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43results about How to "Simple control conditions" patented technology

Process method for preparing synthesis gas by using zero carbon or negative carbon emission system

The present invention discloses a process method for preparing synthesis gas by using a zero carbon or negative carbon emission system. The process method comprises that: 1) first raw material gas is subjected to desulfurization, steam is matched, pressurization and heating are performed, a reaction is performed to obtain first conversion gas, the first conversion gas is output, the output first conversion gas and pure oxygen are mixed and then enter a two-stage furnace to react so as to obtain second conversion gas, and the second conversion gas is output from the two-stage furnace; 2) second raw material gas is subjected to desulfurization, pressurization and heating and then is mixed with pure oxygen and carbon dioxide, then a reforming reaction is performed to obtain third conversion gas, and the third conversion gas is output from the reforming reactor; and 3) the second conversion gas is subjected to heat recovery and then is mixed with the third conversion gas to form crude synthesis gas, wherein the crude synthesis gas is adopted as the subsequent synthesis gas with or without a decarbonization device. According to the present invention, the greenhouse gas emission is reduced, the carbon efficiency is improved, the recycling of the carbon resources of the energy source chemicals is achieved, the hydrogen-carbon ratio of the synthesis gas achieves the ideal ratio of the downstream process requirement, and the zero carbon or negative carbon emission of the whole system is achieved.
Owner:SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI +1

Device and method for producing biogas by distillers' grain fermentation

The invention discloses a device and a method for producing biogas by distillers' grain fermentation. The device comprises a mixing tank, a circulating pump, a reaction tank and a return pipe, wherein the mixing tank, the circulating pump and the reaction tank are sequentially connected through a pipeline, and the reaction tank is connected with the mixing tank through the return pipe. The reaction tank is provided with a water distributor, a first reaction chamber, a primary three-phase separator, a second reaction chamber, a secondary three-phase separator, a flow guide pipe, a drain port and an exhaust port, and the mixing tank is provided with a heating device, an emptying port, a stirrer and a feed port. The method for producing the biogas by distillers' grain fermentation includes the steps: 1) preliminarily fermenting distillers' grain wastewater in the mixing tank; 2) performing two-stage anaerobic fermentation treatment for the distillers' grain wastewater in the reaction tank. The device is stable in running, easy to control, less in discharged sludge quantity and capable of generating the biogas with the methane content of 60% or more. The device and the method are applicable to treating high-concentration distillers' grain wastewater, less in sludge loss, good in organic matter removing effect and low in running cost.
Owner:广州市金龙峰环保设备工程股份有限公司

Aluminum nitride ceramic plate metalization method

The invention relates to an aluminum nitride ceramic plate metalization method, which comprises the following steps of cleaning the surface of an aluminum nitride ceramic plate; forming a titanium conduction layer with the set thickness on the surface of the aluminum nitride ceramic plate; using the aluminum nitride ceramic plate subjected to titanium plating on the surface as a cathode; putting the aluminum nitride ceramic plate into an electrolytic bath; using refined copper as an anode; putting the aluminum nitride ceramic plate into a heat treatment furnace; then, performing heating and temperature rise; seeping the titanium conducting layer to the aluminum nitride to form a TiN metallurgical transition layer and simple substance aluminum; continuously performing heating and temperature rise; sending ultrasonic waves to the aluminum nitride ceramic plate through a ultrasonic wave generating device, so that the liquid-state simple substance aluminum vibrates and flows out; stabilizing the TiN metallurgical transition layer; performing further heating and temperature rise; seeping the titanium conducting layer to the copper plating layer to form a TiCu metallurgical transition layer. Compared with the prior art, the method provided by the invention has the advantages that the liquid-state simple substance aluminum in the TiN metallurgical transition layer vibrates, so that the liquid-state simple substance aluminum melts and is discharged out of the aluminum nitride ceramic plate; the connection intensity of the copper plating layer and the titanium conducting layer is improved; the product quality and the finished product rate are improved.
Owner:FUJIAN HUAQING ELECTRONICS MATERIAL TECH

Method for treating eutrophication substances in sewage through artemia culture and water purifying system

