The invention discloses a method for
recovery and comprehensive resource treatment of
phenol and
ammonia in semi-
coke waste water. The method comprises the following steps: performing standing on the semi-
coke waste water to realize gravity oil removing and separating
recovery, filtering an
effluent through a
coke filter to remove a
solid suspension, and introducing the
effluent in an extraction pre-oil removal reactor for deeply removing oil residue, coke
powder and
tar pollutants in the waste water; performing stripping depickling on the waste water after extraction and pre-oil removal, performing
ammonia distilling and performing extraction
processing to remove and recover the acidic gas,
ammonia and
phenol in the waste water, and introducing the processed waste water which reaches the standard in a biochemical
treatment system; performing extraction
processing to obtain a
phenol-rich organic phase, and converting
phenols in an extract phase to
sodium phenolate through alkali washing
processing to realize separation of an extractant and the
phenols; and introducing a
sodium phenolate solution to an acidifying workshop section for acidifying to prepare crude phenol and
sodium salt. The method can realize separation and enrichment of
phenols, heavy oil, light oil, ammonia and acidic gas in the semi-coke waste water, realizes
resource recovery, at the same time, realizes regeneration and cycle utilization of the extractant and alkali lye, and has good application prospect.