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36results about How to "Reduce pickling process" patented technology

Copper bus bar with high strength, high conductivity and high toughness and preparation method thereof

The invention relates to a copper bus bar with high strength, high conductivity and high toughness and a preparation method thereof. The copper bus bar is characterized in that the material comprises 99.96-99.998% of copper and silver, 0.002-0.02% of yttrium rare earth and 0-0.038% of impurities, wherein silver accounts for 0.0005-0.01% of copper and silver; and the copper master alloy containing the yttrium rare earth is used as a modifier. The preparation method comprises the following steps: (1) melting a copper material: heating the cathode copper in a mains frequency core induction furnace to melt the cathode copper into liquid cathode copper; (2) modifying liquid copper: melting the modifier in the liquid cathode copper and fully mixing the modifier with the liquid cathode copper; (3) drawing a continuously cast copper bar upwards: causing a crystallizer of a continuous casting machine to stretch into the liquid cathode copper, condensing the liquid cathode copper into the copper bar in the crystallizer and drawing the copper bar upwards by means of two pairs of drawing roll mechanisms in the continuous casting machine to lead the copper bar to a take-up machine via a wheel frame; (4) continuously extruding the copper bar at medium temperature and carrying out anti-oxidation cooling; and (5) carrying out draw forming: putting copper bus bar blanks on a drawing machine, carrying out draw forming on the copper bus bar blanks.
Owner:福州市广福有色金属制品有限公司

Method for removing impurities from waste battery leachate

The invention relates to a method for removing impurities from waste battery leachate. The method comprises the following steps that iron powder is added, and filtering is carried out after stirring so as to obtain a copper-removed solution; an oxidant is added to obtain a ferrous-removed solution; a small amount of the ferrous-removed solution is taken and diluted to serve as a base solution, theferrous-removed solution and a pH regulator are added, the pH regulator is continuously added after the ferrous-removed solution is completely added, and filtering is carried out after stirring so asto obtain an iron-aluminum-removed solution and iron-aluminum slag; fluoride is added into the iron-aluminum-removed solution, and filtering is carried out after stirring so as to obtain a calcium-magnesium-removed solution; the obtained iron-aluminum slag is added, and filtering is carried out after stirring so as to obtain fluorine-silicon-removed solution and fluorine-silicon-removed iron-aluminum slag; and manganese powder is added into the fluorine-silicon-removed solution, and filtering is carried out after stirring so as to obtain a purified solution. According to the method, the ironpowder is used for replacing and removing copper, and the cost is low; iron and aluminum are removed through a goethite method, and the slag filtering performance is good; fluorine and silicon are removed from the iron-aluminum slag, so that the waste slag is effectively utilized, and the iron-aluminum slag pickling process is reduced; and the copper is deeply removed through the manganese powder,the environment is protected, and the operation is easy.
Owner:HUNAN BRUNP RECYCLING TECH +2

Preparation method of titanium and titanium alloy large-specification seamless pipe

The invention provides a preparation method of a titanium and titanium alloy large-specification seamless pipe. According to the preparation method, an electromagnetic casting hollow pipe blank is adopted, a two-roller or three-roller skew rolling process is adopted to conduct cogging on the pipe blank for 2-3 passes, then warm rolling-cold rolling-cold stretching or warm rolling-cold stretching or warm rolling-expanding stretching is conducted, and the stretched pipe is subjected to inspection, fixed-length sawing, surface cleaning and finished product annealing and then is packaged and put in storage. By means of the preparation method, the problems of uneven wall thickness, unstable quality, unsuccessful perforation and the like of a pierced billet in the traditional skew rolling-perforation process are avoided; the process link of repeatedly heating and repeatedly rolling a cast ingot in the traditional process is omitted, so that the heating time is shortened, and oxidation of the pipe blank which sucks air after heating is relieved; annealing and pickling procedures and pickling metal loss are reduced; and large-specification seamless pipes with the diameter ranging from 80mm to 424mm and the wall thickness ranging from 2mm to 30mm can be produced to meet market requirements.
Owner:XINJIANG UNIVERSITY

