C under the protection of the mixed gas of 5% of hydrogen and 95% of argon, and the temperature is kept for 2-10 hours before cooling to obtain the FeF3 anode material which can be directly applied to slurry coating.
Owner:沛县度创科技发展有限公司

Powder coating mixing device

The invention belongs to the technical field of the coating processing, and particularly discloses a powder coating mixing device. The powder coating mixing device comprises a driving part and a mixing and stirring unit driven by the driving part. The powder coating mixing device further comprises a material leaking unit. The material leaking unit comprises a plurality of fixedly installed material leaking buckets. An upper surface and a bottom surface of each material leaking bucket are provided with openings. The bottom of the material leaking bucket is provided with a material leaking part.The material leaking part comprises a first material leaking plate installed on the bottom surface of the material leaking bucket. A second material leaking plate is installed below the first material leaking plate. The second material leaking plate is rotatably connected with the first material leaking plate. Each of the first material leaking plate and the second material leaking plate is provided with a first material leaking port. The first material leaking port on the first material leaking plate can be opened or closed by the second material leaking plate in a rotating process. The mixing device with the above structure is capable of solving a problem in the prior art that integration of coating feeding in proportion and coating mixing is not realized, thereby improving processing efficiency.
Owner:CHONGQING QICAIHONG CHEM

Hydrogenation catalyst and preparation method thereof and preparation method of tetrahydrofurfuryl alcohol

The invention relates to the field of tetrahydrofurfuryl alcohol production, in particular to a hydrogenation catalyst and its preparation method and a preparation method of tetrahydrofurfuryl alcohol. The hydrogenation catalyst contains a carrier and a ruthenium component loaded on the carrier. The preparation method of the hydrogenation catalyst comprises the following steps: 1) conducting coprecipitation on a mixed aqueous solution containing a titanium oxide precursor, a zinc oxide precursor and a zirconia precursor, and washing and drying the obtained precipitate, and successively molding, drying and roasting carrier powder obtained after drying so as to prepare the carrier; and 2) adding the carrier prepared in the Step 1) into a water solution of a ruthenium precursor, adding alkaline lye, controlling pH value to 6-9, stirring until a black solid is generated, and successively washing, drying and roasting the black solid. The hydrogenation catalyst of the invention has high activity and selectivity, is applicable to continuous preparation of furfuryl alcohol, and is still highly-efficient in reacting under the solvent-free condition. Thereby, separation of a solvent is avoided, production process is simplified, and costs are lowered.
Owner:CHINA PETROLEUM & CHEM CORP +1
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