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92results about How to "Avoid washing" patented technology

Method for producing reforming feedstock by light and medium gasoline distillates

The invention relates to a method for producing catalytic reformed feedstock by taking light and medium gasoline distillates as raw materials and extracting selective solvent to extract and rectify catalytically cracked gasoline in the absence of hydrogen. The method comprises the following steps: 1, fractionation prefabrication of light and medium distillate raw materials of catalytically cracked gasoline; and 2, extraction, rectification, desulfuration and dearomatization of light and medium distillates of catalytically cracked gasoline, wherein light and medium distillates of catalyticallycracked gasoline obtained in step 1 are fed into the middle-lower part of an extraction-rectification tower, while fresh extraction agent or recycled extraction agent is added from the upper part of the extraction-rectification tower; thus, the light and medium distillates contact the extraction agent inside the tower to generate desulfurized and dearomatized light-component raffinate phase (i.e.catalytic reformed feedstock product) rich in olefin hydrocarbon at the top of the tower after extraction, rectification, desulfuration and dearomatization. The method carries out desulfuration and dearomatization of catalytically cracked gasoline at the same time and reclaims solvent, thereby having the advantages of simple process, moderate operation conditions, hydrogen source saving and low production cost.
Owner:PETROCHINA CO LTD +1

Copper foil anti-oxidation treating fluid, preparation method of copper foil anti-oxidation treating fluid and copper foil anti-oxidation treating equipment

The invention discloses a copper foil anti-oxidation treating fluid, a preparation method of the copper foil anti-oxidation treating fluid and copper foil anti-oxidation treating equipment. The copper foil anti-oxidation treating fluid comprises the following raw material ingredients by weight: 0.05-0.1 g / L hydroxybenzotrizole (HBTA), 0.02-0.05 g / L 2-mercaptobenzothiazole (MBT), 0.1-0.5 g / L of silver nitrate, 0.1-0.5 g / L sodium molybdate, 0.05-0.1 g / L phosphoric acid, 0.5-3 g / L boric acid and the balance of pure water. The copper foil anti-oxidation treating fluid can prevent water washing, reduces the water treatment cost, does not contain such harmful substances to the environment as hexavalent chromium, and meets the demand for environmental protection; an anti-oxidation and anti-passivation film is stable under the high-temperature condition and does not contain zinc metal; and such unstable problems as resistance reduction of a copper foil are solved. A liquid inlet of an anti-oxidation treatment groove of the copper foil anti-oxidation treating equipment is positioned above one end of the feeding side of a copper foil roller, so that two surfaces of the copper foil can be subjected to full anti-oxidation treatment.
Owner:佛冈建滔实业有限公司

Sc2O3-stabilized ZrO2-based electrolyte powder and preparation method thereof, and Sc2O3-stabilized ZrO2 electrolyte ceramic wafer prepared from powder

The invention discloses Sc2O3-stabilized ZrO2-based electrolyte powder and a preparation method thereof, and a Sc2O3-stabilized ZrO2 electrolyte ceramic wafer prepared from the powder. The Sc2O3-stabilized ZrO2-based electrolyte powder is characterized in that zirconyl nitrate, Sc2O3, optional CeO2, nitric acid, and optional auxiliary materials are used as the raw materials, an ammonium bicarbonate-ammonia buffer system is used as a precipitant, and the coprecipitation, mist spray and heat treating method is carried out to prepare the powder of which a bulk phase is a cubic phase. Such Sc2O3-stabilized ZrO2-based electrolyte powder has the advantage that the raw materials are low in price and nontoxic; the Sc2O3-stabilized ZrO2-based electrolyte powder can be prepared into a high-strength dense electrolyte ceramic wafer which has relatively high ionic conductivity stability and the like. Simultaneously, according to the preparation method of the Sc2O3-stabilized ZrO2-based electrolyte powder, follow-up complex processes such as filtering, washing and drying in the coprecipitation method are avoided, the agglomeration is reduced, the product purity is ensured, the process is simple, the process is continuous and efficient in process, and large industrial production is facilitated.
Owner:HUNAN RARE EARTH METAL MATERIAL RES INST

