52results about How to "Increase the pressing density" patented technology

The invention discloses a preparation method of FeSi alloy powder with high direct current superposition characteristics, and belongs to the technical field of alloy powder preparation. The FeSi alloypowder is mainly made of pure iron and metal silicon, and a small amount of manganese and chromium are added. The preparation method comprises the following steps of weighing the ingredients according to a specific proportion, carrying out non-vacuum melting to obtain the alloy melt of required components, and then atomizing to prepare alloy raw powder with an inert gas, obtaining fine powder after the raw powder is collected, screened and graded. According to the preparation method of FeSi alloy powder with high direct-current superposition characteristics, the alloy powder with uniform components and high purity can be obtained, and the powder spherical degree is high; the uniform and compact insulating layer can be easily formed after insulation coating, so that the contact of the alloy matrix is effectively blocked, and the pressed magnetic powder core has good direct-current superposition characteristics.

The invention discloses a ceramic thin plate manufacturing method. The method comprises the following steps of: (1) adding water and gluewater for wetly grinding mixed materials, and then preparing the mixed materials to mud pies, wherein the mixed materials comprise mineral fiber, clay and soapstone; (2) pressing the mud pies to a mud plate by adopting a cylinder ejection manner, and then pressing the mud plate for molding a mud blank; (3) drying the mud blank by adopting a microwave manner, and then cutting the mud blank into brick blanks; (4) glazing the brick blanks; (5) printing the glazed brick blanks; (6) heating for drying the glazed and printed brick blanks; (7) firing the glazed and printed brick blanks to semi-finished products at the high temperature in a kiln; and (8) polishing and edging the semi-finished products to obtain ceramic thin plates. By utilizing the ceramic thin plate manufacturing method, deformation of the brick blanks in the subsequent firing process can be avoided, the biscuit firing section is omitted, the energy consumption is reduced, the product water absorption is low, the product cost is reduced, and the product has high cost performance and strong international competitiveness.

The invention discloses a high-performance powder metallurgy material and a preparation method thereof, components of the powder metallurgy material are Fe, Cr, Cu and C; components and contents thereof for preparing the powder metallurgy material are as follows (by weight percent): 0.35 to 0.5 percent of C, 1.3 to 1.5 percent of Cu, 0.6 to 1.0 percent of Cr, 0.6 percent of hard acid zinc 135, and the balance of Fe, wherein the Cr is added in the form of ferrochrome, the adopted ferrochrome is micro-carbon ferrochrome, and the ferrochrome contains 50 percent of chromium, 0.06 percent of carbon, and the balance of Fe; the hard acid zinc 135 is a lubricant; the powder mixing method of the powder metallurgy material is that the ferrochrome is first subjected to high-energy ball milling until particle diameter thereof is within the range of 0.3 to 1 Mum, and then the powder metallurgy material is mixed with other powder evenly; the pressing and sintering method of the powder metallurgy material is that cold pressing is conducted to powder mixed according to a proportion, with the pressure of 600MPa and the pressurizing speed of 150mm/min, and the powder is molded at 600MPa and then kept for 2min; and the sintering is conducted in dissociated ammonia protective atmosphere, with the temperature of 1120 DEG C, and the sintering time of 40min.

The invention relates to a production method of a hot-pressing carbon graphite material, and is characterized by comprising the following steps of: stirring phenolic resins, 99% alcohol, urotropine and oleic acid into a stirring kettle to prepare phenolic resin adhesive mixing solution; adding graphite powder, carbon black powder, pitch coke powder and needle type coke powder into a kneading kettle, mixing and kneading, heating, adding the phenolic resin adhesive mixing solution, stirring and mixing to obtain a clinker; cooling the clinker, grinding powder, pressing and molding, forming and mold pressing, forming and processing, removing burr and fin, cleaning, and drying or blowing to a finished product through hot blast. According to the invention, by adopting a two-section pressing method, porosity in a press is reduced, the pressed density is improved, the intensity and the wear resistance of a product are improved, materials and air holes are uniformly distributed, creep property of the finished product is reduced, the product has small deformation in a production process, and the precision of the product is improved, by adopting an advance mixing and kneading process, the amount of the resins is reduced, and the heat conductivity of the product is improved, so that the quality grade of the hot-pressing carbon graphite material product is improved, thus the hot-pressing carbon graphite material product has wider purposes.

