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46results about How to "Improve Primary Utilization" patented technology

Casting method for polycrystalline silicon ingot

The invention discloses a casting method for a polycrystalline silicon ingot. The casting method comprises a crucible pretreatment process and an ingot casting process, wherein the crucible pretreatment process comprises the steps of preparing silicon nitride slurry from silicon nitride powder, silica sol and water, spraying the silicon nitride slurry at the side wall and bottom of a crucible, and spraying other silicon nitride slurry at the bottom of the crucible; and soaking silicon powder in an acid solution with strong oxidizing property for 30-60 minutes, then, separating, washing to be neutral, drying the washed silicon powder, next, preparing slurry from the dried silicon powder, the silica sol and the water, spraying the slurry at the bottom of the obtained crucible, and sintering the treated crucible; and the melting stage of the ingot casting process comprises the step of immediately opening a cage to cool when a silicon material floats from the bottom of the crucible. The polycrystalline silicon ingot produced by using the casting method disclosed by the invention has the characteristics of short production period, low cost, long silicon ingot minority carrier lifetime, high primary silicon material utilization ratio and the like, and the obtained polycrystalline silicon wafer has the characteristics of uniform grain size, small defect density, high photoelectric conversion efficiency and the like.
Owner:YANGZHOU RONGDE NEW ENERGY TECH

Preparation method of black-edge-free high-efficiency polycrystalline silicon ingot

The invention discloses a preparation method of a black-edge-free high-efficiency polycrystalline silicon ingot, which comprises the following steps: applying a high-purity quartz sand slurry on the inner side surface of an increased quartz crucible for polycrystalline cast ingots to form a high-purity coating; applying a high-purity fine sand slurry to form a fine sand coating, and carrying out high-temperature quick sintering for 1 hour; spraying a silicon nitride slurry on four walls in the crucible with the two high-purity coatings to form a high-purity silicon nitride coating as a mold release agent; laying a fine silicon material layer on the bottom of the crucible with the silicon nitride coating as a seed crystal layer, and putting a primary silicon material on the seed crystal layer; and opening the heat insulation cage to the height of 5-6cm in the melting stage, testing the residual height of the silicon material with a quartz rod, quickly cooling when the residual height is 5-6mm, entering the crystal growth stage, and controlling the temperature gradient in the crucible to form vertical temperature gradient in the crucible from bottom to top so as to induce the growth of the molten silicon material by utilizing the seed crystal layer laid on the bottom, thereby obtaining the black-edge-free high-efficiency polycrystalline silicon ingot.
Owner:江苏美科太阳能科技股份有限公司

Method for treating wastewater of rubber vulcanization accelerator N-cyclohexyl-2-benzothiazole sulfonamide

The invention belongs to a method for treating wastewater of a rubber vulcanization accelerator N-cyclohexyl-2-benzothiazole sulfonamide (CZ). The method comprises: returning 30%-40% of generated wastewater into a CZ synthesis reaction vessel for indiscriminate application, subjecting the rest part to vacuum distillation, recovering cyclohexylamine; precipitating organic components dissolved in cyclohexylamine, filtering the recovered mother liquid, and putting the precipitated organic matter into the synthesis reaction vessel for continuous reaction, and leading the filtrate to multiple-effect evaporation so as to obtain a sodium chloride saturated solution, conducting concentration so as to obtain a supersaturated solution of sodium chloride, and carrying out centrifugation, thus obtaining sodium chloride; returning part of the evaporated water to the device for reuse, and leaving the left part to biochemical treatment. In order to make the raw material M completely reacted during production, excess cyclohexylamine is added, so that a great amount of cyclohexylamine is contained in the wastewater. By adopting a mother liquid indiscriminate application technology, the mother liquid can be recycled, the primary utilization rate of cyclohexylamine can be enhanced, simultaneously the mother liquid treatment cost can be reduced, and the CZ yield can be improved. After mother liquid indiscriminate application, the CZ product has no abnormal change in appearance, and no obvious change in melting point as well as ash content.
Owner:KEMAI CHEM