Special coating process of cargo tank of product tanker/chemical tanker

InactiveCN102476094AThe construction process is scientific and reasonableShorten special coating cyclePretreated surfacesCoatingsSocial benefitsSurface cleaning
The invention discloses a special coating process of a cargo tank of a product tanker/chemical tanker. The process adopts an integral method instead of an upper and lower part method and has the effects of meeting the construction requirement of the special coating, shorting the special coating period, improving the special coating efficiency, lowering the special coating cost and ensuring smooth special coating construction. The process specifically comprises the concrete steps of protection of fittings and piping systems in a cabin, scaffold setting up in the whole cabin, advance sand blasting in the whole cabin, main sand blasting in the whole cabin, dust absorption and surface treatment inspection in the whole cabin, first coating of the whole cabin, cabin bottom protection, upper part painting, upper part film painting and repairing, upper part film painting inspection, scaffold dismantling, lower part protection removal, treatment of the support point of the lower scaffold; lower surface cleaning and inspection; and lower part painting, lower part film painting and repairing and lower part film painting inspection. The process has multiple considerable effects such as high efficiency, low cost, energy conservation and the like and has the effects of not only ensuring smooth completion of special coating of the 110,000-ton large product tanker but also creating considerable economic and social benefits.
Owner:DALIAN SHIPBUILDING IND

Preparation method of yttrium oxide stabilized zirconium oxide powder based on supercritical dispersion roasting

The invention discloses a preparation method of yttrium oxide stabilized zirconium oxide powder based on supercritical dispersion roasting. The method comprises the following steps: first, weighing zirconium salt and yttrium salt, mixing the zirconium salt with the yttrium salt to prepare a precursor material of the yttrium oxide stabilized zirconium oxide powder, and drying the precursor material; mixing the dried precursor material with a grinding auxiliary agent and a dispersing agent, grinding the mixture into the d10 being less than 100 nm and d50 being greater than 150 nm in a nano-sandmill; continuously conveying the ground slurry into a high-pressure kettle with the temperature being greater than 250 DEG C and the pressure being greater than 6.5 MPa through a metering pump, and spraying the slurry into a calcining furnace for combustion from an outlet, wherein the precursor is dispersed by the grinding auxiliary agent and the dispersing agent which are in a supercritical stateand is decomposed into the yttrium oxide stabilized zirconium oxide powder in the calcining furnace. The yttrium oxide stabilized zirconium oxide powder prepared with the method has small particle size, uniform particle size and nearly spherical morphology, and can meet the requirement of high-end application.
Owner:SHENZHEN ZHONGJIN LINGNAN NONFEMET COMPANY +2

Energy-converting photocatalysis nanophase material and preparation method thereof

The invention discloses an energy-converting photocatalysis nano material and a preparation method thereof. Firstly, 0.02-3.5 mol.L<-1> titanium tetrachloride is used as the raw material, and one or two oxides of the rare earth elements of Yb, Er, Ho and Tm are mixed with the titanium tetrachloride. The mixed rare earth oxides account for 0.01-20 percent of the total weight. The mixed solution is subject to hydrolysis for 20-480 minutes at a temperature of 20-90 DEG C. Then, the mixed solution is extracted by means of an organic extraction method with organic amine so as to remove the Cl<-> in the solution and obtain anatase type nanometer titanium dioxide gel containing rare earth elements, and the titanium dioxide gel is aged for 2-48 hours. Finally, the titanium dioxide gel undergoes hydrothermal crystallization at a temperature of 120-240 DEG C so as to obtain the nano energy-converting photocatalysis material. In the invention, through energy conversion, part of the visible light, which is absorbed by the anatase type titanium dioxide, is converted into ultraviolet energy to be absorbed, without reducing forbidden gap, thereby improving the utilization rate of the visible light by a titanium dioxide photocatalyst, being capable of realizing the industrialization production of titanium tetrachloride hydrolysis and avoiding particle aggregation possibly generated by high-temperature calcining.
Owner:JIANGSU POLYTECHNIC UNIVERSITY

