A preparing method of a
graphene-Au-TiO2 multi-component composite
nanotube material is provided. The method includes a step of preparing a
raw material mixture, namely a step of weighing available nanometer particles TiO2 and NaOH raw materials according to a
mass ratio of 1:8, adding the TiO2 and the NaOH into a
corundum crucible, separately weighing
graphene powder and a gold compound into the
corundum crucible, fully mixing the materials and keeping the mixture for later use; a step of high-temperature melting, namely a step of putting the
corundum crucible containing the material mixture at
room temperature into a vacuum high-temperature furnace isolated from air, closing the door of the furnace, opening an
argon flow valve, feeding
argon to remove air in the furnace body, raising the temperature from
room temperature to 400-500 DEG C at a temperature raising speed of 5 DEG C / min, melting the
raw material mixture, cooling the high-temperature furnace to
room temperature, taking the corundum crucible out and stopping
argon, with the raw materials forming
titanate mixed alkali-melt
frit; a step of performing extraction with boiling water; a step of performing hydro-
thermal treatment under
atmospheric pressure; a precipitating and washing step; and a step of performing
calcination to obtain a finished product. The method has characteristics of a low cost, short time, a greatly increased length and stable properties of the prepared nanotubes, and capability of effectively improving photocatalytic properties of the composite nanometer material.