The invention discloses a method for manufacturing a dry-pressing heterosexual permanent-magnetic material, and belongs to the technical field of a permanent-magnetic material. The method comprises the following steps: crushing a pre-sintering material into crude powder, adding a quadratic formula formed by silicon dioxide and a boric acid to the crude powder and then carrying out ball-milling; scattering the slurry obtained in a ball-milling manner after baking; adding 0.1-3.0% of calcium carbonate according to the weight percent and then agitating and vibration and milling by a blender mixer to obtain mixed powder; adding allocated quantity of camphor powder and calcium stearate to the mixed powder, and then crushing at a high speed, so as to prepare the dry-pressing magnetic powder. Even dispersion can be ensured by adding the calcium carbonate after drying of fine powder is finished, and adhesion of particles is not generated. Therefore, the pressing density of a magnetic body and the control range of the drying temperature range can be improved, and meanwhile, birdnesting is opened as much as possible by a vibration and milling process. Thus, birdnesting between particles is reduced, meanwhile, a corner angle is removed, the prepared permanent-magnetic material has good orientation degree and density, and the performance is significantly improved.

The invention relates to a high-performance powder metallurgy material, wherein components of the powder metallurgy material are iron powder, aluminum powder, chromium iron, zinc stearate and graphite powder; a manufacturing method of the high-performance powder metallurgy material comprises the steps of ball-grinding the chromium iron till the particle diameter is 0.3-1 microns; uniformly mixing with other powders according to the proportion; performing ball-grinding in a high-performance ball grinder for 5-15 min, wherein the ball-grinding medium is anhydrous organic liquid; in the invention, Al is added in the main component, so that the performance of the powder metallurgy material is improved; the indoor bending strength is 2500 MPa and the relative density is more than 99.9%; high pressing density can be obtained after cold-pressing (pre-pressing) is maintained for a certain time; the prepared sintered steel has a uniform texture, high strength and plasticity, excellent performances and low cost.

The invention discloses a warm-pressing process of powder metallurgy. The warm-pressing process comprises the following steps of: a, weighing an alloy powder raw material, a lubricating agent and an additive; mixing the alloy powder, the lubricating agent and the additive in a weight ratio of (10-30): 1: 1 to form a mixed material; b, pressing the mixed material into a pre-formed blank; carrying out warm-pressing treatment on the pre-formed blank; controlling the temperature to 130-150 DEG C and controlling the time to 10-12 hours, wherein the pressing density of warm-pressing forming treatment is 7.5-8g/cm<3>; putting into a furnace to be sintered, wherein the sintering temperature is 1200-1400 DEG C; c, de-burring the sintered pre-formed blank; cutting and machining to form a rough product; and d, carrying out immersing treatment on the rough product; and carrying out surface steam treatment at the temperature of 420-550 DEG C to obtain a finished-product part. The process disclosed by the invention has simple steps; the pressing density is improved by adopting a warm-pressing forming treatment process and the cost of the warm-pressing process is only 1.25; the surface smoothness is good and the sintering shrinking percentage is small; and the yielding strength and the impacting toughness are better than those of a traditional process.

