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60 results about "Food chemistry" patented technology

Food chemistry is the study of chemical processes and interactions of all biological and non-biological components of foods. The biological substances include such items as meat, poultry, lettuce, beer, and milk as examples. It is similar to biochemistry in its main components such as carbohydrates, lipids, and protein, but it also includes areas such as water, vitamins, minerals, enzymes, food additives, flavors, and colors. This discipline also encompasses how products change under certain food processing techniques and ways either to enhance or to prevent them from happening. An example of enhancing a process would be to encourage fermentation of dairy products with microorganisms that convert lactose to lactic acid; an example of preventing a process would be stopping the browning on the surface of freshly cut apples using lemon juice or other acidulated water.

Device and method for detecting analytes

The invention relates to a method for detecting analytes and to a device for carrying out the method, for use for analysis or diagnosis in the fields of chemistry, biochemistry, molecular genetics, food chemistry, biotechnology, the environment and medicine. Marker particles (5) with different electrical properties or a different relative permeability to those of the measuring solution (3) surrounding them are used to detect the analytes (8). The marker particles (5) either bond specifically to the analytes (8) or to a base (2) in competition with the analyte. The analytes (8) are detected by the changes in an electrical field or an electrical current generated by electrodes (2) or in an electrical voltage applied to an electrode or in a magnetic field, said changes being caused by marker particles which have bonded with the analytes or by marker particles which have instead bonded to the base in an electrical field.
Owner:KNOLL MEINHARD

Blood and saliva biomarker optimized food consumption and delivery with artificial intelligence

A computer implemented method for use in conjunction with a computing device, system, network, and cloud with touch screen two dimension display or augmented / mixed reality three dimension display comprising: obtaining, analyzing and detecting user blood and saliva chemistry data and mapping the blood and saliva data into a database associated with a specific user, applying the data with optimization equations and mapping equations to food chemistry such that a user may order food and beverage from a food / beverage distribution point or have food / beverage delivered to the user which has been specifically optimized for their specific blood characteristic target ranges. The method and system uses recursive techniques and neural networks to learn how to optimize food and beverage nutrient efficiency into the users blood chemistry.
Owner:CIRCLESX LLC

Method for removing 5-hydroxymethyl furfural (5-HMF) in high-fructose corn syrup (HFCS)

The invention relates to the food processing technology, in particular relates to a method for removing 5-hydroxymethyl furfural (5-HMF) in high-fructose corn syrup (HFCS), and belongs to the technical field of food chemistry. The method comprises the following steps: (1) feed liquid pretreatment: the chromaticity of the HFCS is controlled at below 30RBU; (2) adsorption: the 5-HMF content in the HFCS discharged from an adsorption column is less than 5mg / kg; (3) ion exchange: the electrical conductivity of the HFCS discharged from an ion exchange column is less than 5mu s / cm, and the PH value of the HFCS is 3-8; (4) deodorization: the chromaticity of the HFCS is less than 5RBU, and the light transmittance of the HFCS is more than 99%; and (5) concentration: the deodorized HFCS is evaporated by an evaporator so as to obtain the finished product of the HFCS with the mass concentration of 75-78%. The method has the advantages of simple process flow, low production cost and obvious removal effect of the 5-HMF (the content is less than 5mg / kg), and the adopted adsorbent can be reused after treatment.
Owner:SHANDONG SCENTS JIANYUAN BIO TECH

High-stability mustard oil nanometer emulsion and preparation method thereof

The invention relates to a high-stability mustard oil nanometer emulsion and a preparation method thereof, and belongs to the technical field of food chemistry and food processing. According to the present invention, the high-stability mustard oil nanometer emulsion is prepared through emulsifying liquid preparation, oil phase preparation, mixing, high-speed shearing and homogenization, and is used for seasoning juices or mustard salad sauces; according to the prepared high-stability mustard oil nanometer emulsion, the water solubility of the mustard oil is improved, and the volatilization of the mustard oil is avoided; and compared with other mustard products, the product of the present invention has the following characteristic that the hydrolysis rate of the isothiocyanate during the storage process is decreased, such that the mustard oil has the good storage stability.
Owner:JIANGNAN UNIV +1

