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50results about How to "Improve mass transfer conditions" patented technology

Method for preparation of 2, 5-dichloronitrobenzene by continuous nitration

ActiveCN106083596AOptimize process flowWith automatic separation functionNitro compound preparationNitrationOil phase
The invention discloses a method for preparation of 2, 5-dichloronitrobenzene by continuous nitration. The method comprises the steps of: adopting three-stage kettle type continuous reaction, adding sulfuric acid, nitric acid and p-dichlorobenzene in an extraction kettle into a first stage nitrification kettle simultaneously to carry out nitrification reaction, letting nitrification liquid enter a next stage nitrification kettle through self-carried raisers of all nitrification kettles in order to react, at the end of reaction in a third stage nitrification kettle, separating an oil phase and an acid phase, carrying out neutralization, washing and dehydration on the oil phase so as to obtain 2, 5-dichloronitrobenzene, internally recycling part of waste acid in the acid phase back to the first stage nitrification kettle, letting the residual waste acid enter an extraction kettle, and performing p-dichlorobenzene extraction, and then conducting separation to obtain acidic p-dichlorobenzene and extracted waste acid, concentrating the extracted waste acid into concentrated sulfuric acid, and making the concentrated sulfuric acid and acidic p-dichlorobenzene enter the first stage nitrification kettle for recycling. The method provided by the invention adopts automation control, cancels a mixed acid preparation procedure, simplifies the technological process, can realize continuous nitrification reaction, continuous nitrification liquid separation and continuous waste acid extraction.
Owner:江苏拓孚工程设计研究有限公司

Injection type spiral stirrer for molten iron desulphurization

ActiveCN110699508AIncrease entrainment cycle flowReduce shear power consumptionRotary stirring mixersTransportation and packagingChemistryEngineering
The invention discloses an injection type spiral stirrer for molten iron desulphurization. A porous injection head (6) and spiral stirring blades (4) are arranged on a stirring shaft. All the stirringblades (4) are uniform in size and are distributed circumferentially evenly at intervals. The center of the whole stirring shaft achieves communication vertically to form a cavity-shaped straight-through injection pipe (7). The lower end of the straight-through injection pipe (7) forks at the porous injection head (6) to form a plurality of small injection conduits (8) in a through mode. All thesmall injection conduits (8) penetrate through the outer surface of the porous injection head (6), and thus a desulfurizer passes through the straight-through injection pipe (7) to be injected to theoutside of the porous injection head (6) in multiple directions from top to bottom. The stirring blades can enlarge the mixed area of axial and radial stirring of the desulfurizer, roll-suction circulation flow is increased, shear power consumption is lowered, and the stress conditions of the stirring blades are improved. The motion mode of desulfurizer vapor in molten iron can be further improved, thus the desulfurizer vapor does spiral rising motion, the dissolution degree is increased, and desulphurization is effective. The injection type spiral stirrer adapts to a long and thin type desulphurization molten iron ladle and meets the current desulphurization process requirements of stirring and injection.
Owner:WUHAN UNIV OF SCI & TECH

Anode rotary vacuum plating device based on PLC (Programmable Logic Controller) control

The invention relates to an anode rotary vacuum plating device based on PLC (Programmable Logic Controller) control. A plating tank of the anode rotary vacuum plating device based on PLC control is placed in a vacuum box, a cathode is placed in the plating tank, a binding post of the cathode is welded on the upper surface of the cathode, an anode is inserted into the cathode and is connected with a motor through a clamping and fixing device, a carbon brush of an anode connecting device is propped against the anode, a plurality of wiring holes are formed in the vacuum box, a wiring sealing block is arranged in each wiring hole, an external electrode wire of the anode is connected with the positive pole of a pulse electroplating power supply through the corresponding wiring sealing block, an external electrode wire of the cathode is connected with the negative pole of the pulse electroplating power supply through the corresponding wiring sealing block, and two external electrode wires of a motor are connected with a PLC through the corresponding wiring sealing blocks respectively. The anode rotary vacuum plating device based on PLC control solves the problem of difficulty in electroplating of negative plating parts having large sizes or complicated structures is solved, and the operation difficulty is lowered.
Owner:JINING XINRUIDA INFORMATION TECH CO LTD

Slurry pump cylinder sleeve internal surface electroplating restoration anode rotation vibrating apparatus

The invention relates to a slurry pump cylinder sleeve internal surface electroplating restoration anode rotation vibrating apparatus. The slurry pump cylinder sleeve internal surface electroplating restoration anode rotation vibrating apparatus comprises a support, a vibration beam, an electromagnet, a spring, an anode rotation device, a plating bath and a programmable logic controller (PLC), one end of the vibration beam is movably connected with the support through a pin, the spring is arranged between the vibration beam and a support crossbeam at the upper portion of the vibration beam, the lower end surface of the vibration beam is fixedly provided with a contact, the electromagnet is arranged just below the contact, the lower end surface of the vibration beam is also fixedly provided with a suspension block, the lower portion of the suspension block is provided with an inverted-U-shaped hole, a suspension rope traverses through the inverted-U-shaped hole and then is fixedly connected with the motor of the anode rotation device, the anode rotation device is connected with anode nickel, a cylindrical roller bearing is arranged outside the anode nickel, a terminal is welded outside the cylindrical roller bearing, the anode nickel is inserted into a cathode slurry pump cylinder sleeve, and the cathode slurry pump cylinder sleeve is placed in the plating bath; and the electromagnet and the motor are respectively connected with the programmable logic controller. The apparatus improves a concentration polarization phenomenon and improves the compactness of a plating layer through realizing automatic control of electroplating restoration.
Owner:海宁市黄湾镇资产经营有限公司