Acid washing-free direct hot galvanizing method of hot-rolled strip steel

The invention relates to an acid washing-free direct hot galvanizing method of hot-rolled strip steel, and belongs to the technical field of metallurgy; mainly aiming at the problems of weak hot galvanizing effect and low oxide scale reduction efficiency in a traditional galvanizing technology, the invention provides a method for improving a hot-rolled strip steel oxide scale reduction ratio; the oxide scale thickness and structure of the hot-rolled strip steel are adjusted in the hot rolling process: the hot-rolled strip steel is straightened in a straightener after being wound; after the surface of the strip is suffered from the bending stress, the strip is repeatedly bent and stretched; the huge difference of iron basal body and oxide scale covering layer material performances is used; the iron basal body is stressed to generate a certain plastic deformation; because of weaker plasticity and low breaking strength, a surface oxide scale layer cannot adapt to the deformation of the iron basal body to cause the internal stress to be higher than the breaking strength so as to finally generate different forms of scale cracks or stripping; the heating reduction is performed in a hydrogen atmosphere to improve the reduction efficiency; and then, the hot galvanizing is performed to obtain a more excellent acid washing-free reduction hot galvanizing effect.
Owner:武汉钢铁有限公司

Copper bus bar with high strength, high conductivity and high toughness and preparation method thereof

The invention relates to a copper bus bar with high strength, high conductivity and high toughness and a preparation method thereof. The copper bus bar is characterized in that the material comprises 99.96-99.998% of copper and silver, 0.002-0.02% of yttrium rare earth and 0-0.038% of impurities, wherein silver accounts for 0.0005-0.01% of copper and silver; and the copper master alloy containingthe yttrium rare earth is used as a modifier. The preparation method comprises the following steps: (1) melting a copper material: heating the cathode copper in a mains frequency core induction furnace to melt the cathode copper into liquid cathode copper; (2) modifying liquid copper: melting the modifier in the liquid cathode copper and fully mixing the modifier with the liquid cathode copper; (3) drawing a continuously cast copper bar upwards: causing a crystallizer of a continuous casting machine to stretch into the liquid cathode copper, condensing the liquid cathode copper into the copper bar in the crystallizer and drawing the copper bar upwards by means of two pairs of drawing roll mechanisms in the continuous casting machine to lead the copper bar to a take-up machine via a wheel frame; (4) continuously extruding the copper bar at medium temperature and carrying out anti-oxidation cooling; and (5) carrying out draw forming: putting copper bus bar blanks on a drawing machine, carrying out draw forming on the copper bus bar blanks.
Owner:福州市广福有色金属制品有限公司

Preparation method of small and medium-sized titanium and titanium alloy thin-wall pipes

The invention discloses a preparation method of small and medium-sized titanium and titanium alloy thin-wall pipes. According to the preparation method, industrial pure titanium is cast by adopting an electron beam cold bed melting-vacuum consumable arc melting process, a TA7 alloy is refined by adopting vacuum induction melting-plasma, impurities in the alloy are removed through melting, dissolving, flotation and sedimentation for removing inclusions in the alloy, the burning loss of low-melting-point alloy elements such as aluminum and tin is reduced, and harmful gas impurities in the alloy are removed. Segmented heating and forging cogging are adopted, and air suction pollution of cast ingots is reduced. The hot rolling-warm rolling-cold rolling process is adopted, so that the plasticity of the alloy can be utilized to the maximum extent, annealing and pickling procedures are reduced, and metal oxidation and pickling metal loss are reduced. The thin-wall pipes with the diameter ranging from phi 6.3 mm to phi 7.26 mm and the wall thickness ranging from 0.10 mm to 0.8 mm are welded through rolled strips to replace seamless pipes, and the method has the advantages of high raw material utilization rate, high production efficiency and good economic benefit.
Owner:XINJIANG UNIVERSITY

Flushing system and method for lubricating oil system of steam turbine generator unit