Efficient continuous crackless flattening method of bamboo

The invention discloses an efficient continuous crackless flattening method of bamboo. The method includes following process steps: (1), pre-treating fresh bamboo tubes; (2), enabling the bamboo tubes to enter a heating pipeline for heating treatment; (3), flattening the bamboo tubes in a heat-insulating space connected with the heating pipeline; (4), post-treating flattened bamboo chips. The method has the advantages that when the fresh bamboo tubes are placed in a high-temperature separated pipeline with temperature of 130-160 DEG C, quick heating and heat-moisture treatment of high-temperature overheated steam are utilized to enable temperature of the bamboo tubes to reach softening points of lignin, cellulose and hemicellulose, and in a subsequent section of the heat-insulating space for high-temperature heating, multiple bamboo tubes or bamboo chips with certain radian are sequentially flattened, cooled and set through flattening rollers which widens progressively. By using the method, treatment temperature for bamboo flattening and labor intensity of workers during operation are lowered, harsh environment for the workers during operation is improved, and production automation level is high; finished products do not need de-yellowing treatment, flattened bamboo is better in physical and mechanical performance, attractive in color and luster and suitable for being used for making artware and furniture and home decoration.
Owner:NANJING FORESTRY UNIV

Joint preparation method of potassium chloroplatinite and potassium chloroplatinate

The invention relates to a joint preparation method of potassium chloroplatinite and potassium chloroplatinate. The joint preparation method comprises the steps of: completely dissolving metal platinum which is taken as a raw material by aqua regia, and adding hydrochloric acid to remove nitrogen compound to obtain chloroplatinic acid solution; neutralizing the chloroplatinic acid solution by using potassium hydroxide solution until the pH value is 5.5-7.5; adding potassium oxalate for reducing to obtain the potassium chloroplatinite; and separating out crystal, and adding hydrogen peroxide into the rest mother liquor to obtain the potassium chloroplatinate. The joint preparation method can be used for preparing two products by charging for once, is simple in technology and short in process flow, does not generate platinum-containing mother liquor, and is high in platinum utilization rate and good in product quality. The potassium chloroplatinite and the potassium chloroplatinate prepared by the invention are mainly used for manufacturing catalysts, chemically analyzing, preparing platinum-containing complexes and platinum-containing metallorganic compounds and the like, and are widely applied to industries such as military industry, electronic industry, medical industry, etc.
Owner:天津市风船化学试剂科技有限公司

High-temperature tunnel kiln type flattening method for bamboo tubes

The invention relates to a high-temperature tunnel kiln type flattening method for bamboo tubes. The method comprises the following process steps of: (1) pre-treating fresh bamboo tubes; (2) stacking the bamboo tubes; (3) flattening the round bamboo tubes in a tunnel kiln; and (4) performing post-treatment on the flattened bamboo chips. The method provided by the invention has the advantages that in a high-temperature divided tunnel kiln at the temperature of 130-160 DEG C, the temperature of the bamboo tubes reaches the softening points of lignin, cellulose and hemicellulose by means of quick heating and heat-moisture treatment of high-temperature superheated steam on fresh round bamboo tubes. Under such a circumstance, under the pressure of a top-mounted oil cylinder in a bamboo tube flattening room, the round bamboo tubes with saw joints are flattened, so that the bamboo flattening treatment temperature as well as the labor intensity and severe environment during operation of workers is reduced. The manufactured flattened bamboos are more excellent in physical and mechanical properties and the like, are attractive in color and luster and are suitable for manufacture of artware and furniture and home decoration. The method provides a more excellent processing method for bamboo industry.
Owner:NANJING FORESTRY UNIV

