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50 results about "Siloxide" patented technology

Siloxides are chemical compounds with the formula R₃SiOM, where R is usually an organic group and M is usually a metal cation. Also called silanoates, they are derived by deprotonation of silanols.

Preparation method of gallium ion-doped lithium lanthanum zirconium oxide solid electrolyte

PendingCN121930011ALi-accumulatorsSolid state electrolyteGallium fluoride
The invention relates to a preparation method of a gallium ion-doped lithium lanthanum zirconium oxide solid electrolyte, and belongs to the field of solid electrolytes. The preparation method comprises the following steps: adding lithium carbonate, lanthanum oxide, zirconium oxide, gallium oxide, a Ga < 3 + >-hydrogen-based silsesquioxane chelating auxiliary agent and ethanol into a ball milling tank for ball milling, drying, and then putting into a muffle furnace for pre-sintering to obtain pre-sintered powder; putting the pre-sintered powder into the ball milling tank again for ball milling, and tabletting to obtain a green body; and placing the green body in a sintering furnace, and carrying out high-temperature sintering in an oxygen atmosphere to obtain the gallium ion-doped lithium lanthanum zirconium oxide solid electrolyte, the Ga < 3 + >-hydrogen-based silsesquioxane chelating auxiliary agent is prepared from gallium fluoride, lithium carbonate, hydrogen-based silsesquioxane, citric acid and deionized water; by doping gallium ions, the ionic conductivity can be remarkably improved; and after the lithium lanthanum zirconium oxide is placed in an air atmosphere for 30 days, the retention rate of ionic conductivity is greater than 97%, and the problem of poor stability of lithium lanthanum zirconium oxide is solved.
Owner:UNITED ENERGY HOLDINGS GROUP CO LTD

Snowflake cream with pearly luster and preparation process thereof

The invention discloses snowflake cream with pearly luster and a preparation process of the snowflake cream. The snowflake cream comprises the following raw material components: a phase A: water; butanediol; glycerol; methyl glucitol polyether-20; a polyacrylate cross-linked polymer-6; sodium hyaluronate; potassium hydroxide (90%); 4-hydroxyacetophenone; xanthan gum; phase B: caprylic / capric triglyceride; cetostearyl alcohol; stearic acid; a polydimethylsiloxane; squalane; simmondsia chinensis seed oil; mineral oil; and polyethylene glycol (PEG)-100 stearate. Glyceryl stearate; tocopheryl acetate; isononyl isononanoate; a phase C: 1, 2-hexanediol; carnosine; a centella asiatica extract; collagen; the snowflake cream has the advantages of uniform pearly luster texture and the advantages of traditional snowflake cream.
Owner:SUZHOU ANTE COSMETICS CO LTD

Preparation method of cresol trozole trisiloxane intermediate

The invention discloses a preparation method of a cresol trozole trisiloxane intermediate, and belongs to the technical field of fine chemical engineering. The preparation method comprises the following steps: by taking 2, 6-dibromo-4-methylphenol as a raw material, reacting with 3, 4-dihydropyran under the action of p-toluenesulfonic acid, so as to generate an intermediate 2-(2, 6-dibromo-4-methylphenoxy) pyran; reacting with sodium methoxide under the action of a catalyst to generate an intermediate 2-(2-bromo-4-methyl-6-methoxyphenoxy) pyran; then generating a Grignard reagent, carrying out coupling reaction on the Grignard reagent and 3-bromine-2-methallyl, finally reacting with benzotriazole lithium salt, and carrying out acidolysis deprotection to obtain the cresol trozole trisiloxane intermediate. The raw materials are available in the market, the overall yield is high, and a route reference is provided for synthesis of the compounds.
Owner:安徽英特美科技有限公司

Supported chiral phosphine heterogeneous catalysts, methods for their preparation and use

ActiveCN116586110BPtru catalystTetraisopropyl titanate
The application discloses a supported chiral phosphine heterogeneous catalyst and a preparation method and application thereof, and relates to the technical field of heterogeneous catalyst preparation. The method comprises the following steps: mixing hollow mesoporous polystyrene nanospheres, chiral phosphine and DCE, stirring, adding FDA, stirring, adding concentrated sulfuric acid dropwise, and reacting to obtain a reactant one; and mixing the reactant one, toluene, tetramethyldisiloxane and tetraisopropyl titanate, and reacting under temperature rise to obtain the supported chiral phosphine heterogeneous catalyst. The application is simple and convenient in a one-pot method, and can efficiently anchor the chiral phosphine and its oxide catalyst to the carrier. The application solves the problems of complicated modification in the existing organic catalyst immobilization process and mass transfer limitation of the prepared catalyst.
Owner:SOUTHWEST UNIV