The invention provides a method for treating eutrophication substances in sewage through artemia culture. The method includes the following steps that S1, a treating pond is built, and salt lake brine is injected into the treating pond; S2, to-be-treated sewage is injected into the treating pond in a continuous or semi-continuous mode, and the net evaporation speed of a water body in the treating pond and the injection speed of the to-be-treated sewage are kept same; S3, the salinity of the water body in the treating pond is adjusted and kept 6 baume to 14 baume, nutrient substances in sewage are used, microalgae, microorganisms and the like are cultured to serve as baits of artemia, artemia in the water body in the treating pond is cultured, and nitrogen and phosphorus eutrophication substances are removed in sewage from water by catching artemia. By means of the method, it is achieved that the eutrophication substances in sewage are efficiently and continuously purified, zero discharging of the eutrophication substances is achieved, artemia produced in the water purifying process is high-quality baits for culturing animals and raw materials in cooperation with feed, and objective economic benefits can be created.
Owner:天津津枫丰年虫科技有限公司

Method for comprehensively recycling sodium, aluminum and iron from red mud

The invention discloses a method for comprehensively recycling sodium, aluminum and iron from red mud. The red mud is mixed with an additive to obtain a raw material, the mixed raw material is subjected to calcination to obtain clinker, the clinker is added to an alkaline adjustment liquid for leaching, slid-liquid separation is performed, and leachate containing aluminum and sodium and magnetic leaching residues are obtained; the additive is a mixed additive composed of a calcium-series additive, a magnesium-series additive and a sodium-series additive. According to the technical scheme, no reducing agent needs to be added, hematite or hematite is converted as magnesioferrite with high magnetism through the magnesium-series additive and enters the leaching residues, and then an iron ore concentrate product is obtained through magnetic separating. In the technical scheme, the atmosphere control process and generation of a great quantity of polluting atmosphere in the current iron recycling process are avoided. In the method, the aluminum recycling rate is 85%, the sodium recycling rate is 92% or above, the sodium content in final residues is lowered to 1% or below, the iron grade of the iron ore concentrate is 50-55%, and the recycling rate is about 70%.
Owner:CENT SOUTH UNIV

Industrial storage and reutilization method of anaerobic ammonia oxidizing bacteria

The invention provides an industrial storage and reutilization method of anaerobic ammonia oxidizing bacteria and belongs to the field of biological treatment of wastewater. The method comprises the following three steps of selecting the anaerobic ammonia oxidizing bacteria, storing and recovering activity: step 1, taking out active sludge from different parts of an anaerobic ammonia oxidizing reactor which is operated normally, and uniformly mixing; introducing high-purity argon gas; selecting the suitable anaerobic ammonia oxidizing bacteria; step 2, precipitating and washing the selected bacteria and then adding a storage matrix; introducing the high-purity argon gas, and selecting environment conditions including temperature, a matrix concentration and the like in a storage process according to different storage periods; step 3, carrying out activity recovery operation of controllable decompression and temperature rising, and step load on the stored anaerobic ammonia oxidizing bacteria, so as to rapidly obtain high-activity anaerobic ammonia oxidizing bacteria capable of being industrially reutilized. According to the industrial storage and reutilization method, high-activity storage of the anaerobic ammonia oxidizing bacteria is realized and operation factors are control conditions which are easily industrially realized; the industrial storage and reutilization method is simple and convenient to operate and low in cost, and has a very high application value.
Owner:BEIJING MUNICIPAL RES INST OF ENVIRONMENT PROTECTION

Process method for preparing synthesis gas using zero-carbon or negative-carbon emission system

