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31results about How to "Play a pore-forming role" patented technology

Alkali-activated high-titanium slag baking-free haycite and preparation method thereof

The invention discloses alkali-activated high-titanium slag baking-free haycite which is characterized by being prepared by mixing 100 weight parts of high-titanium slag micro powder, 12.5 to 30 weight parts of an alkali-activator, 0.5 to 10 weight parts of a pore forming substance and 0 to 10 weight parts of water. A preparation method of the alkali-activated high-titanium slag baking-free haycite comprises the following steps: putting the high-titanium slag micro powder into a disk granulator for stirring, so as to form a uniformly dispersed powder body; adding the pore forming substance, the water and the alkali-activator solution in sequence, and performing stirring, granulation and forming to obtain a blank, wherein the alkali-activator solution is water glass; maintaining the blank under a natural environment condition for 28 days, so as to obtain the alkali-activated high-titanium slag baking-free haycite. By the adoption of the preparation method for preparing the alkali-activated high-titanium slag baking-free haycite, high-temperature baking is not needed; a large mixing amount of the high-titanium slag micro powder can be used, so that a product is light in mass and high in strength; the alkali-activated high-titanium slag baking-free haycite has the characteristics of simple process, low cost, energy conservation, low carbon, environment friendliness and the like.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Batch preparation method for titanium-based air suction element with high porosity

The invention provides a batch preparation method for a titanium-based air suction element with the high porosity. The preparation method comprises the following steps that under the condition of argon protection, titanium powder and a mixture of molybdenum powder, zirconium ferrovanadium powder, zirconium aluminum powder and zirconium nickel powder are evenly mixed, and a titanium-based raw material is obtained; under inert gas protection, the titanium-based raw material and ammonium bicarbonate are evenly mixed, an organic binder bond is added, and an injecting feedstock is formed; the feedstock is deposited on modified metal wires, subjected to forming through isostatic cool pressing and taken out after pressure relief and demoulding, and a blank is formed; under a vacuum state, the blank is stored in trichloro ethylene to be subjected to chemical degreasing treatment and then taken out for cooling, and a chemical degreasing blank is obtained; and the chemical degreasing blank is subjected to high-temperature sintering in a vacuum sintering furnace, cooled and taken out of the vacuum sintering furnace, and then the high-porosity titanium-based air suction element with the porosity being higher than 50% is obtained. According to the titanium-based air suction element with the high porosity, a preparation technique is simple and easy to operate, and the air suction element is high in porosity, good in manipulative performance and excellent in air suction performance.
Owner:DONGGUAN JIAQIAN NEW MATERIAL TECH CO LTD

Preparation method of graphite-phase carbon nitride with large specific surface area

The invention belongs to the field of visible light catalytic materials, and particularly relates to a method for preparing a large-specific-surface-area graphite-phase carbon nitride material by utilizing a low-melting-point precursor and carrying out low-temperature heat treatment on the precursor in a roasting process. The preparation method comprises the following steps: (1) putting a nitrogen-containing precursor into a three-necked flask, putting the three-necked flask filled with the nitrogen-containing precursor into an oil bath pot after the temperature of the oil bath pot reaches themelting point of the nitrogen-containing precursor, and heating and stirring to enable the nitrogen-containing precursor to be in a molten state; (2) heating to keep a molten state, taking out the three-neck flask, and cooling and crystallizing the nitrogen-containing precursor at the molten state at room temperature; and (3) grinding the crystallized nitrogen-containing precursor into powder, putting the powder into a crucible, putting the crucible into a muffle furnace, carrying out programmed heating, and roasting in an air atmosphere to obtain a target product. The method has the advantages of simple process, environmental protection, low cost, high purity of the target product, and high catalytic performance.
Owner:LIAONING UNIVERSITY OF PETROLEUM AND CHEMICAL TECHNOLOGY

Method for preparing wear-resisting large-pore-volume micro-spherical silicon dioxide carrier