Stevia rebaudiana enzyme VI and method for converting rebaudioside-A into rebaudioside-D

The invention belongs to the field of food chemistry, and particularly relates to a method for converting RA (rebaudioside-A) which is taken as a raw material into RD (rebaudioside-D), and the key is stevia rebaudiana enzyme VI and a preparation method thereof. The converting method comprises the following steps: A, the RA of which the purity is higher than 90% is dissolved with water according to the weight measurement ratio of 1:6-1:10m / v; B, UDP-Glu (Uridine Diphosphate Glucose) is added according to the weight ratio that RA:UDP-Glu=15:5-15:9; C, the stevia rebaudiana enzyme VI is added according to the weight ratio that RA: stevia rebaudiana enzyme VI=(800-1200):1 (preferably 1000:1), and then reaction is carried out for 3-7h at the temperature of 40-60 DEG C and the pH of 6-8; and D, a reaction solution is filtered and dried to obtain RD-containing solid matter. The conversion rate of converting RA into RD is larger than or equal to 70%, and the RD content in the solid matter is 60%-70%, can achieve 80% after further separation and purification, and even can be larger than 90%.
Owner:SICHUAN INGIA BIOSYNTHETIC CO LTD

Stevioside derivative prepared by stervioside biotransformation, preparation method and application thereof

The invention relates to a stevioside derivative prepared by stervioside biotransformation and a preparation method and an application thereof, and belongs to the field of food chemistry. According to the method, stervioside, which is used as a substrate, undergoes enzyme catalysis by the utilization of UDP-glucosyltransferase in the presence of a glucosyl donor under conditions of proper temperature, pH, salinity, substrate concentration and the like, so as to obtain a stevioside derivative NY101 with a brand-new structure. The method for preparing the stevioside derivative NY101 by stervioside biotransformation is simple to operate, is low-cost, and has high transformation efficiency. Transformation efficiency can be greater than 90%. Purification is easy, purity is high, and purity can be greater than 95%. The stevioside derivative NY101 can be used in the food and beverage industry and has huge potential application value.
Owner:NANJING NUOYUN BIOLOGICAL TECH CO LTD

Method for measuring pyrethroid pesticides in grain by dispersion liquid micro-extraction-high performance liquid chromatography

The invention belongs to the technical field of food chemistry, and provides a method for measuring pyrethroid pesticides in grain by dispersion liquid micro-extraction-high performance liquid chromatography. Thymol or choline chloride is used as a hydrogen-bond acceptor, valproic acid, hexylic acid, heptanoic acid, caprylic acid, n-nonanoic acid or capric acid is used as a hydrogen-bond donor, the mole ratio of the hydrogen-bond acceptor to the hydrogen-bond donor is 1 / 5, 1 / 4, 1 / 3, 1 / 2, 1 / 1, 2 / 1, 3 / 1 or 4 / 1; a hydrophobic eutectic solvent formed by mixing the hydrogen-bond acceptor and the hydrogen-bond donor is used as an extraction agent, liquid micro-extraction is performed, and the pyrethroid pesticides in grain are measured by high performance liquid chromatography. The method provided by the invention has the advantages of being simple to operate, quick, sensitive, less usage of extraction agent, easy to collect, green and environment-friendly, can be used for detecting pyrethroid pesticides in a number of grain samples. The usage of harmful organic solvent can be avoided, and less extraction agent is used; and the method has the significant advantages of being simple and quick to operate, easy to collect, green and environment-friendly, and good in reproducibility.
Owner:SHANXI AGRI UNIV