Polycrystalline silicon production process and production system used for same

The invention relates to a polycrystalline silicon production process and a production system used for the same. The polycrystalline silicon production process comprises the following steps of: mixing fine trichlorosilane with the concentration of more than 99.99% and hydrogen in the mol ratio of the hydrogen to the fine trichlorosilane of (4-3):1 to be used as a mixed gas feeding material; introducing the mixed gas feeding material into a CVD (Chemical Vapor Deposition) reduction furnace, wherein the mixed gas feeding material sequentially passes through a bubble type gasifying device, a heat exchanger of an inlet / outlet device, and a main furnace of the CVD reduction furnace and an auxiliary furnace of the CVD reduction furnace which are connected in series; carrying out heat exchange on the final exhaust tail gas exhausted by the auxiliary furnace of the CVD reduction furnace and introducing the gas into the main furnace of the CVD reduction furnace to carry out reaction on the surface of a silicon core in the main furnace of the CVD reduction furnace to generate polycrystalline silicon, wherein a byproduct is middle tail gas; mixing the middle tail gas with the supplemented fine trichlorosilane gas and introducing the mixed gas into the auxiliary furnace of the CVD reduction furnace to react on the surface of the silicon core in the auxiliary furnace of the CVD reduction furnace to generate the polycrystalline silicon, wherein the byproduct is the final exhaust tail gas; and carrying out the heat exchange on the final exhaust tail gas which is discharged out of the furnace, and the mixed gas feeding material, and introducing into a reduction tail gas recycling system. The process and the production system disclosed by the invention can be used for manufacturing the high-quality electronic-grade polycrystalline silicon in a high-efficiency and low-cost manner.
Owner:巴彦淖尔聚光硅业有限公司

Automatic weighing and assembling method for cold-pressed recombination bamboo

The invention provides an automatic weighing and assembling method for cold-pressed recombination bamboo. The method includes the following technological steps that (1) impregnated bamboo split drying and separation are performed; (2) bamboo split aligned weighing and bundling are performed; (3) bamboo split bundles are automatically stacked; and (4) water content balancing and pavement of the bamboo split bundles are performed. The automatic weighing and assembling method for the cold-pressed recombination bamboo has the advantages that bamboo splits are subjected to on-line weighing and bundled on an existing impregnated bamboo split drying and separation line, the bundled bamboo splits are automatically stacked through rollers and a lifting device, the water content is balanced, and then two or four bamboo split bundles are delivered into an assembling trough. Existing cold-pressed recombination bamboo production technologies are improved through the method, the production procedures are optimized, the cold-pressed recombination bamboo pavement uniformity is improved, the labor intensity of workers is relieved, the production efficiency and quality are improved, and sound development of the cold-pressed bamboo and the recombination bamboo is guaranteed.
Owner:NANJING FORESTRY UNIV

Parallel small diameter heat pipe enhanced heat exchange device for recovering medium and low temperature flue gas waste heat and preparation method thereof

The invention relates to a parallel small diameter heat pipe enhanced heat exchange device for recovering medium and low temperature flue gas waste heat, aims to solve the problem of waste of medium and low temperature flue gas waste heat generated in small combustion equipment primarily, recovers the flue gas waste heat by means of parallel small diameter heat pipes to produce hot water or heat other substances, and is suitable for recovering waste heat of small flow flue gas or a discontinuous small flow heat source. The parallel small diameter heat pipe enhanced heat exchange device is primarily characterized in that the parallel small diameter heat pipe enhanced heat exchange device is good in heat transfer property, compact in structure, small in size, easy to process and low in cost,and can achieve self transfer of heat and efficient recovery of waste heat, so that the exhaust gas temperature is reduced greatly and the integral efficiency of the system is improved. The device isquite suitable for heat recovery of small capacity medium and low temperature flue gas waste heat and discontinuous waste heat resources, and a heating container is taken conveniently.
Owner:NANJING UNIV OF TECH +1

Continuous production system and production method for bamboo flattened plates

The invention discloses a continuous production system and production method for bamboo flattened plates. The continuous production system is characterized by being electrically connected with a control system and comprising a bamboo softening device for carrying out high-temperature and high-humidity softening treatment on bamboo chips, a bamboo pretreatment device, a planing and flattening all-in-one machine and a bamboo post-processing device, wherein the bamboo pretreatment device and the planing and flattening all-in-one machine are arranged at the feeding end and the discharging end of the bamboo softening device respectively, and the bamboo post-processing device is arranged at the discharging end of the planing and flattening all-in-one machine; and an automatic delivery device andan automatic conveying mechanism which are used for continuously and automatically conveying bamboo chips are arranged between the planing and flattening all-in-one machine and the bamboo softening device and between the planing and flattening all-in-one machine and the bamboo post-processing device respectively, and an automatic feeding device used for continuously and automatically feeding thebamboo chips is further arranged between the bamboo pre-processing device and the bamboo softening device. According to the continuous production system, intelligent control is achieved through the control system, the bamboo softening and flattening effect is good, the bamboo utilization rate is high, the yield of the bamboo flattened plates is remarkably increased, the manufacturing cost is low,continuous and efficient production of large-batch bamboo flattened plates can be achieved, the practicability is good, and the wide industrial application prospect is achieved.
Owner:ZHEJIANG FORESTRY UNIVERSITY

