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58results about How to "Do not change color" patented technology

Nanometer photocatalysis surface protection material for stones and stone cultural relic and preparation method of same

InactiveCN102491781ALong-term protection engravingLong-term protective structureTitaniumSoil resistance
The invention relates to the field of protection of stones and stone cultural relic and provides a nanometer photocatalysis surface protection material for stones and stone cultural relic and a preparation method of the material. According to the invention, titanium alcoholate is taken as the main raw material; the titanium alcoholate, solvent, chelating agent, catalyst and the like are mixed, and are stirred fully under the condition of normal pressure and below the temperature of 100 DEG C to react, so as to obtain anatase titanium dioxide collosol surface protection liquid for stones and stone cultural relic; and a surface protection film made of anatase titanium dioxide photocatalysis material is formed on the surface of a stone, which is cleaned with solvent, through the method of brushing, soaking or the like. The nanometer photocatalysis surface protection material has the advantages that the reversibility is good; the compatibility with stones is good; the acid resistance is strong; the alkaline resistance is strong; the weatherability and the soil resistance are good; the self-cleaning capability is strong; the fungus resistance is good; and the appearance, the color and the hand feeling of the original stone are not affected.
Owner:YUNNAN UNIV

Top dyeing and post-processing method of flame retardant polyester fiber

The invention relates to wool top dyeing of flame-retardant polyester fibers and a post-treatment method thereof. The method comprises the following steps: the flame-retardant polyester fiber wool top is placed in a wool top dyeing machine and operates for 3-5 min at the temperature of 40-50 min, glacial acetic acid is added and PH Value is adjusted to 5-6, monoammonium phosphate and Yuri Huading DIF are added for operating for 5-10min, disperse dye is added for operating for 5-10 min before the temperature rises, the temperature stops rising until 85 DEG C, then the temperature is maintained for 10-15 min, the temperature rises to 100-120 DEG C for operating for 30-60 min, liquor drainage and flushing are carried out with a bath ratio of 1:20-50; the dyed flame-retardant polyester fiber wool top is put into lotion soap with 2-5% of fiber fabric by weight, the lotion soap is processed for 20-30 min at the temperature of 80-90 DEG C, or, the dyed the flame-retardant polyester fiber wool top is first placed in bath consisting of 0.5-2g / L sodium hudroxide , 0.5-2g / L rongalite and 0.5-1g / L nonionic surface active agent for being processed for 20-30 min at the temperature of 70-80 DEG C and then placed in glacial acetic acid bath with 1-4% of fiber fabric by weight for being processed for 10-15 min at the temperature of 40-45 DEG C; the bath ratio is 1:20-1:50. The wool top dyeing of the invention features good levelling of dyeing and high color fastness of dyeing wool top.
Owner:HEILAN HOME

Organosilicon fluorine material for sealing and protecting irony cultural relics and method of producing the same

The invention discloses an organic fluosilicic material used for sealing and protecting an iron cultural relic; the main components of the organic fluosilicic material consists of a main agent, a flatting silica and a thinner; wherein, the component of the main agent is an organic fluosilicic polymer; and the organic fluosilicic polymer is prepared by the hydrolytic polycondensation reaction of an organic silicon mixed monomer and hydroxy fluosilicic oil under the existence of an acid catalyst. The invention also discloses a preparation method of the organic fluosilicic material used for sealing and protecting the iron cultural relic. Test shows that after the organic fluosilicic material is adopted for carrying out sealing and protection on the surface of the iron cultural relic, protections of colorless, transparency, lightless and maintaining the original appearance on the iron cultural relic are realized; the corrosion resistance and the aging resistance are very good; moreover, the organic fluosilicic material has better self-cleaning performance. Not only can the problem of changing the original appearance of the cultural relic commonly existed in iron cultural relic sealing and protecting materials be solved, but also the corrosion resistance and the weatherability can be greatly improved.
Owner:广州市白云文物保护工程有限公司 +1

Composite bionic SiO2/TiO2 protective film and preparation method thereof on the surface of stone historical relic