Preparation process of allium schoenoprasumL. oil

The invention provides a preparation process of allium schoenoprasumL. oil, relating to the food chemistry field. The preparation process is characterized by comprising the following steps: (1) selecting fresh soybean salad oil and small allium schoenoprasumL., cutting off the stalks of the small allium schoenoprasumL. and cutting the leaves of the allium schoenoprasumL. into small sections as narrow and uniform as possible; (2) throwing the fresh soybean salad oil and small allium schoenoprasumL. prepared in the step (1) into a flask in a proportion of 1: 2, putting the flask into an electric jacket and switching on a temperature controller, controlling the temperature at 120-125 DEG C and heating the materials for 2 hours; and (3) filtering, standing and cooling the raw materials heated in the step (2) and taking the upper clear liquor after cooling, thus obtaining the allium schoenoprasumL. oil. The preparation process has the following beneficial effects: the process is simple and practical; the extracted allium schoenoprasumL. oil has pure smell, bright color and long shelf life and is not easy to change taste.
Owner:ANHUI CHINAHERB FLAVORS & FRAGRANCES

High-efficient and safe aquatic product preservative

The present invention relates to the technical field of food chemistry and particularly relates to a high-efficient and safe aquatic product preservative. The aquatic product preservative consists of the following raw materials in percentages by weight: 10-15% of garlic concentrate, 10-20% of chitosan, 10-20% of tea polyphenols, and the balanced water. The object of the present invention is to provide the high-efficient and safe aquatic product preservative which is good in preservative effects and long in shelf life.
Owner:宋国祥

Plant-derived food chemical pollutant risk analysis and detection method

The invention belongs to the technical field of food safety, and discloses a plant-derived food chemical pollutant risk analysis and detection method. The method comprises the steps of acquiring food-related data through a food tracing module; selecting a to-be-detected plant-derived food sample through a sample acquisition module and processing the to-be-detected plant-derived food sample; determining risk factors of the plant-derived food through a risk factor determination module, carrying out risk evaluation and classified statistics, and meanwhile outputting a risk analysis table; carrying out health risk evaluation through the food health risk evaluation module, and finally carrying out health data storage and display. The method is simple, convenient and rapid to operate, accuratein detection result and capable of detecting heavy metal, pesticide and radioactive chemical pollution; risk evaluation and health risk evaluation can be carried out on the basis of detected chemicalpollutants, the risk analysis table is output, the chemical pollution types of different types of food in different production places, different transportation processes and different storage processes are comprehensively and accurately mastered, and food safety control is facilitated.
Owner:龙口海关综合技术服务中心

Method for enhancing gel property of soybean protein by cold plasma

The invention belongs to the field of food chemistry, and discloses a method for enhancing the gel property of soybean protein by cold plasma. The soybean protein is dissolved in deionized water to obtain a soybean protein solution. The soybean protein solution is treated by cold plasma. Then first-stage water bath heating treatment is carried out, then the solution is cooled to room temperature,a coagulant is added for uniform stirring, second-stage water bath heating treatment is carried out, the obtained gel is fully shaped through refrigeration, and the soybean protein gel is obtained. The method for enhancing the gel property of soybean protein by cold plasma has physical and chemical effects, the soybean protein is modified at low temperature, and the strength and structural compactness of the soy protein gel are effectively enhanced.
Owner:SOUTH CHINA UNIV OF TECH

Method for establishing fingerprints of volatile components in agricultural products and their processed products

The invention belongs to the technical field of food chemical pattern recognition, and in particular relates to a method for establishing fingerprints of volatile components of agricultural products and processed products thereof. At present, the main form of fingerprints for food chemical pattern recognition is the spectrum formed by the chromatographic elution curves of chemical components in geographical indication products. People cannot directly obtain relevant information about product quality, and it is not easy to understand intuitively, especially when analyzing When the system is very complex, the application and promotion of this type of fingerprint is limited. The present invention uses volatile components that can represent the sensory quality and style characteristics of agricultural products and processed products to express and analyze the fingerprint characteristics of samples, and establishes chemical pattern characteristics that can intuitively express the analysis objects to establish fingerprints to identify the characteristics and flavors of the objects. The present invention can be used as the objective chemical information barcode of the product itself, and the symbolic effect of expressing the uniqueness of the product is very obvious.
Owner:NORTHWEST A & F UNIV

