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111 results about "Ortho-nitrophenol" patented technology

[nahy-truh-fee-nawl, -nol] noun Chemistry. any compound derived from phenol by the replacement of one or more of its ring hydrogen atoms by the nitro group.

Process for preparing ortho-aminophenol by virtue of continuous catalytic hydrogenation

The invention discloses a process for preparing ortho-aminophenol by virtue of continuous catalytic hydrogenation, and the process is implemented by taking o-nitrophenol as a raw material through carrying out a continuous catalytic hydrogenation reaction in a fixed bed reactor by using a Pd/Al2O3 catalyst, and then separating and purifying the obtained product so as to obtain a target product ortho-aminophenol. The process disclosed by the invention can be used for realizing a continuous catalytic hydrogenation reaction, and is short in technological process, high in degree of automation, low in labor strength, less in equipment investment, and large in production capacity; the Pd/Al2O3 catalyst is good in selectivity and high in activity, and can be used for improving the yield and purity of products, the yield reaches up to 97%, and the purity reaches up to over 99%; no material is discharged and spills over in the whole reaction process, so that the consumption is minimized, therefore, the process is beneficial to resource conservation and environmental conservation, and has good economic and social benefits; both the labor intensity of workers is reduced, and the whole site environment is clean and tidy, so that the intrinsic competitiveness and extrinsic appearance of products are promoted, and therefore, the process is suitable for being widely applied to industrial production.
Owner:宁夏德昊科技产业有限公司

Liquid fertilizer synergistic additive and its manufacturing and using method

InactiveCN101125779AGood effectEnhance the effect and improve the utilization rate of fertilizerFertilizer mixturesGuaiacolPhenol
The invention relates to a liquid chemical fertilizer synergism additive. 0-20 percent of 2,4- dinitrophenol, 0-20 percent of a-naphthylacetic acid, 0-20 percent of indoleacetic acid, 0-20 percent of indolebutyric acid, 0-30 percent of o-nitrophenol, 0-30 percent of p-nitrophenol, 0-20 percent of 5- nitro guaiacol, 0-20 percent of guaiacol, 0-10 percent of brilliant blue, 0-10 percent of polyoxyethylene ethers surfactant and 0-70 percent of methanol according to the weight content are mixed and stirred to produce the liquid chemical fertilizer synergism additive. The fertilizer synergism additive overcomes the shortages of the existing chemical fertilizers, improves chemical fertilizer utilization ratio, reduces chemical fertilizer application and pollution to the environment, has obvious synergism effect, reaches the purpose of increasing production and efficiency, environmental protective and reducing cost, therefore, the popularization of the liquid chemical fertilizer synergism additive has significant social meaning in China as a big agricultural Country.
Owner:刘长福

Orchid plant growth regulator

The invention discloses an orchid plant growth regulator. The orchid plant growth regulator comprises a solid growth regulator and a liquid growth regulator, wherein the solid growth regulator is prepared from sodium para-nitrophenolate, sodium 2-nitrophenolate, 5-nitroguaiacol sodium salt, thiamine hydrochloride, pyridoxine hydrochloride and cyclohexanhexol in a mixing manner. The orchid plant growth regulator has the high affinity and interactivity to cytoplasm of orchid plants, to be facilitated to enter a sensitive part of a plant body, promotes the photosynthesis and the metabolism, accelerates the synthesis and the accumulation of dry substances, achieves the anti-microbial and anti-virus effects, has the characteristics of environment protection and high efficiency, greatly saves the using amount while the high efficiency is ensured, increases the effective utilization rate of raw materials, reduces the toxicity, facilitates the implementing of the medicinal value of the orchid plants, and has low cost; the orchid plant grows vigorously when the orchid plant growth regulator is used, has a high ornamental value, and has the high quality when being used as medicinal materials, has no toxic and side effects and a good medicinal effect.
Owner:GUIZHOU YANHE WUJIANG BIOTECH DEV

Bacillus alcaligenes strain for degrading ortho-nitrophenol and preparing method

The invention discloses a preparing method of bacillus alcaligenes strain Alcaligenes sp., CCTCC No.M206121 of degraded o-nitrophenol, which comprises the following steps: allocating inorganic salt culture medium with dibasic sodium phosphate, monobasic potassium phosphate, manganese sulfate, copperas, addex-magnesium, calcii chloridum, blue copperas, white copperas and hydrogen dioxide solution; adjusting pH value; sterilizing under high temperature; enriching bacterial; sampling from sludge; allocating suspending liquid with soil sample and inorganic salt; seeding into ortho-nitrophenol fresh organic salt culture medium with finite volume seeding quantity; keeping the temperature; culturing on shaker; getting enriched culture; separating and purifying enriched culture in LB solid culture medium. This invention can makes the degraded reach to 99%.
Owner:WUHAN INST OF VIROLOGY CHINESE ACADEMY OF SCI

Water-soluble o-nitrophenol-containing copper porphyrin and Schiff base copper porphyrin complex thereof, and synthesis method and application thereof