Pressureless sintering silicon carbide comprises the following components by mass: 80% to 90% of silicon carbide, 6% to 9% of resin, 0.5% to 0.8% of boron carbide, and the balance release agent. The preparation process for processing the pressureless sintering silicon carbide includes first stirring raw materials for 15 to 25 hours through a powder mixing machine to completely mix the raw materials, conducting spraying pelleting on the raw materials in the material mixing machine, forming powder materials after pelleting in press mode through a press, then filling the powder materials into a sintering furnace, conducting vacuumizing to -0.01MPA, stopping vacuumizing when the temperature rises to 1200 DEG C, filling argon into the sintering furnace to the normal pressure, then enabling temperature to rise to 1800 DEG C, keeping warm for 30 minutes, then continuously enabling the temperature to rise to the range from 2150 DEG C to 2200 DEG C, keeping warm for 30 to 50 minutes and enabling the powder materials to be naturally cooled. Due to the fact that fine powder materials are selected, compression density of product green bodies is improved, resin content is adjusted, the silicon carbide powder materials can conduct chemical reaction more fully in the sintering process, the density can reach 3.18g/cm<3>, and the hardness can reach 2400 HV0.5. The pressureless sintering silicon carbide has better abrasion resistance due to the fact that the density, the hardness and the compression strength are all improved.

Aspects of the invention are based on the discovery that cathode materials and lithium ion batteries comprising the cathode material, having improved thermal stability may be produced from a cathode material that is comprised of a mixture of a lithium metal oxide and a lithium metal phosphate wherein the lithium metal phosphate comprises a volume fraction of secondary particles having a size of 0.1 to 3 μm that is from 5 to 100%, based on the total content of lithium metal phosphate. More specifically cathodes comprising lithium metal phosphates having the recited secondary particle ranges help provide cathode materials that are capable of passing the nail penetration test without generating smoke or flames. Methods of forming the cathode and lithium ion battery comprising the cathode are also provided.

The invention discloses a wireless charging magnetic core for an intelligent watch and a preparation method thereof. Raw materials of the wireless charging magnetic core comprise a main component andan additive, the main component comprises 51.5 to 53.5% Fe2O3, 9.0 to 12.5% ZnO by mole percent, and the balance is MnO; and the additive comprises 100-600 ppm V2O5, 0-200 ppm MoO3, 2000-4500 ppm Co2O3, 100-1000 ppm CaCO3, and 100-500 ppm Nb2O5. The preparation method adopts centrifugal granulation and adopts sealing molding during integral molding. According to the wireless charging magnetic core, types and dosage of main component and additive are reasonably selected, and centrifugal granulation and sealing molding are used. The prepared wireless charging magnetic core has high planar inductance and profiling inductance, low loss in a wide temperature range, sufficient strength and toughness to meet the requirements of use.

The invention belongs to the technical field of tantalum capacitor preparation and particularly relates to a preparation method of a high-voltage ultra-small-capacity non-solid electrolyte tantalum electrolytic capacitor. The method is characterized in that pressing density is improved, a molding mode is changed, the increasing sintering temperature and sintering time are increased, so the strength of a tantalum core is enhanced, tantalum cores are not easy to fall off and have unfilled corners, impurities in tantalum powder are effectively removed, a tantalum core with excellent electrical performance is obtained through an improved forming method, aging process treatment is combined, so the voltage of the prepared non-solid electrolyte tantalum capacitor can reach 180V, the capacitance can reach 0.047 mu F, and the non-solid electrolyte tantalum capacitor has the characteristics of high voltage and ultra-small capacitance.

The invention discloses an automatic production process for soft magnetic manganese zinc ferrite granules and belongs to the technical field of production of soft magnetic manganese zinc ferrite granules. The process comprises the following steps: batch weighing, primary pulping and grinding, primary spray-drying, pre-sintering, secondary pulping and grinding and secondary spray-drying, adding a plasticizer before secondary spray-drying, uniformly stirring and mixing, and performing spray-drying, wherein the plasticizer refers to a phthalic ester plasticizer. With the adoption of the phthalic ester plasticizer, on one hand, the plasticity of the powder is enhanced, plastic deformation (crushing) of powdered granules is easily caused, and the pressed density of a magnetic core is improved. Under the same strength condition of the magnetic core, the molding pressure of the granules can be reduced from 34-36Mpa to 31-33Mpa, the wear rate of a press is reduced by 0.1-0.5%, and the service life of the mold is prolonged by 0.1-0.5%; and the layering phenomenon in the magnetic core pressing process is reduced, and the production efficiency and product quality of the magnetic core are improved.