Benzophenone derivatives serving as tyrosinase activating agents and applications thereof

ActiveCN106420680AGood activation rateEfficient activationCosmetic preparationsHair cosmetics2-hydroxybenzophenoneFood chemistry
The invention belongs to the technical field of cosmetics, medicines and food chemistry, and discloses benzophenone derivatives serving as tyrosinase activating agents and applications thereof. The benzophenone derivatives serve as the tyrosinase activating agents and are one or more than one of 2-hydroxybenzophenone, 3-hydroxybenzophenone, 4-hydroxybenzophenone, 4-methoxybenzophenone, 4-aminobenzophenone, 3-aminobenzophenone, 4, 4'-dihydroxy benaophenonel, 2, 4, 4'-trihydroxybenzophenone or 3-methoxyl-4, 4'-dihydroxy benaophenonel. The compounds disclosed by the invention have intense tyrosinase activation activity and obvious application prospect in medicines (such as treatment of leucoderma) and cosmetics (such as hair-blacking liquid shampoo).
Owner:GUANGDONG IND TECHN COLLEGE

Octenyl succinic acid waxy corn starch ester naringin inclusion compound and preparation method thereof

The invention provides an octenyl succinic acid waxy corn starch ester naringin inclusion compound and a preparation method thereof, and belongs to the technical field of food chemistry. The inventionprovides an octenyl succinic acid waxy corn starch ester naringin inclusion compound, in which naringin is used as a core material, and the octenyl succinic acid waxy corn starch ester (OSAS) with the molecular weight of 1.0*10<4> to 2.0*10<5> Da is used as a packing material for clathration of the naringin, so that the solubility and the bioavailability of the naringin can be improved, and the application of the naringin in in the industries of food, beverages, medicines and the like is expanded.
Owner:ZHEJIANG ACADEMY OF AGRICULTURE SCIENCES

Continuous weighing system for small products and weighing method thereof

The invention belongs to the technical field of pharmacy, food, chemicals and processing and manufacturing, and particularly relates to a continuous weighing system for small products and a weighing method thereof. The weighing system is installed on a support; and the support is used for supporting the weighing system. The weighing system comprises a discharging mechanism, a conveying and transferring mechanism, a push rod, a pushing mechanism, a reset mechanism, a weighing mechanism and a connecting rod following mechanism. The discharging mechanism is arranged at the top of the support; the conveying and transferring mechanism is arranged below the discharging mechanism; the conveying and transferring mechanism comprises a transferring wheel, a plurality of first channels, a plurality of sliding blocks, a plurality of first grooves and a guide base; the pushing mechanism is arranged on one side of the transferring wheel; the reset mechanism is used for pushing the sliding block connected with the push rod to slide in the initial direction along the first channel; and the weighing mechanism is arranged below the transferring wheel. By means of the conveying and transferring mechanism, the small products are not extruded to deform in the whole conveying and transferring process; and the risks of damage and powder leakage of the small products are reduced.
Owner:SHANGHAI QUNTIN-TECH CO LTD

Pectin graft copolymer as well as preparation method and application thereof

The invention relates to the technical field of food chemistry, in particular to a pectin graft copolymer as well as a preparation method and application thereof. The pectin graft copolymer takes pectin as a main body and ferulic acid as a graft. The pectin graft copolymer disclosed by the invention has the advantages of good oxidation resistance, more uniform and smoother surface structure, excellent comprehensive performance, environment-friendliness and easiness in biodegradation, and provides a new way for development of pectin derivative products.
Owner:CHINA AGRI UNIV

Phenolic hydroxyl-containing aryl compound acting as tyrosinase activator and application thereof

The invention belongs to the technical field of cosmetics, medicine and food chemistry and discloses a phenolic hydroxyl-containing aryl compound acting as tyrosinase activator and application thereof. The phenolic hydroxyl-containing aryl compound is used as tyrosinase activator, and is from more than one of 1,5-dihydroxynaphthalene and 2,2'-diphenol. The compound related herein has strong tyrosinase activating activity, and has significant application prospect in medicine (such as for treating vitiligo) and cosmetics (such as hair-blacking shampoo).
Owner:GUANGDONG IND TECHN COLLEGE