Process for the synthesis of an empagliflozin intermediate

This invention discloses a synthetic process for an empagliflozin intermediate, belonging to the technical field of pharmaceutical intermediate synthesis. The synthetic process is as follows: 2-chloro-5-bromobenzoic acid is first mixed with dichloromethane and N,N-dimethylformamide, and thionyl chloride is added dropwise to obtain a dichloromethane solution of acyl chloride. Then, it is reacted with fluorobenzene under anhydrous aluminum trichloride catalysis to obtain intermediate EGAB-3. Then, it is dehydrated by azeotropic reaction with potassium hydroxide aqueous solution in toluene, and then refluxed with 3-hydroxytetrahydrofuran under tetrabutylammonium bromide catalysis to obtain intermediate EGAB-7. Then, it is reacted with 1,1,3,3-tetramethyldisiloxane under anhydrous aluminum trichloride and nitrogen protection, dried, and tested to be qualified to obtain empagliflozin intermediate. This process achieves high purity, high yield, and low isomer impurities in the preparation of empagliflozin intermediate.
Owner:ANHUI MENOVO PHARM CO LTD

A micro-hole crossing hole deburring method for precision components of semiconductor devices

The application relates to a deburring method for a micro-aperture cross-hole of a semiconductor equipment precision component. The method comprises the following steps: deburring liquid: uniformly mixing cage polysilsesquioxane-octakis-epoxy nano silicon dioxide dispersion, phenylboronic acid, octakis octyl cage polysilsesquioxane, an activated dispersant and a first solvent to obtain a first mixed liquid; dissolving an organic acid in a second solvent to obtain a second mixed liquid, adding the second mixed liquid into the first mixed liquid, adjusting the PH value to 3-5 to obtain an environment-friendly deburring liquid; capillary removal: removing the burrs inside the hole of the semiconductor equipment precision component by using the heated deburring liquid, and then performing flushing to obtain the precision component with the removed burrs and the recycled deburring liquid. The above scheme realizes the triple effects of "grinding-dissolving-protection", improves the burr removal effect of the micro-aperture cross-hole of the semiconductor equipment precision component, and can maintain good removal effect for long-term repeated use and heating.
Owner:GD TECH DONGGUAN

A method for preparing a 3D printed impact-resistant, elastic conductor material

This invention discloses a method for preparing a 3D-printed impact-resistant elastic conductor material. Silver particles / silver nanosheets are used as the conductive phase, and polyboron dimethylsiloxane (PBMS) is used as the impact-resistant material. The addition of a polyhydroxyl-based low-boiling-point solvent reversibly adjusts the density of the dynamic B-O crosslinking bonds within PBMS and reversibly increases the number of silanol groups, thereby increasing the hydrogen bond density and enhancing the printability of PBS without affecting its shock-absorbing effect. This invention utilizes the reversible reaction principle between the polyhydroxyl-based low-boiling-point solvent and the dynamic B-O crosslinking bonds to control the decrease and recovery of B-O density. Simultaneously, due to the percolation effect of silver powder particles / silver sheets, the Ag / PBS impact-resistant elastic conductor exhibits excellent conductivity. After vacuum drying of the polyhydroxyl-based low-boiling-point solvent in the printed pattern, the density of the dynamic B-O crosslinking bonds is restored, and the Ag / PBS impact-resistant elastic conductor regains its good shear thickening effect, conductivity, sensing performance, and self-healing properties.
Owner:HEFEI UNIV OF TECH

