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43results about How to "Suitable for large-scale process production" patented technology

Hydrophilic material-doped blended membrane nanoscale zero-valent iron-loading composite material as well as preparation method and application thereof

The invention discloses a hydrophilic material-doped blended membrane nanoscale zero-valent iron-loading composite material as well as a preparation method and application thereof. The method comprises the steps of (1) synthesizing a hydrophilic material; (2) doping the hydrophilic material during a blended membrane synthesis process; (3) soaking the hydrophilic material-doped blended membrane into a bioinspired polymer solution, and functionalizing; (4) soaking the functionalized hydrophilic material-doped blended membrane into a soluble ferric salt solution, and loading an iron ion onto a boehmite-doped blended membrane; (5) soaking the iron-loading blended membrane into a borohydride solution, thus forming the hydrophilic material-doped blended membrane nanoscale zero-valent iron-loadedcomposite material through a high reduction function. The method is low in cost, and the operation process is simple and convenient; and the prepared nanoscale zero-valent iron particles are good indispersing performance, high in reaction activity and easy to recycle, has a good removal capability on heavy metals, organic dyestuffs and antibiotic wastewater, cannot cause secondary pollution, andhas a wide application prospect in the field of environment pollution remediation.
Owner:KUNMING UNIV OF SCI & TECH

Water-based industrial detergent capable of self-defoaminng at normal temperature and preparation method thereof

The invention relates to a water-based industrial detergent capable of self-defoaming at normal temperature and a preparation method thereof. The detergent comprises the following components in percentage by weight: 2-15% of ethylene oxide epoxypropane copolymerized polyoxyethylene, 0.5-5% of triethanolamine, 0.5-4% of sodium metasilicate anhydride, 0.1-2% of fatty alcohol-polyxyethylene ether, 0.1-5% of advanced fatty alcohol (C8-15), 1-5% of sodium gluconate, 0.5-5% of ethylene diamine tetraacetic acid and the balance of water. The preparation method mainly comprises the following steps: dissolving the sodium metasilicate anhydride, the sodium gluconate and the ethylene diamine tetraacetic acid in the water; and then adding the ethylene oxide epoxypropane copolymerized polyoxyethylene, the triethanolamine, the fatty alcohol-polyxyethylene ether, the advanced fatty alcohol (C8-15) and the like in sequence, and mixing to finally obtain the industrial detergent. In the invention, based on the combined action of lipophilic group epoxypropane in the ethylene oxide epoxypropane copolymerized polyoxyethylene and lipophilic group in the system as well as industrial oil stain, the intensity of foam generated in the process of cleaning is reduced so as to realize the self-defoaming effect; through the synergistic effect of various components, optimal cleaning and antirust effects are achieved; simultaneously, through the synergistic effect of various surfactants, the defect that inorganic salts always form white spots on the surface of a workpiece is obviously improved.
Owner:华阳新兴科技(天津)集团有限公司

Micelle modified nanometer zero-valent iron particle and preparation method and application thereof

The invention discloses a micelle modified nanometer zero-valent iron particle and a preparation method and application thereof and belongs to the technical field of preparation and modification of nanometer materials. The modified nanometer zero-valent iron particle comprises nanometer zero-valent iron and environment-friendly micelle poloxamer (comprising poloxamer F68, poloxamer F108 and poloxamer F127; and the poloxamer micelle wraps the surface of the nanometer zero-valent iron. According to the method, in a poloxamer aqueous solution, a solution of a strong reducing agent KBH4, a NaBH4 solution or a green tea solution is utilized to reduce Fe2+ so that Fe0 can be obtained. According to the micelle modified nanometer zero-valent iron particle and the preparation method and the application of the micelle modified nanometer zero-valent iron particle, the nanometer zero-valent iron is modified through the poloxamer, the micelle is formed through self-assembly of the poloxamer in the aqueous solution, stabilization of the nanometer materials is achieved, the prepared nanometer particle is good in dispersing performance and high in reactivity, and the defects that the nanometer particle is prone to clustering in water and prone to oxidation in air are overcome. The pollutant removing capacity of the micelle modified nanometer zero-valent iron particle is far higher than that of a non-modified nanometer zero-valent iron particle, the micelle modified nanometer zero-valent iron particle is friendly to the environment, secondary pollution cannot be generated, equipment needed for preparation is simple, the process is simple and convenient, and the micelle modified nanometer zero-valent iron particle can be widely used for treatment of environmental pollution and the environment restoration field.
Owner:KUNMING UNIV OF SCI & TECH

