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37results about How to "Shorten process operation time" patented technology

Manufacturing method of ice bag for preserving biological products

The invention discloses a manufacturing method of an ice bag for preserving biological products. The manufacturing method comprises the following steps: 1) adding a thickener into hot water or boiling water, and fully stirring till dissolution; 2) adding high molecular water-absorbing resin into a solution in the step 1) while hot, stirring, then standing to carry out full reaction and imbibition on the high molecular water-absorbing resin and the thickener, and forming a gelatinous solid, wherein the reaction time is 5-30minutes; and 3) bagging the gelatinous solid in the step 2), cooling, and then placing into a cold storage, a refrigerating cabinet or a refrigerator at the temperature of -10 DEG C to -20 DEG C for freezing for above 12hours. The invention provides a simple, convenient and high-efficient manufacturing method of a high molecular cold storage agent, namely the manufacturing method of the ice bag for preserving the biological products. The prepared cold storage agent has the advantages of high repeatability, great freezing-thawing phase change latent heat, long cold storage time and fast water absorption speed, and furthermore, the cost of the process is low; and by changing the added thickener, the different phase change temperatures can be obtained for meeting various different application requirements.
Owner:浙江赛灵特医药科技有限公司

Fe and mixed rare earth intermediate alloy for adding rare earth into steel and preparation method for Fe and mixed rare earth intermediate alloy

InactiveCN102383028AGood effectNew form of joiningCrucibleRare earth
The invention relates to a Fe and mixed rare earth intermediate alloy for adding rare earth into steel and a preparation method for the Fe and mixed rare earth intermediate alloy. The alloy is prepared by processing the following raw materials in percentage by weight: 70-95 percent of pure iron and 5-30 percent of mixed rare earth metal. The preparation method comprises the following steps of: performing vacuum melting in a vacuum medium frequency induction furnace crucible, wherein the vacuum degree is less than or equal to 0.1 Pa; and fully deoxidizing by using SiCaBa, and adding mixed rare earth metal into pure molten iron in the crucible when the temperature reaches 1,550-1,650 DEG C, wherein the melting and mixing time is 1-10 minutes. The invention has the advantages that: when the Fe and mixed rare earth intermediate alloy is used in a steel ladle, the rare earth adding effect is good, the rare earth adding form is novel and the rare earth can be added efficiently, the method is easy and convenient to operate, and equipment and operating workers are not added; the yield of the rare earth is greatly improved; the rare earth is uniformly distributed in molten steel; the rare earth adding amount is greatly reduced; the rare earth adding operating environment is effectively improved; the steel melting production efficiency is improved; the quality of the rare earth steel products is improved; and the comprehensive cost is reduced.
Owner:INNER MONGOLIA BAOTOU STEEL UNION

Fe-Ce intermediate alloy for adding rare earth into steel and preparation method for Fe-Ce intermediate alloy

InactiveCN102383029AGood effectNew form of joiningCrucibleRare earth
The invention relates to a Fe-Ce intermediate alloy for adding rare earth into steel and a preparation method for the Fe-Ce intermediate alloy. The alloy is prepared by processing raw materials with the weight percentages that: 70-95 percent of pure iron and 5-30 percent of metal Ce. The preparation method comprises the following steps of: performing vacuum melting in a vacuum medium frequency induction furnace crucible, wherein the vacuum degree is less than or equal to 0.1 Pa; and fully deoxidizing by using SiCaBa, and adding metal Ce into pure molten iron in the crucible when the temperature reaches 1550-1650 DEG C, wherein the melting and mixing time is 1-10 minutes. The invention has the advantages that: when the Fe-Ce intermediate alloy is used in a steel ladle, the rare earth adding effect is good, the rare earth adding form is novel and the rare earth can be added efficiently, the method is easy and convenient to operate, and equipment and operating workers are not added; the yield of the rare earth is greatly improved; the rare earth is uniformly distributed in molten steel; the rare earth adding amount is greatly reduced; the rare earth adding operating environment is effectively improved; the steel melting production efficiency is improved; the quality of the rare earth steel products is improved; and the comprehensive cost is reduced.
Owner:INNER MONGOLIA BAOTOU STEEL UNION