The invention provides a composite bionic SiO2/TiO2 protective film and a preparation method thereof on the surface of a stone historical relic. Ethyl orthosilicate or sodium fluosilicate is used as a silicon source, anhydrous ethanol and glycerol are added, even mixing is performed, and then nano TiO2 particles are uniformly dispersed in the solution to prepare a base solution. The stone historical relic is cleaned and is soaked and pre-treated with a cetyl trimethyl ammonium bromide solution and then is immersed into the base solution, a small amount of deionized water and ammonia water are slowly and dropwise added, and the stone historical relic is taken out, cleaned and dried naturally after sealed storage is performed at room temperature for a period of time. The composite bionic protective film containing main component SiO2 and TiO2 is formed on the surface of the stone historical relic. The composite bionic SiO2/TiO2 protective film prepared by adopting the preparation method has good combinability with the matrix of a stone material, good acid and alkali resistance capability, hydrophily, permeability, antibacterial performance and self-cleaning performance, and the preparation method can be performed at normal temperature and pressure and is friendly and pollution-free to the environment.
Owner:HUAIYIN INSTITUTE OF TECHNOLOGY

Preparation method of waterborne hyperbranched polyurethane acrylate emulsion, UV curing coating and preparation method and application of UV curing coating

The invention belongs to the technical field of UV curing coatings, and particularly relates to a preparation method of a waterborne hyperbranched polyurethane acrylate emulsion, a UV curing coating and a preparation method and application of the UV curing coating. The UV-curable coating is prepared from the following raw materials in percentage by weight: 60 to 80 percent of waterborne hyperbranched polyurethane acrylate emulsion, 0.05 to 0.1 percent of a defoaming agent, 0.5 to 2 percent of a dispersing agent, 2 to 6 percent of a photoinitiator, 1 to 5 percent of modified nano powder, 0 to 10 percent of an environment-friendly solvent, 1 to 3 percent of an adhesion promoter, 1 to 3 percent of an anti-settling agent and 0.3 to 1 percent of a wetting leveling agent. 0.5-1.5% of a thickening agent and 4-10% of a pigment filler; the invention further provides a preparation method of the UV curing coating for a polypropylene packaging barrel. The UV curing coating for the polypropylene packaging barrel, prepared by the invention, has excellent wear resistance and relatively high adhesive force on the polypropylene packaging barrel, and has excellent weather resistance.
Owner:珠海瑞杰包装制品有限公司

Methyl silicate stone protecting agent and manufacturing method thereof

ActiveCN103571327AKeep breath breathableIncrease contact angleCoatingsSodium silicateSilane coupling
The invention discloses a methyl silicate stone protecting agent and a manufacturing method thereof. The methyl silicate stone protecting agent comprises a methyl silicate, at least one type of silane coupling agent, at least one type of polyethylene glycol and at least one type of water, wherein the adding amount of the methyl silicate is 8-20% of the total weight of a polymer; the adding amount of the silane coupling agent is 1-5% of the total weight of the polymer; the adding amount of the polyethylene glycol is 0-5% of the total weight of the polymer; and the adding amount of the water is 70-91% of the total weight of the polymer. The manufacturing method disclosed by the invention comprises the following steps: dissolving the polyethylene glycol in a small amount of hot water according to the proportion, then sequentially adding sodium methyl silicate and the silane coupling agent in a stirring state and finally replenishing water till 100%. The methyl silicate stone protecting agent disclosed by the invention has the advantages of waterborne and environment-friendly properties, no toxicity, no volatilization, no pollution, short curing time, stable chemical performances, simplicity, convenience and flexibility in construction and operation, safety and low cost. The methyl silicate stone protecting agent is suitable for waterproofness and moisture-proofness of various natural stones, artificial stones and the like. The methyl silicate stone protecting agent particularly has an excellent waterproof effect on the stones with relatively large holes, such as sandstone, cavity stone and the like, and can simultaneously prevent affecting the air permeability of the stones.
Owner:XIAMEN NORNS TECH

Finishing type stone protection agent based on fluorosilicone acrylic resin, and preparation method thereof

The invention discloses a finishing type stone protection agent based on fluorosilicone acrylic resin, and a preparation method thereof. The finishing type stone protection agent comprises, by weight,5-20 parts of a fluorosilicone acrylic resin solution, 10-50 parts of a silane coupling agent, 1-10 parts of low molecular weight hydroxyl-terminated silicone oil, 20-85 parts of a diluent and 0.5-2parts of a catalyst. The preparation method comprises the following steps: uniformly mixing the fluorosilicone copolymer resin solution, the silane coupling agent, the hydroxyl-terminated silicone oil, the diluent and the catalyst, and spraying the obtained mixture on the surface of a stone. A perfluorohexyl side group, a long siloxane side group, methacrylate and a side group containing a crosslinkable functional group exist in the molecular structure of the fluorosilicone acrylic resin. The preparation method has the advantages of reasonable cost, simple process and facilitation of large-scale production, and the prepared stone protection agent has good waterproof and oil-repellent effects, does not change the natural appearance or the air permeability of the stone, does not contain eight or more perfluoro chain segments, and meets the environmental protection requirement.
Owner:SOUTH CHINA UNIV OF TECH