The present invention discloses a process method for preparing synthesis gas by using a zero carbon or negative carbon emission system. The process method comprises that: 1) first raw material gas is subjected to desulfurization, steam is matched, pressurization and heating are performed, a reaction is performed to obtain first conversion gas, the first conversion gas is output, the output first conversion gas and pure oxygen are mixed and then enter a two-stage furnace to react so as to obtain second conversion gas, and the second conversion gas is output from the two-stage furnace; 2) second raw material gas is subjected to desulfurization, pressurization and heating and then is mixed with pure oxygen and carbon dioxide, then a reforming reaction is performed to obtain third conversion gas, and the third conversion gas is output from the reforming reactor; and 3) the second conversion gas is subjected to heat recovery and then is mixed with the third conversion gas to form crude synthesis gas, wherein the crude synthesis gas is adopted as the subsequent synthesis gas with or without a decarbonization device. According to the present invention, the greenhouse gas emission is reduced, the carbon efficiency is improved, the recycling of the carbon resources of the energy source chemicals is achieved, the hydrogen-carbon ratio of the synthesis gas achieves the ideal ratio of the downstream process requirement, and the zero carbon or negative carbon emission of the whole system is achieved.
Owner:SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI +1

Preparation method of high-performance solid buoyancy material

The invention relates to a preparation method of a high-performance solid buoyancy material and belongs to the technical field of materials. Iron chloride is mixed in sodium silicate for crosslinkingforming and pyrolysis, pores formed in sodium silicate during pyrolysis and iron particles formed in the pores are taken as catalysts, nanofiber is grown in situ in a hollow glass microsphere matrix,the root part of the fiber is embedded in a matrix, the head extends out of the matrix, the fiber is closely and seamlessly combined with the matrix, the product is taken as filler, the high-performance solid buoyancy material is prepared, the fiber can slide in a local range of the matrix when the material is impacted by external force and broken, a toughening function is produced on the hollow glass microsphere matrix, and the prepared high-performance solid buoyancy material has good impact resistance. The high-performance solid buoyancy material is prepared with a vacuum impregnation method, equipment is simple, conditions are easy to control, the obtained high-performance solid buoyancy material has uniform quality, and hollow glass microspheres are high in filling rate and have goodthermal resistance.
Owner:皮蒙

Silver plated optical fiber Raman probe and preparation method thereof

ActiveCN107841732AExcellent scattering effectEnables real-time in situ portable detectionMaterial nanotechnologyRaman scatteringSilver plateSolvent
The invention discloses a silver plated optical fiber Raman probe and a preparation method thereof, and belongs to the technical field of medical, chemical and environmental detection and food detection. A one-step solvothermal method is adopted, water or ethylene glycol is used as a solvent, optical fibers which are simply pretreated are soaked into a precursor solution of silver to be subjectedto solvothermal reaction, and the optical fiber Raman probe of which the surface is loaded with Ag nano particles is obtained. The silver nano particles prepared through the preparation method are controllable and adjustable in shape and size, operation is easy, and growing of the silver nano particles and loading, on the optical fibers, of the silver nano particles can be further completed. Compared with traditional Raman enhanced substrates, the excellent surface enhancement Raman scattering effect of the silver nano particles are sufficiently combined with the optical conduction effect of the optical fibers, the size and shape of the obtained silver nano particles are adjusted and controlled, the obtained silver plated optical fiber Raman probe shows super-high sensitivity and selectivity when detecting low-concentration materials, can conduct real-time detection under the severe environment, the remote environment and other special environments, and is high in practicability.
Owner:WUHAN UNIV OF TECH

Molybdenum trioxide/polyaniline composite electrode material with layered structure and preparation method thereof

The invention discloses a preparation method for a molybdenum trioxide/polyaniline composite electrode material with a layered structure. The preparation method comprises the following steps: S1, reacting molybdenum trioxide with organic amine in an alcoholic solvent under stirring to produce a white precipitate, and carrying out pumping filtration, washing and pressure-reduced drying so as to obtain an organic amine-intercalated molybdenum trioxide precursor; S2, reacting the organic amine-intercalated molybdenum trioxide precursor with aniline in an organic acid solvent under stirring to produce a light pink precipitate, and carrying out pumping filtration, washing and pressure-reduced drying so as to obtain an aniline-intercalated molybdenum trioxide compound; and S3, heating the aniline-intercalated molybdenum trioxide compound in an air atmosphere to 100 to 150 DEG C at a heating rate of 0.5 to 5 DEG C/min, carrying out heat insulation treatment for 72 to 120 h, then carrying outslow cooling to room temperature so as to obtain the molybdenum trioxide/polyaniline composite electrode material with the layered structure. The molybdenum trioxide/polyaniline composite electrode material prepared by using the method has no problems of poor conductivity, poor cyclic performance and poor rate performance of conventional molybdenum trioxide negative electrode materials.
Owner:SHANXI CHANGZHENG POWER TECH CO LTD