A method for preparing a catalytic membrane for HCl oxidation reaction

This invention relates to a catalytic membrane for HCl oxidation reaction, the preparation method of which includes: Step 1: reacting silica particles with SiO2. ­2 A mixture of ZrO2 sol and silica gel is coated onto a hollow fiber carrier and calcined to obtain a transition layer for the membrane. Step two: A silsesquioxane sol is applied to the transition layer obtained in step one and calcined to obtain a silica membrane. Step three: The silica membrane obtained in step two is subjected to impurity removal treatment. Step four: A solution of silane coupling agent (A) and a metal salt solution (B) are prepared separately and mixed to obtain solution C. The silica membrane treated in step three is immersed in solution C and grafted with nano-metal particles using ultrasonic assistance, followed by a high-temperature reaction to obtain a catalytic membrane. The catalytic membrane designed in this invention, when applied to the HCl oxidation reaction, can separate reactants and products simultaneously, causing the reaction to shift forward, increasing the reaction conversion rate, reducing the reaction temperature, and extending the catalyst lifetime.
Owner:WANHUA CHEMICAL (NINGBO) CO LTD

Preparation process of high-flame-retardance cable

The invention relates to the technical field of cables, in particular to a preparation process of a high-flame-retardance cable. According to the process, low-density polyethylene and an ethylene-vinyl acetate copolymer are adopted as matrixes, silane is grafted through twin-screw extrusion, then nano-composite flame retardants based on magnesium-aluminum layered double hydroxides, phosphine compounds, polyhedral oligomeric silsesquioxane and the like are introduced, and a proper amount of magnesium hydroxide, aluminum hydroxide and zinc borate are added for synergistic flame retardance and smoke suppression. The nano-composite flame retardant is subjected to multiple surface modification and function synergy, so that the interface bonding and dispersity can be remarkably improved, a compact carbonized and ceramic layer is formed, and low-smoke, low-combustion-spread and stable low-dielectric properties are realized.
Owner:东莞市帝深电子有限公司

Method for preparing aerogel powder from waste gel

The invention provides a method for preparing aerogel powder from waste gel, and belongs to the technical field of aerogel material preparation. The method comprises the following steps: by taking waste wet gel generated when an aerogel product is produced from an organic silicon source as a raw material, adding an ammonium fluoride solution, stirring and uniformly mixing, adding hexamethyldisiloxane, n-butyl alcohol and hydrochloric acid for modification, cooling and standing after modification, and separating out an upper-layer gel solution; stirring and cleaning with pure water, standing to obtain washing water, adding a sodium hydroxide aqueous solution, stirring and cleaning, and standing to obtain alkali washing water; and drying through closed-loop spray drying equipment to obtain the aerogel powder. According to the method, resource utilization of the waste gel is achieved, the production cost of the aerogel powder is reduced, environmental pollution is reduced, and the obtained aerogel powder has good hydrophobicity and heat insulation performance.
Owner:HUBEI XINGRUI SILICON MATERIAL CO LTD

A sealant and its preparation method and application

The application provides a sealant and a preparation method and application thereof. The sealant comprises the following components in parts by weight: 100 parts of alpha, omega-dihydroxypolydimethylsiloxane, 2.5-6.5 parts of a plasticizer, 80-100 parts of a filler, 8-15 parts of a crosslinking agent, 1.5-2 parts of a coupling agent and 0.1-0.2 parts of a catalyst, wherein the coupling agent is a reactant of an amino silane coupling agent and a hydroxyl-terminated polybutadiene. The amino silane coupling agent is chemically modified by using the hydroxyl-terminated polybutadiene, so that the adhesion and the moisture and heat resistance of the sealant can be significantly improved.
Owner:GUANGZHOU JOINTAS CHEM

A process for the preparation of a heptaphenyltrihydroxylsilsesquioxane

The present application relates to the technical field of silsesquioxane preparation, in particular to a preparation method of heptaphenyl trihydroxysilsesquioxane; specifically, heptaphenyl trisodium silsesquioxane is prepared by reacting phenyl trimethoxysilane and sodium hydroxide in an organic solvent medium, then tin-doped solid acid catalyst and heptaphenyl trisodium silsesquioxane are added in a tetrahydrofuran medium, and heptaphenyl trihydroxysilsesquioxane is prepared in an ice water bath. The heptaphenyl trihydroxysilsesquioxane prepared by the method has high yield, and the service life of the solid acid catalyst is long, and the solid acid catalyst can be recycled.
Owner:QUZHOU ZHONGTONG CHEM

Process for the preparation of alkali metal salts of oxalate-based chelating structures

