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94results about How to "Well sourced" patented technology

Preparation method of silicon-carbon negative electrode material for high-compaction-density lithium ion battery

The invention discloses a preparation method of a silicon-carbon negative electrode material for a high-compaction-density lithium ion battery. The preparation method comprises the following steps: (1) preparing nano-sized silicon powder; (2) preparing micron-sized porous natural graphite; (3) mixing the prepared nano-sized silicon powder with the porous natural graphite by ball milling; (4) adding a solution in which a carbon source precursor is dispersed into a mixture of the nano-sized silicon powder and the natural graphite for secondary ball milling; (5) coating and carbonizing integrateddevice with a graphite negative electrode material under inert gas protection for granulation and high-temperature carbonization to obtain a silicon-carbon materials with appropriate particle size; and (6) blending the prepared silicon-carbon material with commercial graphite to form a silicon-carbon negative electrode material. The preparation method not only guarantees the first coulomb efficiency and cycle performance of the silicon-carbon negative electrode material, but also significantly improves the compaction density, thereby laying a foundation for further preparation of a high-energy-density battery. In addition, the preparation process is fast and convenient; raw materials are easy to obtain; and large-scale production and application of the silicon-carbon negative electrode material are facilitated.
Owner:赣州市瑞富特科技有限公司

Preparation technology of novel nerve conduit

The invention discloses a preparation technology of a novel nerve conduit, and belongs to the technical field of tents of biological tissue engineering. The preparation technology sequentially comprises a preparation technology of GDNF (glial-derived neurotrophic factor)-carried gelatin microspheres, a synthesizing technology of gelatin-methacrylamide hydrogel, a preparation method of polycaprolactone/gelatin electricity texture nerve conduits, and a combining method of the electricity texture nerve conduits and the GDNF-carried gelatin microspheres. The preparation technology has the advantages that a tent structure with good degradability, biological compatibility and biological safety is realized, and the GDNF is controlled and released by the GDNF-carried gelatin microspheres; compared with blank groups and collagen conduit groups, the regeneration of peripheral nerves is effectively promoted, and the structure and function of restoring damaged nerves can reach the effect similar to the effect of autotransplantation groups; the defect nerves can be bridged, and the stability of axon regeneration environment can be maintained; the invasion of peripheral connective tissues is prevented; the saturing of near and far-heart breaking ends of smaller nerve defect is solved, and the restoration of larger nerve defect is solved.
Owner:JIANGSU PROVINCE HOSPITAL

Method for preparing porous graphene-like material from water hyacinth

The invention relates to a method for preparing a porous graphene-like material from water hyacinth. The method comprises the following steps: washing water hyacinth, drying, carrying out acid boiling on dried water hyacinth in diluted HCl, carrying out pumping filtration, and carrying out vacuum drying; heating in N2 atmosphere to 300-900DEG C, and pre-carbonizing; mixing a pre-carbonized carbonization product with KOH, heating in N2 atmosphere to 400-1000DEG C, annealing for 1-10h, and cooling to room temperature; and cleaning the obtained sample by the diluted HCl, cleaning with distilled water until the sample is neutral, and drying at 80DEG C to prepare the porous graphene material. Living creature harmful to nature is used as a raw material, is changed to valuables, and is in favor of protecting environment; simple acid boiling and annealing treatment are adopted, and the thickness and the size of acid-boiled graphene flakes are controlled by controlling the acid boiling time and the annealing temperature and rate; and the method has the advantages of full source of the raw material, simplicity, reliability, low cost, and suitableness for large scale production. The graphene-like material obtained in the invention is suitable for fields of electrochemistry, electronic devices and environment.
Owner:江苏润美新材料有限公司

Method for preparing highly corrosion-resistant sintered NdFeB magnet

The invention provides a method for preparing a highly corrosion-resistant sintered NdFeB magnet. The method comprises the following steps: performing orientation pressing on sintered NdFeB magnetic powder in a 1.5-2.0T oriented magnetic field under the pressure of 16MPa, performing cold press molding on a pressed shape in an oil-cooled isostatic pressing machine so as to obtain a green body; performing low-temperature vacuum pre-sintering on the green body in a vacuum sintering furnace at the temperature of 850-890 DEG C for 3-3.5 hours so as to obtain a magnet; taking the magnet as a substrate, and covering a non-rare-earth compound layer on the surface of the substrate by adopting a magnetron sputtering method; performing high-temperature sintering in the vacuum sintering furnace for 2-3 hours, performing secondary tempering treatment, filling inert gases of 20-22MPa for applying pressure in the temperature treatment process, thereby obtaining the highly corrosion-resistant sintered NdFeB magnet. According to the magnetron sputtering manner, a diffusion source is attached to the surface of the magnet, grain boundary diffusion is completed in the sintering process, the base bonding force is improved, and the diffusion depth and corrosion resistance are improved.
Owner:EARTH PANDA ADVANCE MAGNETIC MATERIAL

Comprehensive utilization method of hydrargillite-produced 4A zeolite waste residue

The invention provides a comprehensive utilization method of hydrargillite-produced 4A zeolite waste residue. The method comprises the steps of: separating the ferrosilicoaluminum component in the hydrargillite-produced 4A zeolite waste residue by means of acid leaching and filtering, wherein the obtained mixed liquor of filter liquor and filter residue washing liquor is used for preparing a polymeric aluminum ferric chloride water purifying agent; and removing iron from the wet slag obtained by washing the filter residue by means of alkali fusing, roasting and activating, and synthesizing the 4A zeolite by a hydrothermal method by means of adjusting and assembling. Triethanolamine is taken as a complexing agent of the microelement iron in the liquor during synthesizing the 4A zeolite, so that the produce of an iron precipitate is overcome, and the whiteness of a 4A zeolite product is guaranteed; sodium sulfide is reacted with a triethanolamine iron complex in the zeolite-synthesized mother liquor to reduce the triethanolamine and obtain an iron sulfide precipitate; and removing the mother liquor of the iron sulfide precipitate to realize the cycle utilization. The synthesis method of the 4A zeolite adopts a sealed cycle technology, thereby being stable in operation, and free of the generation of new waste liquor and new waste slag.
Owner:HEBEI UNIV OF TECH