High-efficiency oil-saving agent, preparation method and application thereof

The invention discloses a high-efficiency oil-saving agent, a preparation method and the application thereof. The high-efficiency oil-saving agent comprises 0.05-2.0% of fluorenone compound, 0.05-2.0% of nitrotoluene, 80-99.5% of camphor, 0.3-12% of borneol and balance low-grade fatty alcohol. The preparation method of the high-efficiency oil-saving agent comprises the steps of: completely dissolving the fluorenone compound and the nitrotoluene into the low-grade fatty alcohol, then fully mixing the camphor and the borneol, and obtaining the high-efficiency oil-saving agent. When being added into fuel oil, the high-efficiency oil-saving agent has the oil-saving rate reaching up to 30%. As metal salt is not used as an active agent in the high-efficiency oil-saving agent, residues are not left after the fuel oil is fully burnt, and the service life of an engine can be prolonged; the high-efficiency oil-saving agent is solid additive, thus being convenient for transportation and storage, easily dissolved into the fuel oil and low in adding proportion, and not changing the physical property of the fuel oil; and furthermore, the high-efficiency oil-saving agent is safe and can improve the antiknock property. The invention has simple preparation method and low cost, and is wide in application prospect.
Owner:GUANGZHOU DONGDI ENVIRONMENTAL PROTECTION TECH

Methyl silicate stone protective agent and manufacturing method

ActiveCN103571327BNon-toxic and non-volatileNo pollution in the processCoatingsPolyethylene glycolMethyl group
The invention discloses a methyl silicate stone protecting agent and a manufacturing method thereof. The methyl silicate stone protecting agent comprises a methyl silicate, at least one type of silane coupling agent, at least one type of polyethylene glycol and at least one type of water, wherein the adding amount of the methyl silicate is 8-20% of the total weight of a polymer; the adding amount of the silane coupling agent is 1-5% of the total weight of the polymer; the adding amount of the polyethylene glycol is 0-5% of the total weight of the polymer; and the adding amount of the water is 70-91% of the total weight of the polymer. The manufacturing method disclosed by the invention comprises the following steps: dissolving the polyethylene glycol in a small amount of hot water according to the proportion, then sequentially adding sodium methyl silicate and the silane coupling agent in a stirring state and finally replenishing water till 100%. The methyl silicate stone protecting agent disclosed by the invention has the advantages of waterborne and environment-friendly properties, no toxicity, no volatilization, no pollution, short curing time, stable chemical performances, simplicity, convenience and flexibility in construction and operation, safety and low cost. The methyl silicate stone protecting agent is suitable for waterproofness and moisture-proofness of various natural stones, artificial stones and the like. The methyl silicate stone protecting agent particularly has an excellent waterproof effect on the stones with relatively large holes, such as sandstone, cavity stone and the like, and can simultaneously prevent affecting the air permeability of the stones.
Owner:XIAMEN NORNS TECH

Preparing method of long-acting natural stone protective agent

The invention discloses a preparing method of a long-acting natural stone protective agent, and relates to the technical field of stone protection. The preparing method comprises the steps of at first using lichen as a raw material, using methyl alcohol to extract the lichen, conducting concentration on filter liquor to obtain extractive pasty body, then using ethyl orthosilicate as a silicon resource to prepare and obtain a monodispersing silica solution; mixing the silica solution with deionized water, afterwards using oxalic acid to adjust ph, then adding absolute ethyl alcohol into the mixture to be subjected to still standing and aging, conducting surface finish by adding trimethylchlorosilane so as to endow the silica solution with hydrophobicity, finally mixing filter residues after being filtered with standby extractive pasty body and the like in proportion, and obtaining the long-acting natural stone protective agent. According to the preparing method of the long-acting natural stone protective agent, the effective components in the long-acting natural stone protective agent infiltrates inside a stone along with a solvent, and after the solvent volatilizes naturally, the effective components then combine with crystals and form a three-dimensional net-shape dewatering protective film on the surface of and inside the stone, thus foreign polluant is prevented from permeating in, pollutant inside and at the bottom of the stone is prevented from permeating out; meanwhile, the disadvantages that traditional wax type protective agent can only form films on the surface of the stone and thus block holes of the stone are solved.
Owner:CHANGZHOU YAHUAN ENVIRONMENTAL PROTECTION TECH
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