Preparation method of white fabric

The invention relates to a preparation method of a white fabric. The method is characterized by oxygen bleaching and whitening a fabric containing cotton, and comprises the steps of adding a one-bath-one-step method bleaching solution (prepared from 1 to 2g / L of penetrating agent, 1 to 2g / L of anti-creasing agent, 2 to 7 percent (owf) of scutching agent, 2 to 9 percent (owf) of 40 percent by weight caustic soda solution, and 3 to 6 percent (owf) of 30 percent by weight hydrogen peroxide solution) with pH being 10 to 11 into the fabric for oxygen bleaching, then adding a fluorescent whitening agent for whitening, heating at a constant heating rate to 80 to 90 DEG C, carrying out insulation treatment, and cleaning, neutralizing and setting to obtain the white fabric. According to the method,a step of removing hydrogen peroxide is saved, so that the process time can be greatly saved, the water consumption is reduced, and the emission of noxious substances is reduced; the prepared white fabric is free of acidity and less in storage color change, and has a pH value stabilized in an acceptability limit from 5.5 to 7.0, and the whiteness improved by 1 to 2 or more compared with a traditional process; when preparing the white fabric with the same whiteness, the dosage of the fluorescent whitening agent can be saved by 10 to 40 percent, so that the economic benefits of enterprises canbe greatly improved.
Owner:PACIFIC (PANYU) TEXTILES LTD

Lentivirus purification process

The invention discloses a lentivirus purification process. The lentivirus purification process comprises the following steps: S1, clarifying and filtering a lentivirus-containing cell culture to obtain a lentivirus-containing cell culture supernatant; S2, concentrating the supernatant obtained in the step S1 by 8-15 times by adopting a hollow fiber ultrafiltration system; S3, washing and filtering the concentrated solution obtained in the step S2 by at least 10 volumes by using a first buffer solution; S4, carrying out nuclease Benzonase enzyme digestion treatment on the concentrated solution washed and filtered in the step S3, and controlling the treatment temperature to be 25-37 DEG C and the treatment time to be 30-60 minutes; S5, washing and filtering the concentrated solution in the step S4 by at least 10 volumes through a hollow fiber ultrafiltration system so as to remove nuclease Benzonase and nucleic acid fragments, and then adding a second buffer solution into the concentrated solution, wherein the second buffer solution contains Buffer for maintaining the stability of lentivirus particles; and S6, concentrating the lentiviral vector concentrated solution obtained in the step S5 to 5*10<7> TU/mL or above to obtain the purified lentivirus. The lentivirus purification process disclosed by the invention can obviously improve the recovery rate of the lentivirus and is suitable for large-scale production.
Owner:PORTON BIOLOGICS LTD

A continuous ion exchange device and lithium extraction process for extracting lithium

The invention discloses a continuous ion exchanging device for extracting lithium and a lithium extraction process. The continuous ion exchanging device for extracting lithium comprises a running base and a plurality of adsorbing columns; the running base comprises an adsorption region, a drip washing region and a desorption region; the plurality of adsorbing columns are arranged on the running base and are distributed in the adsorption region, the drip washing region and the desorption region; the adsorbing columns in the adsorption region communicate with a raw material liquid charging pipe; the adsorbing columns in the drip washing region communicate with a drip washing liquid charging pipe; the adsorbing columns in the desorption region communicate with a desorption liquid charging pipe; and the positions of the absorption region, the drip washing region and the desorption region on the running base are successively replaced. The lithium extraction process adopts the continuous ion exchanging device; with the passage of time and the operation of the running base, the absorption region, the drip washing region and the desorption region on the running base separately implement adsorption operation, drip washing operation and desorption operation; all regions are continuously and alternately replaced so that the overall lithium extraction operation can be quickly and continuously implemented, and thus the lithium extraction efficiency and the comprehensive development and utilization efficiency of resources are improved.
Owner:QINGHAI SALT LAKE IND