Water-based type soldering flux cleaning agent and preparation method thereof

The invention relates to the technical field of cleaning agents, in particular to a water-based type soldering flux cleaning agent and a preparation method thereof. The water-based type soldering fluxcleaning agent is prepared from the following raw materials in parts by weight: 20 to 40 parts of fatty amine, 20 to 40 parts of glycol ether, 5 to 15 parts of non-ionic surface active agent, and 10to 30 parts of deionized water. The water-based type soldering flux cleaning agent provided by the invention is a water-based type cleaning agent, does not contain a fluoro-carbon solvent and a halogenated hydrocarbon solvent harmful to a human body so as not to hurt human health, is convenient to use, safe, environmentally-friendly, non-toxic and economical, and simple in use method, can be usedfor soaking or ultrasonically cleaning, and is capable of remarkably improving the cleaning work efficiency of parts. The water-based type soldering flux cleaning agent provided by the invention has ahigher cleaning effect on a soldering flux, and can be used for cleaning the soldering flux and welding slags on workpieces; electronic parts treated through the cleaning agent are clean in surface,and can be directly assembled or packaged after being subjected to water rinsing and air drying.
Owner:东莞市亿洁优实电子科技有限公司

Flame-retardant high-molecular material and preparation method thereof

The invention relates to the technical field of high-molecular materials, in particular to a flame-retardant high-molecular material and a preparation method thereof. The preparation method includes:sequentially adding polyvinyl chloride, nano calcium silicate hydrate, calcium sulfate, pyridine-styrene-butadiene latex, polyvinylidene chloride, antimonous oxide, alumina hydroate, zinc borate, magnesium hydroxide, polybenzimidazole fiber, DOPO derivative flame retardant, modified inorganic filler, compatilizer, toughener, plasticizer and defoamer into a multidirectional motion mixing stirrer, mixing and stirring for 15-20min, and stirring while hot melting for 0.8-1h; 2), subjecting a high-molecular material after stirring to double-screw extrusion, wherein length-diameter ratio of a double-screw extruder is 50:1, extrusion temperature at the first stage is 60-80 DEG C, the extrusion temperature at the second stage is 100-120 DEG C, and the extrusion temperature at the third stage is 140-160 DEG C; 3), pelletizing the high-molecular material after double-screw extrusion to obtain the flame-retardant high-molecular material. The flame-retardant high-molecular material is simple in preparation process, low in cost and suitable for large-scale industrial production.
Owner:安徽律正科技信息服务有限公司

A kind of micelle modified nano zero-valent iron particle and its preparation method and application

The invention discloses a micelle-modified nanometer zero-valent iron particle, a preparation method and an application thereof, and belongs to the technical field of preparation and modification of nanometer materials. The modified nano-zero-valent iron particles of the present invention include nano-zero-valent iron and environment-friendly micellar poloxamers (including poloxamer F68, poloxamer F108 and poloxamer F127), poloxamer The micelles are coated on the surface of the nanometer zero-valent iron. The method of the present invention is to use a strong reducing agent KBH4 solution, NaBH4 solution or green tea solution to reduce Fe2+ in a poloxamer aqueous solution to obtain Fe0. The invention adopts poloxamer to modify nanometer zero-valent iron, forms micelles through the self-assembly of poloxamer in aqueous solution, realizes the stabilization of nanomaterials, and the prepared nanoparticles have good dispersion performance and high reactivity High, overcomes its shortcomings of easy aggregation in water and easy oxidation in air. The ability to remove pollutants is much higher than that of unmodified nano-zero-valent iron particles, and it is environmentally friendly without secondary pollution. The equipment required for preparation is simple and the process is simple, and it can be widely used in the treatment of environmental pollution and environmental pollution. Repair field.
Owner:KUNMING UNIV OF SCI & TECH