The invention discloses an additive used for improving the stainless steel sintered density and a method for manufacturing a stainless steel sintered component with the additive. The additive is composed of low-melting-point ferroalloy powder, low-carbon organic acid matter and low-temperature lubricant. After the additive is added to stainless steel powder, the stainless steel powder is pressed under the pressure of 600-900 MPa, and the component is sintered at the temperature of 1200-1350 DEG C. Fast temperature-rising is adopted when the temperature-rising period is 600 DEG C or above, and the temperature-rising rate is 15-60 DEG C/min. The high-density stainless steel sintered component is obtained after sintering. Due to the fact that low-melting-point organic matter is added, when die pressing is conducted, part of liquid lubricant is generated and diffused to the die wall, so that die wall friction is reduced, and the pressing density of the stainless steel powder is well improved. The stainless steel powder is coated with the organic matter and activated before sintering (600-900 DEG C). Meanwhile, low-melting-point alloy is liquefied during sintering, so that a facilitating function is achieved on sintering of the stainless steel powder. The formula of the additive is scientific and reasonable, so that the pressing density of the stainless steel powder can be effectively improved, and a sintered product has higher density and mechanical performance.

The invention discloses a spheroidizing preparation method of crushed Fe-Si-Al magnetic powder, which belongs to the technical field of preparation of metal powder. The preparation method comprises the following operation steps of 1, carrying out ultrasonic cleaning on crushed Fe-Si-Al magnetic powder in an acetone solution, 2, adding the cleaned magnetic powder into a nitric acid aqueous solution for ultrasonic treatment, 3, carrying out sanding treatment on the acidified magnetic powder in a sand mill by adopting mixed zirconia grinding balls with three diameters, and 4, carrying out annealing treatment to obtain the spherical Fe-Si-Al magnetic powder with the median particle diameter of 40-70 microns. The tap density reaches 3.50 to 3.98 g/cm<3>. Compared with a common broken Fe-Si-Al powder core, the powder core prepared from the Fe-Si-Al magnetic powder as a raw material has the advantages that when the relative magnetic conductivity is 59.82-60.15, the density of the powder core reaches 5.90-6.02 g/cm<3>, meanwhile, the direct current bias performance of 100Oe reaches up to 52.85-55.73%, and the magnetic core loss of 50kHz/100mT is only 232.94-248.31 mW/cm<3>.

The invention relates to a preparation method of high-pressure blank strength tungsten powder, and aims to further improve the dependence of a preparation method of tungsten powder in the prior art on specific raw materials and further improve the blank strength of the tungsten powder. According to the method, the specific reduction technology in the tungsten powder preparation process is improved, the hydrogen flow and the gas inlet and outlet flow ratio of the first reduction process, the second reduction process and the third reduction process in the hydrogen reduction process are controlled, the reduction temperature and time are further controlled, and therefore the tungsten powder with the higher pressure blank strength is prepared. The preparation method of the tungsten powder with the high compact strength can be suitable for various wide tungsten oxide raw materials such as yellow tungsten, blue tungsten and purple tungsten, the tungsten powder with the compact strength larger than or equal to 4.7 MPa can be stably prepared without adopting special tungsten oxide raw materials, and the application market prospect is very wide.

A method for producing carbon powder having a defined carbon particle size distribution comprises the steps of:—a) selecting a carbon precursor powder of a defined precursor particle size distribution, the carbon precursor powder consisting of or comprising particles of one or more meltable carbon precursors; b) treating the carbon precursor powder to round at least some of the particles of the carbon precursor and thereby produce a rounded carbon precursor; and c) carbonizing the rounded carbon precursor; wherein the defined precursor particle size distribution is such that on carbonization the powder of defined carbon particle size distribution is produced.