The invention provides a method for preparing a wear-resisting large-pore-volume micro-spherical silicon dioxide carrier. The method comprises the steps that precipitation method silicon dioxide powder or white carbon black with the specific surface area of 250-600 m<2>/g is calcined at the temperature of 730 DEG C to 760 DEG C, the specific surface area of the precipitation method silicon dioxide powder or white carbon black is reduced to 100-220 m<2>/g, and water is added for even mixing; grinding and dispersing are carried out till the average diameter of microparticles ranges from 2 micrometers to 5 micrometers, activated carbon emulsion and a white carbon black emulsus glue solution are added for even mixing, and spray granulation is carried out; pelleted powder is calcined at the temperature of 650 DEG C to 720 DEG C, the micro-spherical silicon dioxide carrier with the average diameter of 50-250 micrometers is prepared, the specific surface area ranges from 60 m<2>/g to 120 m<2>/g, the pore volume ranges from 0.7 ml/g to 1.1 ml/g, and the average pore diameter ranges from 35 nm to 50 nm. High mechanical strength, wear resistance and impact resistance are achieved, and the carrier is suitable for further loading active components and preparing a catalyst for a fluidized bed.
Owner:钟俊超

A kind of flue gas desulfurizer and its preparation method and application

The invention provides a flue gas desulfurizing agent as well as a preparation method and application thereof. The flue gas desulfurizing agent comprises the following raw materials in parts by weight: 30-60 parts of slaked lime powder, 20-60 parts of silica fume, 6-24 parts of a binder and 6-15 parts of crystalline hydrated salt. According to the flue gas desulfurizing agent, active substances inthe slaked lime powder and the silica fume are subjected to a pozzolanic reaction to generate high-strength hydrated silicate; the binder can bind all the raw material components to improve the strength of the flue gas desulfurizing agent; the crystalline hydrated salt plays a pore-forming role by losing crystalline water in the flue gas desulfurizing agent; mutual cooperation of components, theflue gas desulfurizing agent has relatively small stacking density (0.5-0.8 g / cm<3>), relatively high radial crushing strength (120-280 N / cm) and relatively large porosity (40-65%); the desulfurizingagent can be used for a fixed bed reactor or a moving bed reactor, is suitable for purification treatment of SO2-containing industrial flue gas or waste gas at 20-330 DEG C, has relatively high reaction activity, particularly still has relatively high crushing resistance under a relatively high flue gas temperature condition, and is not easy to pulverize and low in bed pressure.
Owner:北京予知环境工程有限公司

Alkali-activated high-titanium slag unfired ceramsite and preparation method thereof

The invention discloses alkali-activated high-titanium slag baking-free haycite which is characterized by being prepared by mixing 100 weight parts of high-titanium slag micro powder, 12.5 to 30 weight parts of an alkali-activator, 0.5 to 10 weight parts of a pore forming substance and 0 to 10 weight parts of water. A preparation method of the alkali-activated high-titanium slag baking-free haycite comprises the following steps: putting the high-titanium slag micro powder into a disk granulator for stirring, so as to form a uniformly dispersed powder body; adding the pore forming substance, the water and the alkali-activator solution in sequence, and performing stirring, granulation and forming to obtain a blank, wherein the alkali-activator solution is water glass; maintaining the blank under a natural environment condition for 28 days, so as to obtain the alkali-activated high-titanium slag baking-free haycite. By the adoption of the preparation method for preparing the alkali-activated high-titanium slag baking-free haycite, high-temperature baking is not needed; a large mixing amount of the high-titanium slag micro powder can be used, so that a product is light in mass and high in strength; the alkali-activated high-titanium slag baking-free haycite has the characteristics of simple process, low cost, energy conservation, low carbon, environment friendliness and the like.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Regeneration method of hydrogenation catalyst

The invention provides a regeneration method of a hydrogenation catalyst. The method comprises the following steps: (1) immersing an inactivated hydrogenation catalyst A in a solvent, carrying out ultrasonic treatment to obtain a catalyst B and a mixed material mixed with black powder, recovering the catalyst B, and filtering the mixed material mixed with the black powder to obtain powder C; (2) grinding the catalyst B into powder, and screening to obtain catalyst powder D; (3) forming, drying and roasting the catalyst powder D to obtain a regenerated carrier; and (4) dissolving the powder C obtained in the step (1) in diesel oil, dipping on a regenerated carrier, and drying to obtain the regenerated hydrogenation catalyst. According to the method disclosed by the invention, additional supplement of active metal components is not needed, interaction between the carrier and metal molybdenum is basically eliminated in the preparation process of the catalyst, and uniform dispersion of molybdenum sulfide can also be realized, so that the obtained regenerated hydrogenation catalyst has relatively good physicochemical properties and activity. And the use amount of the vulcanizing agent can be reduced and the vulcanizing time can be shortened at the start-up stage of the industrial device.
Owner:CHINA PETROLEUM & CHEM CORP +1
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