Rapid inspection method for grease plasticizer

The invention belongs to the technical field of food chemistry, and discloses a rapid inspection method for a grease plasticizer. The method includes the steps: extracting the plasticizer in grease from the grease by the aid of methyl alcohol to obtain extract liquor; performing high-speed refrigerated centrifugation on the extract liquor to obtain liquid supernatant; analyzing the liquid supernatant by the aid of a GC-MS (gas chromatography-mass spectrometer) to obtain a specific value of the plasticizer. The inspection method is high in efficiency and recovery rate, low in loss, accurate indata, easy to operate and applicable to inspection of process grease and batch grease in the production process.
Owner:金胜粮油集团有限公司 +1

Preparation of tans-3,5- dihydroxy-4'- acetylamido-stilbene

The invention relates to preparation of a novel resveratrol derivative trans-3,5-dihydroxy-4'- acetylamido-stilbene, and belongs to the fields of organic chemistry and food chemistry. The invention aims to solve the technical problems by providing a preparation process of the resveratrol derivative tans-3,5-dihydroxy-4'- acetylamido-stilbene, wherein the preparation process has mild reaction conditions, high reaction selectivity, little side reaction, simple separation of products and high yield. The preparation process is characterized in that raw materials including 3,5-dimethoxybenzaldehyde, p-acetamido benzyl chloride, triethyl phosphite and boron tribromide are subjected to three step of chemical reactions to obtain the product trans-3,5-dihydroxy-4'- acetylamido-stilbene.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Stevia rebaudiana enzyme VI and method for converting rebaudioside-A into rebaudioside-D

The invention belongs to the field of food chemistry, and particularly relates to a method for converting RA (rebaudioside-A) which is taken as a raw material into RD (rebaudioside-D), and the key is stevia rebaudiana enzyme VI and a preparation method thereof. The converting method comprises the following steps: A, the RA of which the purity is higher than 90% is dissolved with water according to the weight measurement ratio of 1:6-1:10m / v; B, UDP-Glu (Uridine Diphosphate Glucose) is added according to the weight ratio that RA:UDP-Glu=15:5-15:9; C, the stevia rebaudiana enzyme VI is added according to the weight ratio that RA: stevia rebaudiana enzyme VI=(800-1200):1 (preferably 1000:1), and then reaction is carried out for 3-7h at the temperature of 40-60 DEG C and the pH of 6-8; and D, a reaction solution is filtered and dried to obtain RD-containing solid matter. The conversion rate of converting RA into RD is larger than or equal to 70%, and the RD content in the solid matter is 60%-70%, can achieve 80% after further separation and purification, and even can be larger than 90%.
Owner:SICHUAN INGIA BIOSYNTHETIC CO LTD

Stevioside derivative and application of stevioside derivative

The invention relates to a stevioside derivative and application of the stevioside derivative and belongs to the technical field of food chemistry. The stevioside derivative takes a stevioside derivative compound (I) as a substrate so that the substrate is reacted in the presence of a glucosyl donor and under a catalytic effect of UDP (Uridine Diphosphate)-glucosyl transferase to generate a stevioside derivative compound (IV). The stevioside derivative has the advantages of green and safe production process, low production cost, short period and capability of extremely improving the competitiveness of a product. The stevioside derivative has the advantages of simplicity in operation, high conversion efficiency and easiness of purification, so that the purity of the obtained product is high and can be used for food and beverage industries; the product has an important application value.
Owner:NANJING NUOYUN BIOLOGICAL TECH CO LTD

Method for separating and detecting diphenylamine and rhodamine B by using gold nano channel