Smelting method of corrosion-resistant soft magnetic alloy material

The invention discloses a smelting method of a corrosion-resistant soft magnetic alloy material, and can solve the problems of low yield and low production efficiency of the produced corrosion-resistant soft magnetic alloy material and the like and also can improve the comprehensive performance of the material. The invention adopts the main scheme that a cast ingot for smelting an intermediate-frequency furnace or a vacuum induction furnace or other equipment is subjected to electroslag re-melting to obtain a high-quality heat processing blank. A formula for slag subjected to electroslag re-melting is calcium fluoride: calcium oxide: aluminum oxide=(65-80):(1-5):(15-25); and the filling ratio of 0.5-0.6 is adopted during re-melting. The smelting method has the following advantages that: the segregation is reduced, the organization is fined, the contents of P and S elements are reduced, the contents of inclusions are reduced, and the distribution of the inclusions is improved, so that the forming performance (the yield is improved by about 5-10 percent) and the use performance of materials are improved; and the produced blank has good surface quality and needs not to be peeled off, so that the material one-time utilization ratio (about 5-10 percent) and the production efficiency (about 5-10 percent) can be improved.
Owner:CHONGQING UNIVERSITY OF SCIENCE AND TECHNOLOGY

Joint preparation method of potassium chloroplatinite and potassium chloroplatinate

The invention relates to a joint preparation method of potassium chloroplatinite and potassium chloroplatinate. The joint preparation method comprises the steps of: completely dissolving metal platinum which is taken as a raw material by aqua regia, and adding hydrochloric acid to remove nitrogen compound to obtain chloroplatinic acid solution; neutralizing the chloroplatinic acid solution by using potassium hydroxide solution until the pH value is 5.5-7.5; adding potassium oxalate for reducing to obtain the potassium chloroplatinite; and separating out crystal, and adding hydrogen peroxide into the rest mother liquor to obtain the potassium chloroplatinate. The joint preparation method can be used for preparing two products by charging for once, is simple in technology and short in process flow, does not generate platinum-containing mother liquor, and is high in platinum utilization rate and good in product quality. The potassium chloroplatinite and the potassium chloroplatinate prepared by the invention are mainly used for manufacturing catalysts, chemically analyzing, preparing platinum-containing complexes and platinum-containing metallorganic compounds and the like, and are widely applied to industries such as military industry, electronic industry, medical industry, etc.
Owner:天津市风船化学试剂科技有限公司

Preparation method of nitrided iron nano-powder and high-pressure gas-solid reaction bed thereof

The invention discloses a preparation method of nitrided iron nano-powder and a high-pressure gas-solid reaction bed of the nitrided iron nano-powder and effectively prepares the nitrided iron nano-powder in an energy-saving mode. The preparation method of the nitrided iron nano-powder comprises the following steps: ferric salt and alkali precipitator are quickly mixed in a reactor, and ferric hydroxide powder is obtained after the reaction; the ferric hydroxide powder is put into the high-pressure gas-solid reaction bed, and ammonia and gas storage tank gas are ventilated to conduct the reaction; under a sealing condition, reaction resultant is discharged into a material storage tank, and finally the required the crystal type nitrided iron nano-powder is obtained. The high-pressure gas-solid reaction bed of the nitrided iron nano-powder comprises a gas sparger, a powder supporting net, a heater, a quick connector, a material storage tank valve, a material storage tank, a heating power source, a thermocouple, a gas inlet valve, a gas inlet, a gas outlet valve, a gas outlet, a reaction bed side wall and a ventilation valve. The preparation method of the nitrided iron nano-powder and the high-pressure gas-solid reaction bed of the nitrided iron nano-powder are simple in operation and energy-saving, the rection equipment can be connected in parallel, and the batch production amount is big.
Owner:UNIV OF SCI & TECH LIAONING

