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51results about How to "Mild handling" patented technology

Rare-earth oxide modified high-selectivity catalyst for adiponitrile hydrogenation and hexylenediamine production, preparation method and application thereof

The invention discloses a rare-earth oxide modified high-selectivity catalyst for adiponitrile hydrogenation and hexylenediamine production, a preparation method and application thereof. An alumina-supported nickel-based catalyst is used as an active component, and at 25-90 DEG C and through a parallel flow precipitation process, a low-content rare-earth oxide is used for the modification. A tankreactor is adopted at the low temperature and without an alkaline reagent to carry out a reaction at the pressure of 1-9 MPa for 1-6 h so as to achieve adiponitrile catalytic conversion for high-selectivity preparation of hexylenediamine. No alkaline reagent or NH3 is added during the reaction process to inhibit side reaction of cyclization. The environmental pollution is reduced; and the catalysthas high mechanical strength, the reaction post-treatment is simple and the reaction condition is relatively mild. According to the method and in part of the embodiments, the conversion rate of adiponitrile reaches up to 100% according to set reaction parameters, and selectivity of the product hexylenediamine can reach up to 90%. The invention has good economic benefit and industrial applicationprospects.
Owner:DALIAN UNIV OF TECH

Direct dyeing process for chemical fiber

The invention provides a direct dyeing process for a chemical fiber. The direct dyeing process for the chemical fiber comprises the steps of pretreatment, pre-shaping, modification treatment, dyeing, soaping, color fixing, after-treatment, drying, sizing, calendaring and rolling. According to the direct dyeing process for the chemical fiber, the modification treatment is added, so that performances of a chemical fabric are subjected to the modification treatment basically, the dyeing degree of the fabric is increased, and the difficulty of a subsequent dyeing step is reduced; during dyeing, the mass utilization of inorganic salt is avoided; furthermore, substitute alkali is used for replacing a conventional sodium carbonate substance, so that the consumption is reduced, a color fixation effect is also improved, and the washing fastness of the chemical fiber is further improved; soaping and color fixing processes are added, so that the dyeing fastness is good; environment-protection formaldehyde-free TCD-R is utilized in the color fixing process, and color-fixed fibers are gradually dried, so that the firmness of the fibers is greatly improved; the post-treatment process is added, so that the color fastness and the flexibility of the fabric are improved, the roughness of the fabric is reduced, and the fabric is fluffy and has high resilience.
Owner:TAICANG CHENGLE CHEM FIBER

Three-plasmid whole sealing environmentally friendly vibration fluidized bed dryer

The invention relates to a three-plasmid whole sealing environmentally friendly vibration fluidized bed dryer which is suitable for drying powder material of regular shape such as Laroflex MP with granularity ranging from 50mu m to 5000mu m. The drier comprises a foundation (9), a lower housing (13), a fluidized bed body (6), an upper housing (18) and a bag type dust collector (24); wherein the lower housing (13) is supported on the foundation (9) by a slantly arranged plate spring (12), a case type vibration exciter (14) is arranged at the front end of the lower housing (13), the fluidized bed body (6) is arranged above the lower housing (13) and internally provided with a hood-shaped fluidized bed plate (7), the upper housing (18) is arranged above the fluidized bed body (6) and internally provided with a plurality of groups of bag type dust collectors (24). An air-reserve tank (24.6) is arranged outside the upper housing (18), a plurality of air branch pipes (24.3) are internally arranged in the air-reserve tank (24.6), wherein each air branch pipe (24.3) is provided with a pulse solenoid valve (24.5), the bottom part thereof is provided with an air source hole (24.7). The drier of the invention features low energy consumption, high production efficiency, good operation stability and good uniformity of products.
Owner:江阴丰力生化工程装备有限公司

Low-consumption papermaking wastewater treatment system

The invention discloses a low-consumption papermaking wastewater treatment system which comprises a wastewater pool, a first flocculating settling pool, a fiber recoverer, a second flocculating settling pool, a biological degrading pool and a reused water pool, wherein the wastewater pool is connected to the water inlet end of the first flocculating settling pool; the water discharging end of the first flocculating settling pool is connected to the water inlet end of the fiber recoverer through a pipeline; the water discharging end of the fiber recoverer is connected to the water inlet end of the second flocculating settling pool; the water discharging end of the second flocculating settling pool is connected to the water inlet end of the biological degrading pool; the water discharging end of the biological degrading pool is connected to the reused water pool; a sludge pool is arranged at the bottom of the first flocculating settling pool; the second flocculating settling pool comprises an upper layer, a middle layer and a bottom layer; a water drain pipe connected to a biological settling pool, a backflow pipe connected to the first flocculating settling pool and a sewage drain pipe connected to the sludge pool are respectively arranged at the upper layer, the middle layer and the bottom layer of the second flocculating settling pool. The low-consumption papermaking wastewater treatment system is thorough in wastewater treatment effect and low in energy consumption, and is favorable for popularization and application.
Owner:山西云冈纸业有限公司

Preparation method and application method of electro-Fenton composite membrane cathode