Process for preparation potassium salt for plant ash

The invention relates to a method for preparing sylvite from plant ash, which is characterized in that the plant ash is put into a vessel, water with the weight which is more than twice of the weight of the plant ash is added into the vessel for carrying out fully stirring for 10 minutes to 20 minutes, potassium hydroxide with the weight which is 0.2 percent to 5 percent of the total weight of the plant ash and the water is added for carrying out fully stirring for 10 minutes to 20 minutes, the PH value of the plant ash solution is adjusted to 10 to 14 for sedimentation to remove other impurities, and colorless, transparent and pure solution is obtained after fine filtration; the solution filtered is put into a reaction kettle, 2 percent to 5 percent of selected acid in which the content of the plant ash and the water is 10 percent to 50 percent of the total weight is added according to preparation requirements and the measure value of the potassium ion in the plant ash for carrying out fully stirring for 10 minutes to 20 minutes, and the PH value is adjusted to 4 to 5; heating is carried out for vaporizing the water in the solution, a centrifuge is used for dehydration till the water content is less than 5 percent, and then product obtained is crashed into 50-mesh to 200-mesh fine powder and the sylvite is obtained. The plant ash used as the raw material in the invention is economic and environment-friendly, thereby having great benefit and grand development prospect.
Owner:王玉新

Satellite roof refined thermal design device

InactiveCN108528760AReduce the impactReduce temperature gradients and fluctuationsCosmonautic partsArtificial satellitesThermal insulationSatellite
The invention discloses a satellite roof refined thermal design device which comprises a satellite roof, a multilayer structure, a thermal insulation gasket and screws, wherein the multilayer structure comprises a satellite interior multilayer thermal insulation assembly and a satellite exterior multilayer thermal insulation assembly; the satellite interior multilayer thermal insulation assembly is coated on the lower side of the satellite roof and arranged towards the satellite interior side; the satellite exterior multilayer thermal insulation assembly is coated on the upper side of the satellite roof and arranged towards the satellite exterior side; a load is connected onto the satellite roof by virtue of screws; the thermal insulation gasket is positioned between the load and the satellite roof. According to the satellite roof refined thermal design device disclosed by the invention, the influences of space environment and internal external heat flux on the roof can be greatly reduced, the temperature gradient and fluctuation of the roof can be reduced, and different temperature requirements of the roof on a transition section and during an in-orbit period can be met; due to athermal insulation design of the roof and the load, heat leakage of the load can be effectively reduced, and the temperature gradient and fluctuation of the roof can be reduced; the thermal design method is reasonable and feasible, full in material source, high in reliability, simple in process operation, easy to realize and low in cost.
Owner:SHANGHAI SATELLITE ENG INST

Method for preparing iron oxide red pigment by utilizing titanium white waste acid

The invention relates to a method for preparing iron oxide red pigment by utilizing titanium white waste acid, which belongs to the technical field of pigment powder. The method comprises the following steps: firstly locally neutralizing waste acid by utilizing ammonium, adjusting the pH of the waste acid, hydrolyzing and precipitating metal impurities such as titanium, aluminum vanadium and chromium in the waste acid in a sulfate form, allowing ferrous to remain in a liquid phase, oxidizing the ferrous into ferric iron by virtue of the combined effect of the chlorine gas and hydrogen peroxide with high reduction performance, obtaining a pretreatment solution, then performing enzymolysis on an acid-containing fruit, mixing an enzymatic solution rich in organic carboxylic acid and the pretreatment solution, extracting a chelated-state ferric iron by virtue of an extracting agent, mixing microorganisms and an extraction phase, fermenting, degrading organic carboxylic acid by utilizing microorganisms, enabling the ferric iron to be exposed again, then precipitating the ferric iron by utilizing the sodium hydroxide, obtaining ferric hydroxide precipitates, and sintering at a high temperature, thus obtaining the iron oxide red pigments. According to the method, the waste acid is used as a raw material, so that the source is sufficient, the cost is low, the entire process flow is simple and easy in operation, and the application prospect is wide.
Owner:YIWU WADOU PICTURE

Processing technique for efficiently removing ocean oil spill

The invention discloses a processing technique for efficiently removing ocean oil spill. The technical solution of the invention is as follows: the processing technique for efficiently removing the ocean oil spill comprises the following steps of: (1) air-drying and screening sediments of the muddy sand beach taken from the entrance of the Dagu River to obtain particulate matters with particle size of not more than 35.5 mu m; (2) sorting to obtain the separated particulate matters with particle size of 6-10 mu m; (3) mixing the right amount of particulate matters with sea water, preparing a particle solution of 200-1000 mg/L, and filling the solution in a can to store; and (4) according to the oil spill quantity in the sea water, selecting the particle solution with proper concentration, spraying the particle solution on the surface layer of the oil spill, and stirring the solution through a propeller of a cleaning vessel until the oil spill is fully removed. The processing technique for efficiently removing the ocean oil spill has the following beneficial effects that: (1) by adopting the particulate matters made of natural sediments, the ocean oil spill is removed, toxicity and pollution are free, and interference to the original ecological system after using is less; (2) the processing technique has very high removing efficiency on the oil spill with low concentration; and (3) as the particulate matters have sufficient sources, the particulate matters need not be recycled after using, and further, the cost is low.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)
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