The invention discloses water-soluble o-nitrophenol-containing copper porphyrin and a Schiff base copper porphyrin complex thereof, and a synthesis method and an application thereof, and belongs to the field of chemical application. The synthesis method of THE o-nitrophenol-containing copper porphyrin and the Schiff base complex thereof is disclosed by using functional group modification as a main means. The application of the water-soluble o-nitrophenol-containing copper porphyrin and the Schiff base copper porphyrin complex thereof in biological activity, including the interaction of calf thymus DNA (ct-DNA) and in-vitro antitumor researches, is introduced. A pyridyl cation is introduced to a porphyrin ring through modification, so the hydrophilicity of lipophilic porphyrin compounds is greatly increased; and the increase of the solubility overcomes a severe defect of the porphyrin derivatives, so the anticancer performance is significantly increased. A result of the study of the application shows that the water-soluble o-nitrophenol-containing copper porphyrin and the Schiff base complex thereof have good in-vitro antitumor activity.
Owner:NORTHWEST UNIVERSITY FOR NATIONALITIES

Method for preparing o-nitrophenol through phenol nitration selectivity

InactiveCN102942487AIncreased nitrification conversionGood ortho selectivityPhysical/chemical process catalystsNitro compound preparationWater vaporHeteropoly acid
The invention discloses a method for preparing o-nitrophenol, which comprises the following steps: nitrating phenol in mild conditions with silica loaded heteropoly acid cesium as a catalyst and low-concentration nitric acid as a nitrating agent; and successively performing extraction, distillation, steam distillation and recrystallization to obtain the o-nitrophenol. The silica loaded heteropoly acid cesium is formed by loading 1% to 40% (wt%) of heteropoly acid cesium to silica. The method for preparing o-nitrophenol has the advantages of high phenol conversion rate, high o-phenol nitration selectivity, easiness in preparation of the catalyst, high catalytic activity, easy separation of the catalyst after the action, reusability and broad application prospects.
Owner:LIAOCHENG UNIV

Preparation method and application of modification electrode

The invention discloses a preparation method and application of a modification electrode. According to the preparation method, a polysulfanilic acid modified graphite electrode is prepared, the electrochemical behavior of o, m and p-nitrophenol on the electrode is studied through a cyclic voltammetry method, and a cyclic voltammetry curve is subjected to semi-differential treatment, so that the sensitivity and the separation degree of the electrode are further improved. The result shows that in a phosphate buffer solution of which the pH value is 8.00, the modified electrode has a remarkable function in distinguishing electrochemical oxidation of three isomers and a function of remarkably improving the current sensitivity. Compared with a naked graphite electrode, according to the graphite electrode, the differences of two adjacent oxidation peak potentials between o-nitrophenol and p-nitrophenol and between p-nitrophenol and m-nitrophenol are respectively increased to be 90mV and 155mV from 80mV and 133mV, and meanwhile the measurement sensitivity is remarkably improved, the peak current and the concentration of components are in relatively good linear response, and the electrode is good in reproducibility and stability.
Owner:XUCHANG UNIV

Synthesis of benzoxazolinone

A synthesis process of benzoxazolinone is a reaction process is organic solvent in a sealed high pressure reactor with CO and o-nitrophhenol as raw material, Se as catalyst, DBU and triethylamine as cocatalyst. The molar amount of Se is 0.1-20 % that of reactant, organic strong alkali DBU 10-200 %, triethylamine 10-200%, the molar ratio of reactant to the solvent is 1 to 1-50, the reaction time is 2-20 hr, the reaction temperature is 50-200 deg.C and CO reactant pressure is 1-10 MPa gauge pressure. The present invention has simple operation, easy-to-obtain material, fewer reaction steps and high yield.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Method for returning straws to field

The invention discloses a method for returning straws to a field. According to the method, straws are collected, naturally dried and crushed; the crushed straw is soaked in a treatment solution; filtering is carried out, and the soaking solution is removed; the straw is steamed; the steamed straw is buried in field ditches; an organic fertilizer is applied, and soil is used for covering and is compacted. According to the invention, the straw is crushed, soaked in the treatment solution and is steamed; a composite synergist (o-nitro phenol sodium, polyaspartic acid, potentilla anserine, gibberellin, hydroxyacetamide, and sodium tripolyphosphate) is added to the organic fertilizer; with microbes in the soil, lignin in the straw can be fully degraded, and straw decomposition efficiency is greatly improved. Therefore, straw returning time is shortened, and the occurrence of wheat root diseases under a corn straw returning condition is reduced.
Owner:INST OF SOIL SCI CHINESE ACAD OF SCI

Method for preparing cyclopentanol by direct hydration of cyclopentene

The invention belongs to the field of organic chemical industry and specifically relates to a method for preparing cyclopentanol by direct hydration of cyclopentene. According to the method, materials composed of cyclopentene, water and a mixed solvent continuously pass through a fixed bed filled with a catalyst to undergo a hydration reaction, wherein the mixed solvent is composed of o-nitrophenol and alcohol according to the weight ratio of (0.5-1.5):1; after the hydration reaction, reactants are cooled and layered to obtain an oil phase and a water phase; and the oil phase material undergoes rectification at normal pressure, a fraction of 38-55 DEG C is condensed to obtain unreacted cyclopentene, a fraction of 105-120 DEG C is condensed to obtain a solvent, and a fraction of 135-165 DEG C is condensed and collected to obtain refined cyclopentanol. Conversion rate of cyclopentene is high. The solvent is more stable. During the preparation process of cyclopentanol by hydration, cyclopentene and the solvent basically undergo no side reaction to produce by-products. Thus, refining of cyclopentanol is simpler, and energy consumption is reduced.
Owner:CHINA PETROLEUM & CHEM CORP +1
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