Preparation method for lithium-enriched manganese-based cathode material

The invention discloses a preparation method for a lithium-enriched manganese-based cathode material, belonging to the field of cathode materials for lithium ion batteries. The method comprises the following steps: preparing a water solution of a mixture of a lithium salt, a nickel salt, a manganese salt and an M salt according to a stoichiometric ratio of a chemical formula Li1.5Ni<0.25-x>Mn<0.75-x>M<2x>O2.5 (x is more than or equal to 0.003 and less than or equal to 0.02 and M is cobalt or chromium); adding a pre-set amount of urea to obtain a mixed solution; enabling the mixed solution to react in a sealed container at 70-90 DEG C under an agitating condition to obtain a reaction system containing first sediment; dropwise adding (NH4)2CO3 water solution into the system and reacting to obtain a reaction system containing second sediment; carrying out evaporation treatment on the reaction system containing the second sediment at 75-85 DEG C to remove water in the system to obtain a precursor containing Li, Ni, Mn and M; and carrying out two times of sintering treatment on the grinded precursor to obtain the lithium-enriched manganese-based cathode material. The method does not need to use clean water to wash so that wastewater is not generated and the loss of Li, Ni, Mn and other metal ions is avoided.
Owner:CHERY AUTOMOBILE CO LTD

Method for reducing harmful materials in by-product hydrochloric acid in production process of chlorobenzene

The invention provides a method for reducing harmful materials in by-product hydrochloric acid in a production process of chlorobenzene. The method comprises the following steps: compressing normal-temperature hydrogen chloride gas separated by a chlorobenzene system to 0.08-0.12MPa through a Roots blower, condensing the hydrogen chloride gas through a primary condenser, condensing water and low-boiling-point materials, separating the hydrogen chloride gas through a gas-liquid separator, then continuously compressing the hydrogen chloride gas to 1-1.5MPa through a compressor, condensing the hydrogen chloride gas through a secondary condenser for further removing organic impurities, filling the hydrogen chloride gas into an adsorption tower from the bottom of the adsorption tower with adsorbent, removing other impurities to obtain qualified hydrogen chloride gas, absorbing the qualified hydrogen chloride gas through water and then obtaining industrial pure hydrochloric acid. The purityof hydrogen chloride obtained by the method is high; the quality of the by-product hydrochloric acid is high; the wastewater is not generated; the enterprise income is increased; meanwhile, the methodis simple in process and easy to operate; the benzene-series organic matters recycled from the by-product hydrochloric acid enter a benzene recycling tank and return to the chlorination process for recycling, so that the material loss is reduced, and the production cost is reduced.
Owner:ANHUI DONGZHI GUANGXIN AGROCHEMICAL CO LTD

Novel chlorobenzene production process

The invention provides a novel chlorobenzene production process. Chlorobenzene used in the novel chlorobenzene production process comprises the following raw materials: anhydrous benzene, chlorine, acatalyst and a positioning agent. The novel production process comprises the following steps: preparing the anhydrous benzene; enabling the anhydrous benzene to flow out from the bottom of a benzene high-level tank, metering by using a flowmeter, and continuously putting into a chlorinator from the bottom of the chlorinator; buffering qualified chlorine made after gasification of liquid chlorine by using a chlorine buffer tank, introducing into the chlorinator from the bottom of the chlorinator to flow upwards together with the anhydrous benzene along flows in a same direction, carrying out areaction under the action of the catalyst and the positioning agent in the chlorinator so as to generate a chlorination liquid, and carrying out aftertreatment on the chlorination liquid, thereby obtaining chlorobenzene. By adopting the novel production process provided by the invention, the problem that a great deal of wastewater is generated from water washing and alkali washing in the conventional method can be avoided, no wastewater is generated, in addition, the catalyst is long in service life, the equipment is long in service life, the detection cycle can be prolonged, a product made byusing the process is high in purity, and due to adoption of an iron catalyst and chelate EDTA-Fe with iron as the center as the positioning agent, the process is low in wastewater generation rate andgreen, environmentally friendly and fee of pollution.
Owner:ANHUI DONGZHI GUANGXIN AGROCHEMICAL CO LTD
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