InactiveCN104090035ASeparation is fast, accurate and effectiveReasonable methodComponent separationCarcinogenFood chemistry
The invention discloses a method for separating and detecting diphenylamine and rhodamine B by using a gold nano channel. A PC (polycarbonate) membrane is used as a template, and gold is deposited on hole walls of the PC membrane template with nano aperture by adopting a chemical deposition method to obtain a functional hydrophobic gold nano channel; diphenylamine serving as a hydrophobic molecule easily passes through the hydrophobic gold nano channel; the rhodamine B is a cationic compound, belongs to a hydrophilic molecule and can not migrate in the hydrophobic gold nano channel; separation of the diphenylamine and the rhodamine B is realized according to the difference of the hydrophobic property of the two; the transmission quantity of each of the diphenylamine and the rhodamine B passing through the gold nano channel is detected by using an ultraviolet detector. The method can be applied to the fields of contemporary medicinal chemistry, agricultural chemistry, food chemistry and biochemistry, and is particularly used for separating carcinogenic substances such as food dyes and protecting food safety and body health.
Owner:HUNAN CITY UNIV

Lentinan soluble bean for improving intestinal immunity of children by diet and preparation method thereof

InactiveCN112544712ALess chemical residueResidue reductionMilk preparationBiotechnologyGut immunity
The invention discloses a lentinan soluble bean for improving intestinal immunity of children by diet and a preparation method thereof, and the lentinan soluble bean comprises the following raw materials in parts by weight: 10-40 parts of organic lentinan solution, 5-10 parts of trehalose, 100-120 parts of skim milk powder, 10-20 parts of whey powder, 25-30 parts of cereal starch, 10-50 parts of yolk powder, 1-5 parts of ferment powder, 1-5 parts of composite probiotics, 0.5-1 part of compound vitamin and 5-10 parts of organic honey. According to the invention, organic lentinula edous are adopted for the first time for preparing the yoghourt soluble beans. The organic food is less in chemical substance residue, less in pollution, better in taste, healthier, free of other side effects and suitable for children to eat.
Owner:ZHONGXIANG XINGLI FOOD

Aryl compounds containing phenolic hydroxyl groups as tyrosinase activators and their applications

The invention belongs to the technical field of cosmetics, medicine and food chemistry and discloses a phenolic hydroxyl-containing aryl compound acting as tyrosinase activator and application thereof. The phenolic hydroxyl-containing aryl compound is used as tyrosinase activator, and is from more than one of 1,5-dihydroxynaphthalene and 2,2'-diphenol. The compound related herein has strong tyrosinase activating activity, and has significant application prospect in medicine (such as for treating vitiligo) and cosmetics (such as hair-blacking shampoo).
Owner:GUANGDONG IND TECHN COLLEGE

Method for re-preparing oil from Antarctic krill defatted dried shrimp dregs

The invention belongs to the fields of foods, chemistry and medicine and particularly relates to a method of re-preparing oil from defatted dry residue of Euphausia superba. The method comprises: micronizing dry residue, extracting with a mixed solvent of n-hexane and ethyl alcohol, and subjecting filtrate of extract to rotary evaporation to obtain oil. The oil yield is 4.67-5.9%.
Owner:SHANDONG NORMAL UNIV

Low-sensitization Qianye tofu and preparation method thereof

The invention discloses a low-sensitization Qianye tofu and a preparation method thereof, and the method comprises the following steps: soybean protein isolate and reducing sugar are subjected to a wet glycosylation reaction to obtain glycosylated modified soybean protein isolate; and adding an ice-water mixture, glutamine transaminase, soybean oil and corn starch into the glycosylated modified soybean protein isolate, and processing to prepare the low-sensitization Qianye tofu. The invention belongs to the field of food chemistry, and relates to a preparation method of low-sensitization Qianye tofu with glycosylation modified soybean protein isolate as a main raw material. According to the method, the sensitization of the soybean protein isolate can be reduced by 30-50%, and the Qianye tofu prepared from the glycosylation modified soybean protein isolate has good elasticity and chewiness, and has no obvious difference in elasticity, cohesiveness and chewiness indexes compared with common Qianye tofu.
Owner:CHINA AGRI UNIV