Forming method of composite material winding shaft containing injection layer

The invention relates to a forming method of a composite material winding shaft containing an injection layer, belongs to the field of mold forming and aims to solve the problem that an existing composite material winding shaft with a fluid material interlayer cannot be formed. A mold body is mounted on a horizontal winding machine, the outer surface of the mold body is sanded with 200-mesh sand paper, then the sanded surface of the mold body is cleaned with cotton yarns, and the mold body is coated with a mold releasing agent; and the surface, coated with the mold releasing agent in the firststep, of the mold body is coated with body colloid, carbon fibers are mounted on a winding tensioner of the horizontal winding machine, first-layer annular winding of the carbon fibers is performed on the outer surface of the mold body, the initial tension of the first-layer annular-wound carbon fibers is set to be 30+/-3N/cluster, the winding angle is set to be 85-90 degrees, winding is repeatedfor two to four times, the winding length of the first annular-wound carbon fiber layer is 150-500 mm, and the total wound layer thickness of the first annular-wound carbon fiber layer is 0.5-2 mm. By means of the forming method of the composite material winding shaft containing the injection layer, integrated forming of the fluid material interlayer and the first and second carbon fiber composite layer is achieved.
Owner:HARBIN FRP INST

Hydrophilic material-doped blend film-loaded nano-zero-valent iron composite material and its preparation method and application

The invention discloses a hydrophilic material-doped blend film-loaded nano-zero-valent iron composite material and its preparation method and application. The method includes: (1) synthesizing the hydrophilic material; (2) during the synthesis process of the blend film, Doping with hydrophilic materials; (3) Soaking the blended membranes doped with hydrophilic materials into a biostimulated polymer solution for functionalization; (4) Immersing the functionalized blended membranes doped with hydrophilic materials in a soluble iron salt solution , so that iron ions are loaded onto the boehmite-doped blend membrane; (5) The blend membrane loaded with iron ions is immersed in borohydride salt solution, and the hydrophilic material doped blend membrane is formed by strong reduction. Nano-zero-valent iron composite material; the method is low in cost and easy to operate, and the prepared nano-zero-valent iron particles have good dispersion performance, high reactivity, easy recovery, good removal ability for heavy metals, organic dyes and antibiotic wastewater, and will not It produces secondary pollution and has broad application prospects in the field of environmental pollution restoration.
Owner:KUNMING UNIV OF SCI & TECH

Oxygen vacancy-enriched bismuth molybdate photocatalytic material as well as preparation method and application thereof

The invention discloses an oxygen vacancy-enriched bismuth molybdate photocatalytic material, which relates to the technical field of photocatalysis, has a chemical formula of Bi4MoO9, and is prepared by the following steps: (1) dissolving bismuth nitrate in a proper amount of deionized water, and adding a dispersing agent while stirring to react for 1 hour; dissolving soluble vanadium salt in a proper amount of water, and stirring for 30 minutes; mixing and stirring the solutions to form a precursor solution A; (2) respectively dissolving bismuth nitrate and Na2MoO4. 2H2O in a proper amount of nitric acid and sodium hydroxide, and then adding citric acid into the bismuth nitrate solution; mixing the solutions to form a precursor solution B; (3) respectively adjusting the pH values of the solution A and the solution B to 7, standing, mixing, and transferring to a hydrothermal reaction kettle for reaction; and (4) cooling the reaction kettle, drying powder obtained by suction filtration, and roasting at high temperature to obtain a sample. The prepared photocatalytic material is very high in oxygen vacancy activity, simple in reaction condition and convenient to control, and has a very strong degradation effect on rhodamine 6B.
Owner:CHONGQING UNIV OF ARTS & SCI
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