This invention discloses a
raw material pretreatment method for
zone melting purification of high-purity aluminum, belonging to the field of non-
ferrous metal refining technology. The
pretreatment method includes alkaline washing, acid
neutralization, cleaning and
drying, and vacuum-protected loading steps. High-purity aluminum
raw material is immersed in a 5-8%
sodium hydroxide aqueous solution at
room temperature for 5-30 seconds, and removed when bubbles begin to form on the substrate. The alkaline-washed aluminum material is then immersed in an 8-12%
nitric acid or
acetic acid aqueous solution for
neutralization for 10-20 seconds. After acid
neutralization, the aluminum material is cleaned and dried, then placed in a
zone melting furnace. A vacuum is drawn, and
inert protective gas is introduced to
atmospheric pressure or a slightly
positive pressure. This method thoroughly removes
oxide scale from the surface and bonding surfaces of the aluminum material, effectively preventing secondary oxidation during post-treatment transfer and loading. It creates continuous and unobstructed
molten pool propagation conditions for the
zone melting process, ensuring the smooth progress of the purification process and the high quality of the final product. This method is particularly suitable for eliminating
oxide scale on the bonding surfaces of segmented aluminum rods to ensure the smooth operation of the zone melting process.