The invention discloses a preparation method of a
titanium, aluminum,
niobium,
zirconium and
molybdenum alloy, and belongs to the technical field of preparation of
titanium alloys. The method comprises the following steps: weighing Ti, Al, Nb, Zr and Mo
metal powder according to certain proportions, mixing the
metal powder, performing intermittent dry type ball
grinding through a ball grinder to obtain mixed
powder, putting the obtained mixed powder into a
graphite mold, prepressing the mixed powder, placing the
graphite mold into a
discharge plasma sintering furnace, applying
axial pressure of 10 to 50 MPa for
sintering under the condition that the vacuum degree is 2 to 8 Pa, heating the mixed powder in a multi-stage heating mode to 1,000 to 1,150 DEG C, preserving the heat for 3 to 8 min, cooling the mixture to
room temperature, and demolding the mixture, thus obtaining the
titanium, aluminum,
niobium,
zirconium and
molybdenum alloy material. The titanium, aluminum,
niobium,
zirconium and
molybdenum alloy prepared by the method disclosed by the invention has the advantages of uniform component, high compactness,
high intensity, high
plasticity and the like; and in addition, the method is easy to operate, short in time, energy-saving and
environmentally friendly and has a good popularization value.