The invention discloses a flushing system and method for a lubricating oil system of a steam turbine generator unit. The method includes the first step of connecting a bearing pedestal with an oil inlet and return pipe according to the design state, the second step of removing a bearing oil inlet pipe inside the bearing pedestal, the third step of starting a first oil filtering machine and cleaning a main oil tank and the bearing pedestal, the fourth step of shutting down the first oil filtering machine, pouring all lubricating oil of the main oil tank into an oil storage tank through a second oil filtering machine, and cleaning the main oil tank and the bearing pedestal, and the fifth step of pouring the lubricating oil in the oil storage tank into the main oil tank through the second oil filtering machine, starting the first oil filtering machine, sampling the lubricating oil of the main oil tank for testing, recovering an oil pipe inside the bearing pedestal and finishing the flush if the oil meets NAS7, and carrying out the steps 3-5 repeatedly if the oil does not meet NAS7. The lubricating oil can return to the main oil tank after directly entering the bearing pedestal and being flushed, so that provisional measures taken for oil inlet and return pipes of bearing pedestals are reduced, the cost is reduced, the installation period is shortened, and oil is prevented from secondary pollution.
Owner:POWERCHINA SEPCO1 ELECTRIC POWER CONSTR CO LTD

Fur chromium-free and aldehyde-free tanning process

The invention discloses a fur chromium-free and aldehyde-free tanning process. The process includes the steps of pre-soaking, primary soaking, fleshing, degreasing, washing, enzyme bating and tanning. The degreasing process includes the steps that 0.8-1.2 g / L of a penetrating agent, 0.5-1 g / L of sodium carbonate, 1.5-2.5 g / L of an anion degreasing agent, 0.2-0.7 g / L of an enzymatic soaking agent 100-c, 0.2-0.7 g / L of lipase and 0.5-1 g / L of neutral enzyme FN are added; Ph is 6.5-7.5, the water temperature is 38-40 DEG C, and reaction time is 2-4 h; and after degreasing is completed, dehydration and cleaning are performed, and the tanning process is executed. The tanning process includes the steps that 1.5-2.5 g / L of Bascal S, 1.5-2.5 g / L of fatty aldehyde and 8-12 g / L of an aluminum tanning agent are added, and the water temperature is 38-40 DEG C; and after reaction is carried out for 1.5-2.5 hours, the PH value is 3-3.5, and 10-15 g / L of chromium powder is added at twice. The adjustment solution pH does not need to be adjusted by adding acid as for the Ph in the degreasing procedure, neutral salt and acid are avoided, tanned fur and fleece are loose and flexible, and a fur plate is plump, flexible and elastic. All the indexes can meet the industrial standard requirement. In addition, the pickling procedure is omitted, namely the neutral salt and acid are avoided, and pollutant emission is reduced.
Owner:桐乡市鑫诺皮草有限公司

High-temperature-resistant titanium alloy plate and annealing method thereof

The invention discloses a high-temperature-resistant titanium alloy plate. A titanium alloy plate material is prepared from the following components in percentage by weight: 0.5 to 1.2 percent of aluminum, 3 to 5 percent of silicon, 0.2 to 0.5 percent of iron, 1.2 to 1.8 percent of nickel, 0.1 to 0.2 percent of carbon and the balance of titanium. A preparation process of the titanium alloy plate comprises the following steps: 1, mixing all the raw materials according to the formula amounts, feeding the mixture into a vertical type induction heating furnace, controlling heating temperature at 1,400 to 1,450 DEG C for smelting, and performing ingoting to form a titanium alloy ingot; 2, performing hot rolling on the titanium alloy ingot prepared in the step 1 to prepare a titanium alloy plateblank; 3, performing thermal treatment on the titanium alloy plate blank prepared in the step 2; 4, performing alkaline pickling on the titanium alloy plate subjected to the thermal treatment in thestep 3 to remove a surface oxide film, and mechanically grinding the titanium alloy plate till the surface coarseness is 0.5 to 1 [mu]m, thereby obtaining the titanium alloy plate. The high-temperature-resistant titanium alloy plate is good in thermal stability and high-temperature creep resistance. The invention further discloses a method of annealing the titanium alloy plate.
Owner:BAOJI YONGSHENGTAI TITANIUM IND

