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42results about How to "Good anti-stickiness" patented technology

Production method of abietic maleic anhydride resin

The invention relates to a production method of abietic maleic anhydride resin, comprising the following two reaction steps of: 1, carrying out addition reaction on abietyl and maleic anhydride to generate an abietic maleic anhydride addition product; and 2, carrying out esterification reaction on the abietic maleic anhydride addition product and pentaerythritol to generate the abietic maleic anhydride resin. The production method is easy and convenient to operate, has the advantages of large temperature control range, high operability, small investment and stable product quality and is a method suitable for industrialized production; in the production method, appropriate process conditions including raw material proportion, reaction temperature, reaction time, catalysts, and the like, are adopted, thereby the acid value and the molecular weight range of a resin product can be effectively controlled; in addition, the resin product obtained with the production method has higher acid value of 150-170 mg KOH/g, reasonable softening point at 140-155 DEG C and good water solubility and is suitable for producing water-based ink, and a formed coating film has toughness and better after-tackiness resistance, water resistance and alkali resistance.
Owner:上海华谊精细化工有限公司上海南大化工厂

Preparation method of rosin modified phenolic resin

The invention relates to a preparation method of a rosin modified phenolic resin. The method comprises the following three steps of reactions: 1. performing condensation of tert-butylphenol, bisphenol A, tung oil and solid formaldehyde under the action of catalyst magnesium acetate and lime to generate polymer of hydroxymethyl tert-butylphenol; 2. performing an addition reaction with rosin to generate an addition product; and 3. performing esterification of the addition product, pentaerythritol and glycerin under the action of catalyst zinc chloride to generate the rosin modified phenolic resin. The preparation method adopts proper raw material proportioning, reaction temperature, reaction time, catalyst and other technical conditions, thus during the production process, the resin viscosity can be effectively controlled, and the operation is simple and flexible and has good effect. The quality of the product is increased, the oil solubility of resin is good, the oil medium viscosity is high, the normal heptane capacity is 4.5ml/g or more; and the prepared paint film ink has good water resistance and alkali resistance, high hardness, excellent anti-after-binding performance, quick-drying performance, lightness and strong adhesive force. Therefore, the preparation method of the invention is applicable to industrial production.
Owner:SHANGHAI HUAYI FINE CHEM CO LTD

High-gloss washing resistant environmental-friendly print paste and preparation method thereof

The invention discloses high-gloss washing resistant environmental-friendly print paste and a preparation method thereof; the printing paste comprises water-based acrylic emulsion, modified water-based polyurethane emulsion, ammonia, defoaming agent, preservative, water-based wax emulsion, wetting and leveling agent, dispersing agent, toner, moisturizing agent and thickener. The preparation method comprises the steps that: A. stirring and filtration: the water-based acrylic emulsion and the water-based polyurethane emulsion are added into a dispersion cylinder by the formula ratio, and are stirred while being sequentially added with the ammonia, the defoaming agent, the preservative, the water-based wax emulsion, the moisturizing agent, the wetting and leveling agent and the dispersing agent; after the materials are added in, the mixture is stirred for 10min to 20min until being uniform fully; the mixture is filtered by a 200-mesh filter mesh bag; B. dispersion and grinding: the toneris added into the liquid mixture, stirred and dispersed for 30min to 50min; the thickener is added in, stirred and dispersed for 10min to 20min; and then the liquid mixture is ground on a three-roll grinder; and C. detection and packaging: the product is sampled to detect the pH value, the viscosity and the fineness, and the product is packaged after all the indexes are qualified.
Owner:BAILIHE CHEM ZHONGSHAN
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