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A raw material pretreatment method for high-purity aluminum zone refining purification

PendingCN122279614Aavoid over corrosionavoid corrosionPretreatment methodAqueous sodium hydroxide
This invention discloses a raw material pretreatment method for zone melting purification of high-purity aluminum, belonging to the field of non-ferrous metal refining technology. The pretreatment method includes alkaline washing, acid neutralization, cleaning and drying, and vacuum-protected loading steps. High-purity aluminum raw material is immersed in a 5-8% sodium hydroxide aqueous solution at room temperature for 5-30 seconds, and removed when bubbles begin to form on the substrate. The alkaline-washed aluminum material is then immersed in an 8-12% nitric acid or acetic acid aqueous solution for neutralization for 10-20 seconds. After acid neutralization, the aluminum material is cleaned and dried, then placed in a zone melting furnace. A vacuum is drawn, and inert protective gas is introduced to atmospheric pressure or a slightly positive pressure. This method thoroughly removes oxide scale from the surface and bonding surfaces of the aluminum material, effectively preventing secondary oxidation during post-treatment transfer and loading. It creates continuous and unobstructed molten pool propagation conditions for the zone melting process, ensuring the smooth progress of the purification process and the high quality of the final product. This method is particularly suitable for eliminating oxide scale on the bonding surfaces of segmented aluminum rods to ensure the smooth operation of the zone melting process.
Owner:KUNMING METALLURGY INST