Method for extraction and purification of corn silk general flavone, and use of corn silk general flavone

InactiveCN102309694BBest Adsorption Separation ConditionsHigh purityMetabolism disorderPlant ingredientsPurification methodsClinical efficacy
The invention relates to a method for extraction and purification of corn silk general flavone, and a use of corn silk general flavone. The method adopts corn silk as a raw material and comprises the following steps of raw material snipping, extraction, condensation and purification. The method is characterized in that the extraction step comprising carrying out extraction by an ethanol solution with concentration of 60% at a temperature of 60 DEG C for 3 hours, wherein a solid-liquid ratio is 1: 20; and the purification step comprising purifying crude extract by a HPD-100 macroporous resin. The prepared corn silk general flavone is added into rabbit forage according to an addition ratio of 2% and has substantial effects of reducing blood fat, wherein P is less than or equal to 0.1. The method has simple operation steps and low costs, is suitable for practical production operation, and can develop integrated utilization of agricultural and sideline products and promote economic prosperity in the country. The method for extraction and purification of corn silk general flavone belongs to the field of corn silk general flavone research and lays the foundation for good development and utilization of corn silk and research of clinical curative effect basis of corn silk general flavone.
Owner:ANHUI AGRICULTURAL UNIVERSITY +1

Method for promoting separation of valuable metals and calcic gangue minerals in waste residue

The invention discloses a method for promoting separation of valuable metals and calcic gangue minerals in waste residue. The method comprises the following steps of: based on calcic waste residue as a treatment object, first, generating anhydrous calcium sulfate crystals by calcic gangue minerals in waste residue through hydrothermal activation; then, through hydrating and crystallizing regulation, hydrating anhydrous calcium sulfate crystals to calcium sulphate dihydrate crystals and enabling the calcium sulphate dihydrate crystals to grow to hundreds of microns; and then, separating the crystals and other substances by a physical separating method. The hydrothermal activating technology comprises the following steps of: adding an additive; and controlling hydrothermal temperature, hydrothermal time, stirring speed and liquid-solid ratio. The hydrating regulation technology comprises the following steps of: adding an excitant, controlling hydrating time, adding crystal seeds, controlling aging time and the like. According to the method provided by the invention, calcium and other valuable metals in waste residue can be recycled at the same time, so that the method is beneficial to realizing reduction, harmlessness and reclamation of waste residue.
Owner:湖南益石科技有限公司

Metallization method of aluminum nitride ceramic plate

The invention relates to an aluminum nitride ceramic plate metalization method, which comprises the following steps of cleaning the surface of an aluminum nitride ceramic plate; forming a titanium conduction layer with the set thickness on the surface of the aluminum nitride ceramic plate; using the aluminum nitride ceramic plate subjected to titanium plating on the surface as a cathode; putting the aluminum nitride ceramic plate into an electrolytic bath; using refined copper as an anode; putting the aluminum nitride ceramic plate into a heat treatment furnace; then, performing heating and temperature rise; seeping the titanium conducting layer to the aluminum nitride to form a TiN metallurgical transition layer and simple substance aluminum; continuously performing heating and temperature rise; sending ultrasonic waves to the aluminum nitride ceramic plate through a ultrasonic wave generating device, so that the liquid-state simple substance aluminum vibrates and flows out; stabilizing the TiN metallurgical transition layer; performing further heating and temperature rise; seeping the titanium conducting layer to the copper plating layer to form a TiCu metallurgical transition layer. Compared with the prior art, the method provided by the invention has the advantages that the liquid-state simple substance aluminum in the TiN metallurgical transition layer vibrates, so that the liquid-state simple substance aluminum melts and is discharged out of the aluminum nitride ceramic plate; the connection intensity of the copper plating layer and the titanium conducting layer is improved; the product quality and the finished product rate are improved.
Owner:FUJIAN HUAQING ELECTRONICS MATERIAL TECH
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