ActiveCN116925147BEasy to separate and purifylow costPhosphoric Acid EstersPotassium fluoride
The application belongs to the technical field of compound preparation, and particularly relates to a preparation method of an alkali metal salt of an oxalate chelate structure, at least comprising the following steps: mixing tris(trimethylsilyl) phosphate, an oxalate and a phosphorus-containing or boron-containing fluorine compound in a first organic solvent, stirring and heating to obtain lithium phosphate, trimethyl fluorosilane gas, and difluorobisoxalate phosphate or difluorooxalate borate, filtering the reaction solution to obtain lithium phosphate solid and a difluorobisoxalate phosphate solution or a difluorooxalate borate solution; adding a second organic solvent for recrystallization after concentration; and obtaining difluorobisoxalate phosphate or difluorooxalate borate solid after filtration, and drying the solid under reduced pressure to obtain a finished product. The process is simple, and the cost is low. By-products lithium phosphate, potassium fluoride and hexamethyldisiloxane can be directly sold as products after purification. Therefore, the application has an atomic utilization rate close to 100%, no invalid waste, less three-waste emissions, and is friendly to the environment.
Owner:CHANGDE DADU NEW MATERIAL CO LTD

A softener for use in the same bath as a waterproofing agent, its preparation method and its application

This application discloses a softener for use in conjunction with a waterproofing agent, its preparation method, and its application. The preparation method includes the following steps: S1: reacting a double-ended hydrogen-containing silicone oil with a long-chain carbide under the action of an inert gas and a catalyst to prepare a first intermediate; S2: reacting the first intermediate, octamethylcyclotetrasiloxane, 3-methacryloyloxypropylmethyldimethoxysilane, and 3-(2,3-epoxypropoxy)propylmethyldimethoxysilane to prepare a second intermediate; S3: reacting the second intermediate with an organic diamine to prepare the softener for use in conjunction with the waterproofing agent. The softener of this application, used in conjunction with a waterproofing agent, can maintain good waterproofing while improving fabric softness.
Owner:NINGBO RUNHE HIGH TECH MATERIAL CO LTD

Light conversion type ETFE film for photovoltaic packaging and preparation method thereof

The invention relates to the technical field of preparation of tetrafluoroethylene copolymer films, and provides a light conversion type ETFE film for photovoltaic packaging and a preparation method thereof, the ETFE film comprises the following raw materials by weight: 100 parts of an ethylene-tetrafluoroethylene copolymer; 0.1-1 part of a light conversion agent; the chemical general formula of the light conversion agent is A2BXO6: Ln < 3 + >, A is at least one of Ca < 2 + >, Sr < 2 + > and Ba < 2 + >, B is Zn < 2 + > or Mg < 2 + >, X is Ti < 2 + > or Si < 2 + >, and Ln < 3 + > is one or more of Sm < 3 + >, Tb < 3 + > and Eu < 3 + >; the weight part of the compatilizer is 20%-50% of the weight part of the light conversion agent, and the compatilizer is a phosphate ester surfactant or a siloxane compound containing perfluoroalkyl. Compared with the prior art, the ETFE film has the advantages that the use of auxiliaries such as a light stabilizer and an antioxidant can be avoided, the potential risk caused by the compatibility of various auxiliaries is avoided, the complexity and the cost of the formula are reduced, and the mechanical property and the photoelectric conversion property of the ETFE film are improved.
Owner:SHANDONG XUBEI NEW MATERIAL CO LTD

Vehicle tires

UndeterminedDE102025102446A1Classical mechanicsSilicon dioxide
The invention relates to a vehicle tire (1) comprising: a) a tire carcass (4) with a first side region (5), a second side region (6) and a central region (7) arranged between them, comprising at least one carcass ply (8, 18) with a plurality of rubberized reinforcing elements (9) extending through the first side region (5), the second side region (6) and the central region (7) of the tire carcass (4); b) a tread strip (4) located radially further outwards relative to the tire carcass (4); c) an inner tire layer (11) located radially further inwards relative to the tire carcass (4), wherein at least a portion of the rubberized reinforcing elements (9) of the carcass ply (8, 18) enclose an angle (14) in the range of 80° to 90° with respect to the circumferential direction (3) in the first side region (5) and in the second side region (6) and an angle (15) in the range of 5° in the central region (7). up to 75°wherein a damping element (12) is arranged on the inner layer (11) of the vehicle tire (1), wherein the damping element (12) is arranged on the inner layer (11) of the tire by means of a connecting device (29), wherein the connecting device (29) comprises a mixture of organopolysiloxanes, wherein the mixture of organopolysiloxanes comprises in particular calcium carbonate, siloxanes, trimethoxysilanes, carbon black and / or silicon dioxide.
Owner:CONTINENTAL REIFEN DEUTSCHLAND GMBH