Fluorescence detection test paper and its preparation method and application, identification method of inferior oil

The invention relates to the technical field of food chemistry, in particular to a fluorescent detection test paper, which comprises: a test paper base material and a fluorescent molecular probe combined in the test paper base material; the fluorescent molecular probe is polar Sensitive fluorescent probe capable of identifying trace polar impurities in non-polar solutions. The method for identifying inferior oils and fats provided by the present invention utilizes the fluorescence detection test paper of the present invention to detect changes in the fluorescence spectra of standard oils and fats and samples to be tested. It can detect the quality of grease or identify inferior grease (such as waste oil) within a few seconds. It has the characteristics of high sensitivity, strong specificity, high accuracy, fast detection speed and low cost.
Owner:清水湾生物材料(深圳)有限公司

Method for detecting inositol in food

The invention relates to a method for detecting inositol in food, and belongs to the field of food chemical detection. The method for detecting inositol in food comprises the following steps of: mixing to-be-detected food, water and ethanol to prepare a food detection solution; detecting the food detection solution by using an ultra-high performance liquid chromatography-mass spectrometer to determine whether the food detection solution contains inositol or not; and if the food detection solution contains inositol, taking sorbitol as an internal standard substance, and detecting the food detection solution by adopting an internal standard method so as to determine the content of inositol in the to-be-detected food. The method for detecting inositol in food can be used for efficiently and accurately detecting whether food contains inositol and detecting the content of inositol.
Owner:武汉嘉谷肽业生物科技有限公司

Phenolic acid starch ester as well as preparation method and application thereof

The invention discloses a phenolic acid starch ester as well as a preparation method and application thereof, and belongs to the technical field of food chemistry. The preparation method comprises the following steps: (1) adding starch into water, heating, carrying out pre-gelatinization treatment, and dehydrating and drying to obtain pre-gelatinized starch; (2) mixing phenolic acid, pre-gelatinized starch, lipase, a solid acid catalyst and a water absorbent in an organic solvent, and reacting at 40-80 DEG C in combination with ultrasonic treatment to obtain a phenolic acid starch ester turbid liquid; and (3) carrying out solid-liquid separation on the phenolic acid starch ester turbid liquid to obtain the phenolic acid starch ester. According to the invention, ultrasonic treatment is utilized in the lipase catalytic reaction process to promote dispersion of starch and improve the enzyme activity, and the solid acid catalyst and the water absorbent are combined to synergistically promote the increase of the reaction efficiency. The preparation method is efficient and safe, and starch sources are not limited; the prepared phenolic acid starch ester has good biological activity, and has a good effect on preventing and treating metabolic diseases, especially diabetes and obesity.
Owner:ZHEJIANG UNIV

Method for efficiently preparing Maillard intermediate by utilizing spray drying-vacuum drying

The invention discloses a method for efficiently preparing a Maillard intermediate by utilizing spray drying-vacuum drying and belongs to the technical field of food chemistry. The method comprises the following steps: taking amino acid and reducing sugar as raw materials, and carrying out heating for 20-120 minutes at the temperature of 60 DEG C to 100 DEG C firstly to obtain a primary reaction solution; then, carrying out spray drying on the primary reaction solution to obtain Maillard primary powder; and finally, performing vacuum drying, thereby obtaining Maillard intermediate powder. According to the method, the synergistic effect of high-temperature instantaneous dehydration-vacuum drying and a thermal reaction is utilized, in a process that the content of free water is reduced and the fugacity of water not prone to flowing is improved, directional conversion of beta-elimination dehydration in molecules to bound water is promoted, conversion balance between N-glycosylamine and deoxidized amino sugar moves rightwards, and the purpose of efficiently preparing the deoxidized amino saccharide Maillard reaction intermediate is achieved; and meanwhile, the defects of high pollution, high toxicity and high cost of a traditional organic solvent preparation method are overcome, and the problem of low yield of a water-phase Maillard reaction is also solved.
Owner:JIANGNAN UNIV +1
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