Method of extracting gutta-percha through enzymolysis

Provided is a method of extracting gutta-percha through enzymolysis. One of natural eucommia skin or eucommia leaves or eucommia wing skin is placed in clean water to be cleaned and dried, and moisture content of the eucommia skin, the eucommia leaves, or the eucommia wing skin is enabled to be less than 5%. A compound enzyme which comprises, by mass, 0.27% of cellulose, 0.01% of pectinase, and 0.02% of protease is added, enzymolysis undergoes 1-3 days under stirring at a speed of 500 r / min under 50 DEG C. Mixture after the enzymolysis is filtered, dregs of the filtered mixture are sent to an ultrasonic extraction tank for ultrasound extraction, and glue mixed liquor is produced. The glue mixed liquor is filtered in a grading mode, impurities are eliminated, and the glue mixed liquor with the impurities eliminated is sent to a separation tank. Eventually the gutta-percha is extracted through the method that gutta-percha crystals are precipitated at a low temperature. The method is simple in process, little in pollution, high in yield rate, low in cost, and ideal in effect; the extraction rate reaches more than 95%, and the gutta-percha content reaches 99.9%; and the produced gutta-percha is long in gelatin silk, high in tensile and tearing-proofing physical strength, and capable of being applied to wide fields.
Owner:HENAN HENGRUIYUAN IND

Device and method for rapidly preparing high-yield activated carbon by coupling of pressure pump with microwaves

The invention belongs to the technical field of carbon material preparation and provides a device and a method for rapidly preparing high-yield activated carbon by coupling of a pressure pump with microwaves. The device comprises a programmed controller, a feed unit, a reaction furnace, a pressure pump unit, a microwave heating unit, an explosive spraying and cooling unit and a pyrolysis gas treating unit. Friction and collision of raw material molecules are caused by the microwaves, reaction activation energy is reduced, and the process operation time is shortened greatly. Retention time of volatile matter is prolonged by pressing of the pressure pump, the volatile matter is promoted to be deposited on surface of semi-coke, and accordingly, yield of solid carbon is increased; condensationpolymerization of tar is also promoted by pressing, and production of the tar is reduced substantially or avoided. Besides, pyrolysis gas can be produced from inside of the raw materials by the aid of microwave heating, pyrolysis gas molecules retain in the raw material molecules under the pressing action to play a role of in-situ self-template and shuttle back and forth freely in the raw materials non-directionally to substantially promote pore development of the activated carbon, the instantaneous popcorn effect is beneficial to secondary pore forming of the pyrolysis gas, and the specificsurface area of a carbon material is increased.
Owner:DALIAN UNIV OF TECH

A kind of preparation method of reactive gemini quaternary ammonium salt leather fungicide

The invention discloses a preparation method of a reactive gemini quaternary ammonium salt leather bactericide. The preparation method comprises the following three steps: first step, carrying out esterification reaction on bromoacetyl bromide and fatty alcohol to generate bromine acetate; second step, carrying out nucleophilic substitution on trans-1,4-dichloro-2-butene and diethylamine to generate trans-N,N,N',N'-tetraethyl-2-butene-1,4-diamine; and third step, carrying out quaterisation on products obtained from the first two steps to obtain a reactive gemini quaternary ammonium salt. The preparation method is easy to operate, the yield of products is high, the cost of raw materials is low, the practicality is high, and moreover, a method for synthesizing diamine intermediate in the second step provides a new thinking and new method for synthesis of the gemini quaternary ammonium salt. Owing to existing of prepared bactericide molecular structure ester groups, the sterilizing property is improved, and biodegradability can be good. In addition, owing to existing of active groups C=C in the structure, the chemical activity of the gemini quaternary ammonium salt is improved, the gemini quaternary ammonium salt can be further chemically bounded into skin collagen and leather coating resin materials, and the long-lasting sterilizing property can be achieved.
Owner:SICHUAN UNIV