Micro-vacuum automatic balance filling machine and filling method

ActiveCN104528615BMeet filling requirementsConducive to large-scale improvementFilling using counterpressureBuffer tankEngineering
The invention discloses a micro-vacuum automatically-balanced filling machine and a filling method. A vacuumizing system is arranged on the filling machine; a plurality of vacuumizing silicone tubes are distributed on the side wall of a material cylinder of the filling machine, two ends of each vacuumizing silicone tube are respectively located on the inner and outer sides of the material cylinder, and the end parts, located on the inner side of the material cylinder, of the vacuumizing silicone tubes are connected with a central vacuumizing pipe of a filling valve; vacuumizing suction disc assemblies are respectively arranged at a bottle feeding workstation and a bottle discharging workstation on the material cylinder, the end parts, located on the outer side of the material cylinder, of the vacuumizing silicone tubes are communicated with the vacuumizing suction disc assemblies, and each vacuumizing suction disc assembly is connected with a negative pressure buffer tank and a vacuum pump through a vacuum tube. The filling method comprises the following steps that the whole vacuumizing system is in a negative pressure state; when the filling machine rotates, packaging bottles on the bottle feeding workstation are vacuumed by virtue of the vacuumizing system after packaging bottles are fed to the bottle feeding workstation, and then opening the filling valve is opened, and sauce is filled; after the packaging bottles are fed in and discharged out of the bottle discharging workstation, the filling valve is closed, and then residual sauce at bottlenecks of the packaging bottles is extracted by virtue of the vacuumizing system.
Owner:LEE KUM KEE XIN HUI FOOD

A polysilicon production process and a production system for the process

The invention relates to a polysilicon production process and a production system used in the process. It includes mixing refined trichlorosilane with a concentration of more than 99.99% and hydrogen at a hydrogen:refined trichlorosilane molar ratio of 4 to 3:1 as a mixed gas feed into the CVD reduction furnace, and the mixed gas feed passes through the Bubble carburetor, heat exchanger for inlet and outlet, CVD reduction furnace main furnace and CVD reduction furnace auxiliary furnace connected in series; the final tail gas discharged from the CVD reduction furnace auxiliary furnace enters the CVD reduction furnace main furnace after heat exchange, and then enters the CVD reduction furnace main furnace. The surface of the silicon core in the furnace reacts to form polysilicon, and its by-product is intermediate tail gas; the intermediate tail gas is mixed with supplementary refined trichlorosilane gas and then enters the auxiliary furnace of the CVD reduction furnace, where the silicon core surface in the auxiliary furnace of the CVD reduction furnace generates The reaction produces polysilicon, and its by-product is the final tail gas; after the final tail gas comes out of the furnace, it exchanges heat with the mixed gas feed and then enters the reduction tail gas recovery system. The process and production system can produce high-quality electronic-grade polysilicon with high efficiency and low cost.
Owner:巴彦淖尔聚光硅业有限公司

Compound fertilizer generation system

The invention discloses a compound fertilizer generation system, and solves the problems of uneven particle, high moisture content, more returning charge and the like in the production and granulationprocesses of the existing compound fertilizer. In the technical scheme, the compound fertilizer generation system comprises a pretreatment system, a granulation system, a posttreatment system and a charge and returning charge system which are sequentially connected, the granulation system comprises a roller provided with a drive device, a discharge structure is connected to the rear end of the roller, a charge tube, an acid mixing tube, a tubular reactor and an ammonia spraying tube bundle are sequentially arranged at the front section of the roller from top to bottom, the acid mixing tube, the tubular reactor and the ammonia spraying tube bundle are respectively provided with a sprayer; the charge tube is connected with the charge and returning charge system, the tubular reactor is connected with an ammonia station, the pretreatment system and a sulfuric acid storage tank respectively; the acid mixing tube is connected with a tail gas treatment system and the sulfuric acid storage tank respectively; and the ammonia spraying tube bundle is connected with the ammonia station. The system is simple, saves energy and reduces consumption, the product strength is high, the returning rate is low, the production efficiency is high, the water solubility is good, and the compound fertilizer generation system is environmentally friendly.
Owner:HUBEI UNIV OF TECH
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