The invention discloses a
porous carbon particle adsorption material capable of preparing ultra-pure
helium through one-step purification as well as a preparation method and application of the
porous carbon particle adsorption material. The method comprises the following steps: (1) carbonizing
biomass particles; (2) dipping the carbonized
biomass particles in a
nitrogen source-containing
aqueous solution; (3) carrying out CO2 activation pore-forming and
nitrogen functional group
doping on the
nitrogen source impregnated carbonized
biomass particles obtained in the step (2) at high temperature; and (4) fully activating the
nitrogen source impregnated carbonized biomass particles, performing programmed cooling, and introducing
water vapor to perform secondary pore forming and
oxygen functional group
doping to obtain the
porous carbon material. According to the method, the porous
carbon particle adsorbent is prepared from natural biomass, the pore size distribution is concentrated, nitrogen and
oxygen containing functional groups are rich, the adsorbent has ultrahigh adsorption and capture capacity on various impurities in the crude
helium under the low-temperature condition, the impurities in the crude
helium can be removed in one step, the helium is purified to reach the 6N standard, and the method is suitable for industrial production. And the application requirement of high-efficiency removal of impurities in the production process of ultra-pure helium is met.