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35results about How to "Achieve high-value conversion" patented technology

Method for preparing bioethanol

The invention provides a method for preparing bioethanol. The method comprises the following steps of: performing constant-temperature shaking culture on plant fiber and seed liquid of a cellulase producing strain for 0 to 5 days in a fermentation culture medium, inoculating seed liquid of an ethanol producing strain into the fermentation culture medium, and continuing to perform constant-temperature shaking culture for 3 to 7 days; and filtering fermentation liquor, and distilling a filtrate under reduced pressure to obtain the bioethanol. The method for preparing the bioethanol is high in yield and low in cost, is environment-friendly, and is suitable for industrialized production.
Owner:JIANGSU UNIV OF SCI & TECH

Method for extraction of mulberry pectin via coupling of N-methyl morpholine oxide and cellulase

The invention discloses a method for extraction of mulberry pectin via coupling of N-methyl morpholine oxide and cellulose, which comprises the following steps of: (1) processing mulberry barks with the N-methyl morpholine oxide: using the mulberry barks as raw materials, processing the mulberry barks with the N-methyl morpholine oxide for equal-component separation of pectin and cellulose in the mulberry barks, adding water after processing, so that the pectin is dissolved in water and the cellulose, hemicellulose, lignin and other components are precipitated; (2) processing the cellulase: taking the supernatant liquid, adding the cellulase for processing, and removing cellulose impurities; and (3) preparing the pectin: bleaching the supernatant liquid, adding ethyl alcohol for precipitation of the pectin, washing with absolute ethyl alcohol, and drying and grounding into powder to obtain the mulberry pectin. The N-methyl morpholine oxide is used as a processing agent to extract the pectin in the mulberry barks, the pectin can be extracted efficiently, only 20-50min is needed for processing with the NMMO (N-methyl morpholine oxide), the final yield of pectin can reach 11 percent, and the efficiency of extraction of the pectin from the mulberry barks can be increased.
Owner:JIANGSU UNIV OF SCI & TECH

Preparation method of mulberry protein active peptide

The invention discloses a preparation method of mulberry protein active peptide. The method comprises the following steps that mulberry leaves and mulberry bark are washed, dried and smashed, a treating agent prepared from magnetic graphene oxide, dilute acid and hydrogen peroxide is added for digestion, the magnetic graphene oxide is recycled through a magnet, the pH value is adjusted to be 4.5-5.5, precipitate is obtained through centrifugation, water is added into the precipitate for dissolving and filtration, filtrate contains mulberry protein solution, heating treatment is carried out, cooling is carried out, the pH value is adjusted to be 7-8.5, protease is added for heat preservation, the product is placed in an ultrasonic field for ultrasonic assisted enzymolysis, high-temperature heating is carried out for inactivating enzyme, centrifugation is carried out, supernate is collected, decoloring, suction filtration, ultrafiltration, dialysis, ion exchange and concentration are carried out, and the mulberry active peptide is obtained. Mulberry leaves and mulberry bark are adopted as raw materials for preparing the active peptide, and the raw materials are agricultural waste, are low in cost and are of great significance in environmental protection and waste resource utilization. The mulberry protein extraction content and mulberry protein active peptide conversion efficiency are higher compared with a conventional method, and physical and chemical property is stable.
Owner:JIANGSU UNIV OF SCI & TECH

Preparation method of mulberry fiber composite three-dimensional oil-water separation membrane

ActiveCN112717472ASolve the problem of purely physical mixingIncrease the space contact areaSemi-permeable membranesLiquid separationMultilayer membraneFiber
The invention discloses a preparation method of a mulberry fiber composite three-dimensional oil-water separation membrane, and belongs to the technical field of membranes. The preparation method comprises the following preparation steps: (1) preparing mulberry fibers; (2) treatment and modification of mulberry fibers: using enzyme partial treatment and ionic liquid mixed liquid treatment; (3) preparing a single-layer membrane: adding a cross-linking reagent, a hydrophobic reagent and an initiator, and drying and molding to obtain a molded hydrophobic and oleophylic single-layer membrane; and (4) preparation of the three-dimensional multilayer membrane: preparing the single-layer film into the multi-layer three-dimensional composite membrane by adopting an ionic liquid composite cross-linking agent according to application requirements. The method has the beneficial effect that a new way is provided for resource utilization of biomass wastes. The method has the advantages of high efficiency, environmental friendliness and the like, the spatial dimension and the contact area of the membrane are improved, and the problem of poor mechanical properties of the membrane in the use process is solved.
Owner:JIANGSU UNIV OF SCI & TECH