An adsorbent, its preparation method and application

The present invention provides a wicking agent, a preparation method thereof and an application thereof, relating to the field of oilfield chemistry. The wicking agent provided by the present invention comprises a compound shown in Formula I. In Formula I, R1 is selected from carboxyl groups; X + represents a cationic group and is selected from one of sodium atoms and potassium atoms; n = 6, 8, 10, 12; POSS is cage-like silsesquioxane. Due to the presence of the POSS group in the wicking agent provided by the present invention, which replaces the traditional hydrophobic alkyl chain, the wicking agent has a larger hydrophobic area, thus having a stronger effect of reducing the free energy of the oil-water interface and being more likely to obtain a lower oil-water interfacial tension. At the same time, the benzene ring in the wicking agent has good thermal stability and has a sulfonate group as a strong hydrophilic group, thereby providing a novel Gemini surfactant with a super-large hydrophobic area and good thermal stability, which has broad application prospects in high-temperature and high-salt oil reservoirs.
Owner:SINOPEC OILFIELD SERVICE CORPORATION +2

Preparation method of EVA waterproof coating

The application relates to the technical field of paint, and discloses a preparation method of EVA waterproof paint, in which montmorillonite is activated and reacted with toluene diisocyanate to obtain isocyanate modified montmorillonite. EVA is hydrolyzed under the catalysis of potassium hydroxide to obtain hydroxylated EVA. An epoxy group trisiloxane intermediate is reacted with terephthalic acid under the ring-opening esterification of benzyl triethyl ammonium chloride to obtain p-hydroxy trisiloxane benzoate. The p-hydroxy trisiloxane benzoate, the hydroxylated EVA, the isocyanate modified montmorillonite and toluene diisocyanate are crosslinked under the catalysis of stannous octoate, then a defoaming agent and a dispersing agent are added, and stirring is carried out until uniformity, so that the EVA waterproof paint is obtained. The prepared EVA waterproof paint has good mechanical properties and waterproof performance.
Owner:JIANGSU FANPIN NEW MATERIAL CO LTD

Silanol-containing organic-inorganic hybrid coatings for high resolution patterning

Silanol-containing organic-inorganic hybrid coatings on semiconductor substrates for forming patterns thereon. The present coatings can be produced by coating of semiconductor substrates with metal and silanol containing polyhydridosilsesquioxane resin solutions. Provided herein is also a method for patterning a metal and silanol containing polyhydridosilsesquioxane coated substrate with radiation of light at a specific wavelength, the method comprising the steps of irradiating a coated substrate along a selected pattern to form an irradiated structure with a region of irradiated coating and a region with un-irradiated coating and selectively developing the irradiated structure to remove a substantial portion of the un-irradiated coating to form a patterned substrate. The invention allows for obtaining a preselected silanol content polyhydridosilsesquioxane resin, and adjustment of the silanol content will make it possible to obtain a highly sensitive coating for application in EUV.
Owner:PIBOND OY

Bismuth-based metal passivator and preparation method thereof

The invention belongs to the technical field of metal passivators, and particularly provides a bismuth-based metal passivator and a preparation method thereof. The preparation method of the bismuth-based metal passivator comprises the following steps that bismuth salt, auxiliary metal salt and organic carboxylic acid react under nitrogen protection, a heteronuclear metal organic cluster compound is obtained, then the heteronuclear metal organic cluster compound reacts with a silane coupling agent under the catalyst condition, and the bismuth-based metal passivator is obtained. The bismuth-based metal passivator prepared by the preparation method can be anchored on the surface of an FCC (fluid catalytic cracking) catalyst through siloxane groups at a low temperature to reduce loss or invalid dispersion of bismuth active components, and can reduce agglomeration of the bismuth active components through auxiliary metals at a high temperature, and meanwhile, the auxiliary metals can also cooperate with the bismuth active components to react with polluted metals, so that the metal passivator can be applied to the FCC catalyst. And a stable new phase is formed, so that polluted metal is effectively passivated.
Owner:JIANGSU CHUANGXIN PETROCHEM