The invention relates to a preparation method and an application method of an electro-Fenton composite membrane cathode, and the method comprises the following steps: uniformly dispersing nano-particles of a heterogeneous iron-containing catalyst in an electrostatic spinning solution, and collecting electrostatic fibers on a conductive carbon material carrier capable of producing hydrogen peroxide by adopting an electrostatic spinning technology, enabling the nano-particles to form an electrospinning catalytic membrane along with the electrostatic fiber generation process and loading the nano-particles on the carrier. According to the preparation method, the yield of hydrogen peroxide can be remarkably improved, especially in the electrostatic fiber generation process, a carbon felt which is modified by graphene and carbon black and has good conductivity is adopted as a fiber receiving device, hydrogen peroxide is efficiently generated in situ on the interface of the modified carbon felt, and .OH is generated in situ on the nano-particle catalysis interface. The yield of hydrogen peroxide is greatly improved, and the micro-pollutants enriched on the surface of the membrane cathode are efficiently catalyzed, so that the efficient removal of the micro-pollutants is realized.
Owner:HEBEI UNIV OF TECH

Method for jointly extracting multiple kinds of yolk protein based on water phase separation and product

The invention provides a method for jointly extracting multiple kinds of yolk protein based on water phase separation and a product. The method includes the steps that (1), fresh yolk is taken, a water phase solution with the volume 0.5-5 times that of the yolk is added for dilution, and the material is stirred, and is subjected to standing or is centrifugally layered; an upper-layer component A,a middle-layer component B and a lower-layer component C are obtained, wherein the water phase solution is polysaccharide matter with the mass percentage concentration of 0.1-0.5% or 2-8% of a water solution of low-molecular polymers; (2), the component A is taken, and yolk low-density lipoprotein is prepared; (3), the component B is taken, and yolk immune globulin is prepared; (4), the componentC is taken, and phosvitin and yolk high-density lipoprotein are prepared. The process is simple and short, the operation is easy, four kinds of yolk protein can be jointly extracted, the extracting efficiency is high, and the unit raw material output is high; extraction is carried out based on water phase separation, reagents used in the method are all food-grade or medicine-grade components, andthe reagents are green and safe; the treatment process is mild, and the functional characteristics and the bio-activity of the protein can be reserved to the maximum degree.
Owner:CHENGDU UNIV

Method for removing heavy metal in enzymatic hydrolysate of sea cucumber by joint use of chelating resins

The invention discloses a method for removing heavy metal in enzymatic hydrolysate of sea cucumber by joint use of chelating resins. The method comprises the following steps of connecting chelating resin containing ethylsuleenyl and 2-aminopyridine and PS-EDTA chelating resin in series, and eluting the enzymatic hydrolysate of sea cucumber by the serially connected chelating resin; decomposing the sea cucumber into polypeptide under the action of enzyme, and removing the heavy metal in supernatant by the chelating resins. While the heavy metal ion is removed, the influence to the content and property of other effective ingredients in the enzymatic hydrolysate is avoided; the Hg, Ni, Cu, Cr, Pb and Cd in the enzymatic hydrolysate of sea cucumber can be effectively removed, the other components are used as raw materials of health-care products, and the standard of health-care products is met. The method has the advantages that the method is simple, and the effect is obvious; under the condition of higher selectivity, the influence to the effective ingredients of the product is avoided, multiple types of metal ions can be removed at one time, the adsorbing rate is high, the resin regeneration is easy, the cost is low, and the scaled production requirement is met.
Owner:山东圣洲海洋生物科技股份有限公司

Method for producing edible food package paper with bean peel as raw material

The invention discloses a method for producing edible food packaging paper with soybean hull as a raw material. The method comprises the following steps: the soybean hulls are subject to superfine comminution, are treated by pressurization for 20 minutes to 2 hours under the pressure of between 130 and 320kPa, and are cooled; an enzymatic reaction is performed under the conditions that the mass concentration of soybean hull powder is between 1 and 25 percent, the mass ratio of cellulose to the soybean hull powder is between 0.1 to 1 and 10 to 1, the temperature is between 25 and 70 DEG C, andthe rotating speed is between 50 and 350rpm; the reaction is terminated when the hydrolysis degree of the reaction reaches between 5 and 20 percent; a filtrate is vacuum concentrated and decolorized by hydrogen peroxide, and then a food thickener and a food plasticizer are added for stirring evenly; the ultrasonic degassing is performed for 30 to 120 minutes after the beating; the filtrate is placed into a mold for molding; and the edible food packaging paper is obtained through drying at a temperature of between 55 and 70 DEG C. The method has green raw material and chloride-free environment-friendly process, has no discharge of acid liquids or alkaline liquids, provides a new approach for the utilization of high added values of biomass resources, and also provides broad prospect for thedevelopment of special paper.
Owner:SOUTH CHINA UNIV OF TECH

Paper making wastewater treatment system

A paper making wastewater treatment system comprises a wastewater basin, a first flocculating settling basin, a fiber recoverer, a second flocculating settling basin, a biodegradation basin and a recycled water basin, wherein the wastewater basin is connected to the water inlet end of the first flocculating settling basin, the water discharge end of the first flocculating settling basin is connected to the water inlet end of the fiber recoverer, the water discharge end of the fiber recoverer is connected to the water inlet end of the second flocculating settling basin, the water discharge end of the second flocculating settling basin is connected to the water inlet end of the biodegradation basin, and the water discharge end of the biodegradation basin is connected to the recycled water basin; a sludge basin is arranged on the bottom of the first flocculating settling basin, the second flocculating settling basin comprises an upper layer, a middle layer and a bottom layer, and the upper layer, the middle layer and the bottom layer are provided with a drainage pipe connected to the biodegradation basin, a return pipe connected to the first flocculating settling basin and a blow-off pipe connected to the sludge basin respectively. The system can treat wastewater thoroughly, is low in energy consumption, and can be used and popularized easily.
Owner:乾坤环保股份有限公司
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