A method for preparing carbon-based transition metal sulfide composite electrode material based on pyrolysis bio-oil

The invention belongs to the technical field of biomass resource utilization and electrode material preparation, and relates to a method for preparing a carbon-based transition metal sulfide composite electrode material based on pyrolysis bio-oil. First, dissolving nickel sulfate or cobalt sulfate into an alcohol / water solution to prepare a bio-oil absorbing solution; then using the absorbing solution to capture the bio-oil produced by biomass pyrolysis, drying the absorbing solution after the pyrolysis reaction, and then passing After being calcined in a reducing atmosphere and cooled to room temperature, the composite electrode material can be prepared. The invention uses bio-oil produced by biomass pyrolysis as raw material, and the prepared composite electrode material has excellent supercapacitor performance: under the current density of 1 A / g, the specific capacitance of the composite electrode material is as high as 1000 F / g above. In addition, the biomass raw material of the invention is cheap, green and sustainable, and the preparation process is simple, which provides a new approach and idea for the high-value conversion of biomass resources and the preparation of carbon-based transition metal sulfide composite electrode materials.
Owner:山东济清科技服务有限公司

Production process of 2-amino-3,5-dibromobenzaldehyde

The invention relates to the technical field of pharmaceutical chemicals, in particular to a production process of 2-amino-3,5-dibromobenzaldehyde. The method comprises the following steps: mixing iron powder and hydrochloric acid, adding an extracting agent and 3-nitro-o-dibromomethyl benzene, adjusting the pH value to 7-9 after the reaction is finished, conducting filtering, and separating the liquid to obtain an 3-amino-o-dibromomethyl benzene extraction reaction liquid; adding sulfuric acid into the reaction solution, conducting stirring, and conducting separating to obtain a 3-amino-o-dibromomethyl benzene sulfuric acid reaction solution; adding hydrobromic acid into the sulfuric acid reaction solution, dropwise adding bromogen and / or an oxidizing agent, controlling monobromine to be less than or equal to 0.2%, and adding chloroform to obtain a 2-amino-3,5-dibromodibromomethyl benzene organic solution; adding a dimethylamine aqueous solution and sodium bicarbonate into the organic solution, and separating the solution after the reaction to obtain a 2-amino-3,5-dibromobenzaldehyde chloroform reaction solution; and concentrating, refining and decoloring the chloroform reaction solution to obtain the 2-amino-3,5-dibromobenzaldehyde. The method provided by the invention can be used for industrially synthesizing the 2-amino-3,5-dibromobenzaldehyde, and the nitro waste material generated in the o-nitrobenzaldehyde production process can be utilized.
Owner:JIANGXI RONGXING PHARMA

A kind of preparation method of simulated cellulase

The invention discloses a method for preparing simulated cellulase. The method comprises the following steps: taking a cellulose material, washing, removing the impurities, drying, grinding, and screening, thereby obtaining cellulose powder; uniformly mixing and stirring the obtained cellulose powder with ionic liquid according to a mass ratio of 1-20:100, preserving the temperature, performing assisted microwave treatment so as to expand the fibers, washing to remove the ionic liquid, and drying to remove the moisture, thereby obtaining a primary sample; adding the obtained primary sample into a crucible, putting the crucible into a tube furnace, and performing heating treatment under gas protection; adding a mixed acid, adding water and washing to remove the impurities, and drying to obtain dried powder, thereby obtaining the sample powder; adding the obtained sample powder into an organic base, stirring, heating, reacting, and washing by using a cleaning solvent, thereby obtaining the simulated cellulase. The simulated cellulase prepared by the method is high in binding ability with a substrate (a cellulose material) and good in thermal stability, high-temperature catalysis can be performed, the catalytic effect is good, the cost of the raw materials is low, and the cellulase can be repeatedly utilized.
Owner:JIANGSU UNIV OF SCI & TECH

A method for co-producing bioethanol and pullulan from lignocellulosic substances