Treatment method applied to chemical industrial wastewater

The invention discloses a treatment method applied to chemical industrial wastewater. The treatment method comprises the following treatment steps of (a) chemical industrial wastewater pretreatment, (b) biochemical treatment of chemical industrial wastewater and (c) physical treatment of chemical industrial wastewater. According to the treatment method, the chemical industrial wastewater is sequentially subjected to the chemical industrial wastewater pretreatment, the biochemical treatment of chemical industrial wastewater and the physical treatment of chemical industrial wastewater, and the chemical industrial wastewater reaching the discharge standard is obtained. The treatment method is especially suitable for treatment of organic chemical industrial wastewater having strong biological toxicity and poor biochemical properties and can deeply treat chemical industrial wastewater, the harmful matter content in the treated wastewater is reduced to the most degree, the lower treatment degree is avoided, and accordingly the problem that treated wastewater still cause large environmental pollution is solved. In addition, in the wastewater treatment process, all links can be performed in order, the treatment method is simple in structure, scientific, convenient, strong in pertinence, high in automation degree, low in actural application cost, advanced in technology and good in treatment effect, and the chemical industrial wastewater treatment problem is well solved.
Owner:衢州市协成化工有限公司

Strengthening method for removing ammonia nitrogen and organic matters in rear activated carbon filter for ultrafiltration

The invention discloses a strengthening method for removing ammonia nitrogen and organic matters in a rear activated carbon filter for ultrafiltration, particularly discloses a strengthening method for removing ammonia nitrogen and organic matters in the rear activated carbon filter for ultrafiltration in drinking water treatment, and aims to solve the problem that the capacity of the activated carbon filter for removing the ammonia nitrogen and the organic matters is limited. The strengthening method comprises the steps of firstly, arranging a coagulation sedimentation unit in front of an activated carbon filter, and arranging an ultrafiltration unit at the rear of the activated carbon filter; then, adopting different strengthening measures according to different concentrations of ammonia nitrogen and organic matters in inlet water of the activated carbon filter. The method comprises the following concrete steps: (1) when the concentration of the ammonia nitrogen is less than 1.5mg / L and the index of potassium permanganate is less than 3mg / L, changing the activated carbon filter to be in an upward flowing way; (2) when the index of the potassium permanganate is greater than 3mg / L, additionally arranging an ozone unit in front of the activated carbon filter in the step (1); (3) when the concentration of the ammonia nitrogen is greater than 1.5mg / L, aerating at the bottom of the activated carbon filter in the step (1); (4) when the concentration of the ammonia nitrogen is greater than 1.5mg / L and the concentration of the permanganate is greater than 3mg / L, combining the step (2) and the step (3).
Owner:HARBIN INST OF TECH

A kind of method for preparing 2,5-dichloronitrobenzene by continuous nitration

ActiveCN106083596BOptimize process flowWith automatic separation functionNitro compound preparationThree stageNitration
The invention discloses a method for preparation of 2, 5-dichloronitrobenzene by continuous nitration. The method comprises the steps of: adopting three-stage kettle type continuous reaction, adding sulfuric acid, nitric acid and p-dichlorobenzene in an extraction kettle into a first stage nitrification kettle simultaneously to carry out nitrification reaction, letting nitrification liquid enter a next stage nitrification kettle through self-carried raisers of all nitrification kettles in order to react, at the end of reaction in a third stage nitrification kettle, separating an oil phase and an acid phase, carrying out neutralization, washing and dehydration on the oil phase so as to obtain 2, 5-dichloronitrobenzene, internally recycling part of waste acid in the acid phase back to the first stage nitrification kettle, letting the residual waste acid enter an extraction kettle, and performing p-dichlorobenzene extraction, and then conducting separation to obtain acidic p-dichlorobenzene and extracted waste acid, concentrating the extracted waste acid into concentrated sulfuric acid, and making the concentrated sulfuric acid and acidic p-dichlorobenzene enter the first stage nitrification kettle for recycling. The method provided by the invention adopts automation control, cancels a mixed acid preparation procedure, simplifies the technological process, can realize continuous nitrification reaction, continuous nitrification liquid separation and continuous waste acid extraction.
Owner:江苏拓孚工程设计研究有限公司