Hydrolysis-resistant polycarbonate composition

ActiveUS12649852B2SulfonatePolymer science
The present invention relates to a polycarbonate composition including the following components: A) 80-97.5 parts by weight of aromatic polycarbonate; B) 0.1-0.3 part by weight of metal organic sulfonate; C) 0.3-0.7 parts by weight of anti-dripping agent; D) 0.1-4 parts by weight of hydrolysis stabilizer; and E) 2-7 parts by weight of polysilsesquioxane. The total amount of the composition is 100 parts by weight. The present invention also relates to a shaped article made from the composition. The polycarbonate composition according to the present invention has a good combination of hydrolysis resistance and flame retardance.
Owner:COVESTRO DEUTSCHLAND AG

Method for magnesium-cobalt bimetal pyrophosphate catalyzing hydrosilylation reaction and application

The application relates to a method and application of magnesium-cobalt bimetal pyrophosphate catalyzed silicon-hydrogen addition reaction, which is prepared by taking an alkenyl-containing compound and a hydrogen-containing silane or hydrogen-containing silicone oil as raw materials and under the action of a magnesium-cobalt bimetal pyrophosphate catalyst to carry out silicon-hydrogen addition reaction to obtain an addition product. The chemical structural formula of the magnesium-cobalt bimetal pyrophosphate is Mg x Co 2‑x P2O7, wherein 0
Owner:HANGZHOU NORMAL UNIVERSITY

Liquid formulation of RNA

PendingCN122514299AAdjuvantMeth-
This invention relates to an RNA liquid formulation comprising: (a) at least one RNA composition comprising at least one isolated RNA molecule and a silica carrier, and (b) an adjuvant selected from (A), (B), and (C): (A) having the general formula (I)M j D k T l The polyglycerol ester, wherein M is [C3H5(OR'')2O 1 / 2 D is [C3H5(OR'')1O] 2 / 2 T is [C3H5O] 3 / 2 ], j=1 to 10, preferably 2 to 3, more preferably 2; k=0 to 10, preferably greater than 0 to 5, more preferably 1 to 3; l=0 to 3, preferably 0 to 1, more preferably 0; wherein, the sum of j+k+l is 1 to 20, preferably 2 to 4, more preferably 3, wherein each group R'' is independently selected from acyl groups R'-C(=O)- and H, provided that at least one group R'' is not equal to H; wherein each group R' is independently selected from monovalent aliphatic, saturated or unsaturated hydrocarbon groups having 3 to 39, preferably 7 to 21, more preferably 9 to 17 carbon atoms; (B) Formula (II)M 1 o D 1 p D' q Among the polyether-modified siloxanes, M 1 It is P 1 3SiO 1 / 2 D 1 It is P 1 2SiO 2 / 2 D' is P 1 P 2 SiO 2 / 2 o is 2, p is between 0 and 0.1, q is between 1.0 and 1.15, P 1 Independently, it is a hydrocarbon group having 1 to 8 carbon atoms, P 2 Independently for equation (III)—P 3 O[CH2CH2O] m [CH2CH(CH3)O] n P 5 The polyether groups have m ranging from 3.4 to 11.0 and n ranging from 2.5 to 8.0, and the condition is that m / n is 1.9 to 2.8, P 3 Independently, it is a divalent hydrocarbon group having 2 to 8 carbon atoms, P 5The form is hydrogen; and (C) is an organic modified polysiloxane of formula (IV) where a+b+c+d+2=20 to 210, a is 15 to 205, b is 1 to 12, c is 1 to 12, d is 1 to 12, R groups are each independently the same or different aliphatic or aromatic hydrocarbon groups having 1 to 10 carbon atoms, R4 groups are each independently the same or different R, R1, R2 or R3 groups, R1, R2 and R3 groups are each independently different polyether groups of general formula (V) where e is 3 to 11, f is 6 to 30, g is 0 to 15, h is 0 to 5, i is 0 to 6, and R5 are independently the same or different, and each is a methyl, acetyl or hydrogen group.
Owner:EVONIK OPERATIONS GMBH

POLYORGANOHYDROCATIONAL SILOXIDE COMPOSITION WITH A LEWIS ACID MONOCATIONIC PHOSPHONIUM SALT

ActiveDE602023013778T2Phosphonium saltSilica hydride
Owner:DOW GLOBAL TECHNOLOGIES LLC +1