The invention discloses a method for combined production of bioethanol and pullulan from lignocellulose substances. The method comprises the following steps: subjecting the lignocellulose substances to alkaline-process pretreatment and xylanase enzymatic hydrolysis and then carrying out solid-liquid separation so as to respectively obtain a hemicellulose hydrolysate (xylose liquid) and a solid-phase residue; subjecting the solid-phase residue to lignin extraction so as to obtain a cellulose residue; directly applying the xylose liquid to fermentation production of pullulan (wherein yield is no less than 0.29 g of pullulan per g of xylose) and subjecting the cellulose residue to synchronous saccharification and fermentation to produce ethanol; subjecting fermentation broth containing pullulan to fermentation and distillation with fiber residue, carrying out alcohol precipitation on obtained ethanol, carrying out extraction and refining so as to obtain a pullulan product, combining ethanol-containing waste liquid produced during purifying with cellulose residue ethanol fermentation broth and carrying out distillation so as to realize recovery and reuse of ethanol. The method can realize full utilization and high-value conversion of hemicellulose and cellulose, saves resources and achieves the purposes of environmental protection and economic benefit improvement.
Owner:TIANJIN UNIV OF SCI & TECH

A kind of preparation method of mulberry base solid acid

The invention discloses a preparation method of a mulberry twig-based solid acid. The preparation method comprises the steps: firstly washing cleanly impurities and mud on mulberry twigs, peeling, drying, smashing, and thus obtaining a mulberry twig powder; then mixing the obtained mulberry twig powder with N-methyl morpholine oxide according to a ratio of 1:8-10, stirring at the temperature of 80-100 DEG C with the stirring time of 0.5-3 h, and assisting with ultrasonic treatment to make fibers swelled, then washing to remove N-methyl morpholine oxide, adding an auxiliary agent according to a ratio of the mulberry twig powder to the auxiliary agent of 20:1 to make the mulberry twig powder activated, and drying to remove water; then putting the obtained product into a crucible, placing in a tube furnace, adjusting the furnace temperature to 400-500 DEG C, and carrying out heating treatment with nitrogen protection and the treatment time of 1-5 h; and finally, adding fuming sulfuric acid according to a ratio of the mulberry twig powder to a 20% fuming sulfuric acid of 1:1-5, treating, washing to remove impurities, and drying to obtain the mulberry twig-based solid acid. The solid acid has the advantages of small particles, good adsorption property on reaction substrates, good catalytic effect, high thermal stability, high acid value, and low cost, and the raw materials are waste materials.
Owner:JIANGSU UNIV OF SCI & TECH

A kind of preparation method of mulberry active peptide

The invention discloses a preparation method of mulberry active peptide, which comprises the following steps: after washing, drying and crushing mulberry leaves and mulberry bark, adding a treatment agent composed of magnetic graphene oxide, dilute acid and hydrogen peroxide to extract, and using Magnet recovers magnetic graphene oxide, adjusts the pH value to 4.5-5.5, centrifuges to obtain the precipitate, dissolves the precipitate with water and filters, the filtrate contains mulberry protein solution, heats it, cools and adjusts the pH value to 7-8.5, adds protease to keep warm, and puts Ultrasonic-assisted enzymolysis in an ultrasonic field, high-temperature heating to inactivate the enzyme, centrifugation, collecting the supernatant, decolorization, suction filtration, ultrafiltration, dialysis, ion exchange and concentration to obtain the mulberry active peptide. The present invention adopts mulberry leaf and mulberry bark as raw material to prepare active peptide, and the raw material is agricultural waste with low cost, which is of great significance for environmental protection and resource utilization of waste; the method extracts mulberry protein content and conversion efficiency of mulberry active peptide Both are more than the conventional method, and the physical and chemical properties are stable.
Owner:JIANGSU UNIV OF SCI & TECH

Method for preparing carbon-based transition metal sulfide composite electrode material based on pyrolytic bio-oil

The invention belongs to the technical field of biomass resource utilization and electrode material preparation, and relates to a method for preparing a carbon-based transition metal sulfide compositeelectrode material based on pyrolysis bio-oil. The method comprises the following steps: firstly, dissolving nickel sulfate or cobalt sulfate into an alcohol/water solution to prepare a bio-oil absorption solution, capturing bio-oil generated by biomass pyrolysis by using the absorption liquid, drying the absorption liquid after the pyrolysis reaction is finished, calcining the absorption liquidin a reducing atmosphere, and cooling the absorption liquid to room temperature to obtain the composite electrode material. According to the invention, bio-oil generated by biomass pyrolysis is used as a raw material, and the prepared composite electrode material has excellent supercapacitor performance: under the current density of 1 A/g, the specific capacitance of the composite electrode material is as high as 1000 F/g or above. Besides, the biomass raw material is low in price, green and sustainable, the preparation process is simple, and a new way and idea are provided for biomass resource high-value conversion and preparation of the carbon-based transition metal sulfide composite electrode material.
Owner:山东济清科技服务有限公司
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