High-quality flax staple fiber processing method

The invention discloses a high-quality flax staple fiber processing method. The high-quality flax staple fiber processing method adopts flax staple fibers as the raw materials and comprises the steps of pretreatment, boiling off, hot water washing, cold water washing, dehydration and drying. The method has the advantages that a weak base and an environment-friendly auxiliary are adopted to remove most of impurities such as pectin, lignin and the like, the selected auxiliary is non-toxic, tasteless, low in cost, good in impurity removal effect, and excellent in biodegradablity without causing wastewater pollution, and the damage to the strength of the fibers caused by a strong base, high temperature and high pressure in the traditional process is solved, and furthermore, the processing procedure is shortened. The processing method is capable of obviously improving the split degree and the uniformity of the flax staple fibers, enhancing the whiteness and the flexibility thereof and improving the spinnability. The split degree of the processed flax staple fiber finished product can achieve 1800 Nm, the average length thereof is 65mm, the breaking force thereof is 112-122cN, and the elongation thereof is 4.6-5.0%; therefore, the technical requirements of the production of flax yarns for circular machine weft knitted single jersey are well met.
Owner:QIQIHAR UNIVERSITY

Flushing system and flushing method of lubricating oil system of turbogenerator set

The invention discloses a flushing system and method for a lubricating oil system of a steam turbine generator unit. The method includes the first step of connecting a bearing pedestal with an oil inlet and return pipe according to the design state, the second step of removing a bearing oil inlet pipe inside the bearing pedestal, the third step of starting a first oil filtering machine and cleaning a main oil tank and the bearing pedestal, the fourth step of shutting down the first oil filtering machine, pouring all lubricating oil of the main oil tank into an oil storage tank through a second oil filtering machine, and cleaning the main oil tank and the bearing pedestal, and the fifth step of pouring the lubricating oil in the oil storage tank into the main oil tank through the second oil filtering machine, starting the first oil filtering machine, sampling the lubricating oil of the main oil tank for testing, recovering an oil pipe inside the bearing pedestal and finishing the flush if the oil meets NAS7, and carrying out the steps 3-5 repeatedly if the oil does not meet NAS7. The lubricating oil can return to the main oil tank after directly entering the bearing pedestal and being flushed, so that provisional measures taken for oil inlet and return pipes of bearing pedestals are reduced, the cost is reduced, the installation period is shortened, and oil is prevented from secondary pollution.
Owner:POWERCHINA SEPCO1 ELECTRIC POWER CONSTR CO LTD

Dyeing method of bio-based nylon 56 fabric disperse dye

PendingCN114369962AHigh authenticity rate of printingGood coloring rateDyeing processDisperse dyeTextile printer
The invention relates to the technical field of textile, and discloses an anhydrous printing method for bio-based nylon 56 fabric, which comprises the following steps: 1) treating the bio-based nylon 56 fabric by using a stabilizer to obtain gray fabric in a pre-treatment scouring process; or the fabric made of the high-stability bio-based nylon fiber is directly used as the gray fabric; and 2) thermal transfer printing or hot melting direct printing. The printing process is simple to operate, basically free of wastewater discharge, energy-saving and emission-reducing, and meets the environmental protection requirement; according to the method, the nylon 56 grey cloth of the common biotechnology is subjected to stabilizer treatment before printing, so that the nylon fabric is protected to a certain extent, and the nylon fabric is prevented from being damaged due to overhigh temperature in the heat transfer printing process or the high-temperature ageing and color fixing process of direct printing. The method disclosed by the invention is particularly suitable for fabrics made of high-stability bio-based nylon fibers, and the nylon fabrics prepared by the method do not need to be treated by adopting a stabilizer, and have the advantages of high printed certified product rate, good dyeing degree, high color fastness and good quality.
Owner:上海普弗门化工新材料科技有限公司
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