A process for preparing a high flame retardant cable

The present application relates to the technical field of cable, in particular to a preparation process of high flame-retardant cable. The process adopts low-density polyethylene and ethylene-vinyl acetate copolymer as the matrix, and introduces nanometer composite flame retardant based on magnesium-aluminum layered double hydroxide, phosphine compound and cage polysilsesquioxane, and appropriate magnesium hydroxide, aluminum hydroxide and zinc borate for synergistic flame retardation and smoke suppression through double-screw extrusion grafting silane. The nanometer composite flame retardant is modified on multiple surfaces and functions synergistically, which can significantly improve the interface combination and dispersibility, form a dense carbonized and ceramic layer, and achieve low smoke, low combustion spread and stable low dielectric performance.
Owner:东莞市帝深电子有限公司

Preparation method and application of 5-bromo-2-chloro-4 '-ethoxydiphenylmethane

PendingCN121824276ABuffers strong Lewis acidsAccelerate the ruptureOrganic chemistryOrganic compound preparationChlorobenzeneKetone
The invention relates to a preparation method and application of 5-bromo-2-chloro-4 '-ethyoxyl diphenylmethane, (5-bromo-2-chlorphenyl) (4-ethyoxyl phenyl) ketone is subjected to a reduction reaction to obtain 5-bromo-2-chloro-4'-ethyoxyl diphenylmethane, and the route is high in reaction rate and few in by-product. In addition, the organic ether solvent is lower in toxicity, low in boiling point and easy to remove. The used reagent (tetramethyldisiloxane as a reducing agent) is low in price and good in reaction activity, so that the reaction time is short. The reaction conditions are mild, high-temperature and high-pressure conditions are not needed, the reaction operation and post-treatment are simple and convenient, only conventional operations such as liquid separation concentration and crystallization are needed, and less wastewater is generated in the reaction; reagents with low safety such as a reducing agent sodium borohydride and the like are not used in the reaction, the safety of the whole reaction is high, the yield of the reaction route is high, and therefore the method is suitable for large-scale and industrial production.
Owner:ZHEJIANG MENOVO PHARMA

Polysilsesquioxane liquid precursor, cured object, and production methods therefor

PendingUS20260184855A1Polymer sciencePtru catalyst
A polysilsesquioxane liquid precursor includes a copolymer of a trifunctional silicon alkoxide and a difunctional silicon alkoxide, and residual silanol group fraction fSiOH in the copolymer is 0.02 to 0.3. A method for producing a polysilsesquioxane liquid precursor includes subjecting a trifunctional silicon alkoxide and a difunctional silicon alkoxide to a hydrolysis reaction and a polycondensation reaction in an aqueous solution without using an organic solvent in the presence of an acid catalyst, with aging during the hydrolysis reaction and the polycondensation reaction.
Owner:AGC INC +1

Preparation method of solid acid catalyst, solid acid catalyst and application

The invention discloses a preparation method of a solid acid catalyst, the solid acid catalyst and application, and relates to the technical field of catalysts. The solid acid catalyst is prepared by mixing a benzene diacid compound, a zirconium salt compound, concentrated hydrochloric acid and water and carrying out hydrothermal reaction, the preparation method is simple and easy to implement, the Bronsted acid site on the prepared catalyst shows very high catalytic activity and selectivity, the required reaction conditions are mild, and the catalyst is convenient to separate from a reaction system and can be repeatedly utilized. Besides, when the solid acid catalyst is applied to preparation of the single-ended hydrogen-containing silicone oil (such as 1, 1, 1, 3, 3-pentamethyldisiloxane), the single-ended hydrogen-containing silicone oil with higher yield can be obtained, and meanwhile, the preparation process of the single-ended hydrogen-containing silicone oil can be simplified.
Owner:JIANGSU MAYSTA CHEM

A lithium / sodium ion battery adhesive based on silsesquioxane and a preparation method and application thereof

The application discloses a lithium / sodium ion battery adhesive based on silsesquioxane and a preparation method and application thereof, and belongs to the technical field of new energy materials. The preparation method is as follows: a solvent, a cage-type silsesquioxane, mixed monomers and a catalyst are mixed, water and oxygen in a reaction system are removed; and the reaction is carried out under the protection of nitrogen or argon, so that the lithium / sodium ion battery adhesive based on silsesquioxane is obtained. The adhesive is obtained through one-step reaction, and has good bonding effect and negative electrode capacity improvement effect on lithium ion batteries and sodium ion batteries.
Owner:NANJING UNIV