Novel industrial wastewater treatment equipment

The invention discloses novel industrial wastewater treatment equipment. The novel industrial wastewater treatment equipment structurally comprises an equipment main body, a water inlet pipe, a motor,a control box, a water pipe structure, an adsorption precipitation device, a plug-flow aeration device and a temperature induction connection mechanism, wherein the water inlet pipe is vertically connected to the rearmost part of an upper end surface of the equipment main body; the adsorption precipitation device vertically penetrates through the leftmost part of an inner cavity of the equipmentmain body and is interpenetrated with the inner part of the water inlet pipe; the left half part of the plug-flow aeration device is mechanically connected to the middle part of an inner bottom surface of the adsorption precipitation device. According to the novel industrial wastewater treatment equipment disclosed by the invention, parts including the plug-flow aeration device, the temperature induction connection mechanism and the like are mutually matched, so that the temperature of industrial wastewater flowing through an adsorption precipitation part of the equipment can be detected in anindustrial wastewater treatment process, and mass transferring conditions of pollutants in a water treatment process are enhanced; a condition that water temperature is too high so that the activityof sludge is influenced is avoided; the industrial wastewater treatment effect of the equipment is ensured and the stable performance of the equipment is effectively improved.
Owner:泉州市西决三维科技有限公司

Method for treating vanadium-containing waste catalyst

The invention provides a method for treating a vanadium-containing waste catalyst. The method comprises the following steps of, A) carrying out ball-milling on the deoiled waste catalyst to obtain a powdery waste catalyst; B) mixing the powdery waste catalyst to obtain a mixed material; C) granulating the mixed material, and drying to obtain mixed material particles; and D) cooling and solidifying the mixed material particles, and roasting in a fluidized bed furnace to obtain sodium modified clinker. According to the method, sodium salt roasting in the fluidized bed furnace is realized, the contact between a sodium salt additive and the vanadium-containing waste catalyst and the contact between cold solid particles and air are strengthened, the chemical reaction kinetic conditions of sodium salt roasting are improved, the leaching rate of vanadium in the sodium salt clinker is increased, and the vanadium leaching rate of the sodium salt clinker can reach 95% or above; the problems that the temperature of a rotary kiln is not easy to control and the rotary kiln is easy to knot are solved, and organization and implementation of production are facilitated; and during sodium salt roasting, self-heating generated by oxidation of carbon and sulfur in the waste catalyst is utilized, so that the production cost is reduced.
Owner:BEIJING PRUDENT CENTURY TECH CO LTD +2

Downward flow type denitrification and phosphorous removal expanded bed biological filter and method for treating sewage by applying same

The invention discloses a downward flow type denitrification and phosphorous removal expanded bed biological filter and a method for treating sewage by applying the same. The downward flow type denitrification and phosphorous removal expanded bed biological filter comprises a water distribution region, a filter screen plate, a floating ceramsite filter bed, a filter bed fluidization and buffering region, a filter-head filter plate, a water outlet region, a bottom water collection and gas distribution device and a water collection and gas distribution channel box, wherein the floating ceramsite filter bed is composed of crushed shale floating ceramsite arranged between the filter screen plate and the filter-head filter plate; the crushed shale floating ceramsite has an irregular shape and the density of water wetted particles is 0.95g/cm<3>+/-0.5g/cm<3>; shale ceramsite is coarse and hydrophilic so that biofilm colonization is easy to realize; backwashing is adopted so that the activity of a biofilm is easy to maintain, the de-mold is not liable to occur and a denitrification biological nitrogen removal function is prominent; after sewage is subjected to primary micro-flocculation in the water distribution region, phosphorous-containing floc has a deep penetration distance in an expanded filter bed gap and a phosphorous removal effect is facilitated; the crushed ceramsite and the relatively large filter bed depth ensure the phosphorous removal and filtering capability. By adopting the downward flow type denitrification and phosphorous removal expanded bed biological filter, the loss of a filtering water head of an expanded bed is small and a filtering material is easy to fluidize and is not hardened.
Owner:SOUTH CHINA UNIV OF TECH

A wood-based panel waste water treatment system and process

The invention provides an artificial board wastewater treatment system and technology. The artificial board wastewater treatment system comprises a physical-chemical separating tank, a water collecting and regulating tank, an air flotation reaction tank, a water distributing trough, an anaerobic fluidization bed, a hydrolysis fluidization bed, an aerobic fluidization bed, a coagulation reaction tank, a micro-filtering device, an O3 oxidation column, a clear water tank and an accident tank, wherein the machine is characterized in that three grade biological fluidization beds of the anaerobic fluidization bed, the hydrolysis fluidization bed and the aerobic fluidization bed are combined to perform biological wastewater treatment. Compared with the conventional artificial board wastewater treatment technology by using a fixing bed and an activated sludge system, the machine disclosed by the invention is adopted for treating artificial board waste water by designing the technological parameters of relevant working procedures, and the machine has unique advantages in the aspects of treating organic waste water which is high in concentration and difficult to degrade. Key equipment of the system is small in volume, the whole system has stronger resistance to impact load, the sludge is sufficiently degraded, and the problem of sludge bulking is solved.
Owner:NANNING JINKE ENVIRONMENTAL ENG
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