Manufacturing method of ice pack for preserving biological products

The invention discloses a manufacturing method of an ice bag for preserving biological products. The manufacturing method comprises the following steps: 1) adding a thickener into hot water or boiling water, and fully stirring till dissolution; 2) adding high molecular water-absorbing resin into a solution in the step 1) while hot, stirring, then standing to carry out full reaction and imbibition on the high molecular water-absorbing resin and the thickener, and forming a gelatinous solid, wherein the reaction time is 5-30minutes; and 3) bagging the gelatinous solid in the step 2), cooling, and then placing into a cold storage, a refrigerating cabinet or a refrigerator at the temperature of -10 DEG C to -20 DEG C for freezing for above 12hours. The invention provides a simple, convenient and high-efficient manufacturing method of a high molecular cold storage agent, namely the manufacturing method of the ice bag for preserving the biological products. The prepared cold storage agent has the advantages of high repeatability, great freezing-thawing phase change latent heat, long cold storage time and fast water absorption speed, and furthermore, the cost of the process is low; and by changing the added thickener, the different phase change temperatures can be obtained for meeting various different application requirements.
Owner:浙江赛灵特医药科技有限公司

A process for preparing aluminum-silicon solution by dissolution of laterite nickel ore smelting slag

The invention belongs to the technical fields of environment and materials and relates to a process method for preparing an aluminum-silicon solution by taking smelting slags of laterite-nickel ores as raw materials. The process method comprises the following steps: performing alkali fusion on metallurgy waste residues of the laterite-nickel ores, intensifying a water logging process with ultrasound and adding Al(OH)3 as an aluminum source for adjusting the silicon-aluminum molar ratio to obtain a water-slag mixed crude aluminum-silicon dissolution solution; performing extraction filtration and liquid-solid separation to obtain the aluminum-silicon solution and solid-state filter residues at a certain molar ratio respectively. The process method has the benefits that the recovery rates ofSi and Al are increased by 44% and 65% respectively, and the particle size of filter residue particles treated by the ultrasound is smaller than that of the particles that are not treated by the ultrasound and are stirred mechanically, so that valuable metals, namely aluminum and silicon, in the laterite-nickel ores can be fully dissolved out and recycled; through independent or combined use of the ultrasound and the intensifying of the water logging process with the ultrasound, and a method for adjusting the silicon-aluminum molar ratio in the solution by effectively utilizing a low-valence aluminum source, the resources of the metallurgy waste residues of the laterite-nickel ores are utilized efficiently at low cost, the harm to the ecological environment is reduced, and the economic andenvironmental benefits of a process technology of comprehensive utilization of the metallurgy waste residues of the laterite-nickel ores are improved.
Owner:UNIV OF SCI & TECH BEIJING

A kind of preparation method of white fabric

The invention relates to a preparation method of a white fabric. The method is characterized by oxygen bleaching and whitening a fabric containing cotton, and comprises the steps of adding a one-bath-one-step method bleaching solution (prepared from 1 to 2g / L of penetrating agent, 1 to 2g / L of anti-creasing agent, 2 to 7 percent (owf) of scutching agent, 2 to 9 percent (owf) of 40 percent by weight caustic soda solution, and 3 to 6 percent (owf) of 30 percent by weight hydrogen peroxide solution) with pH being 10 to 11 into the fabric for oxygen bleaching, then adding a fluorescent whitening agent for whitening, heating at a constant heating rate to 80 to 90 DEG C, carrying out insulation treatment, and cleaning, neutralizing and setting to obtain the white fabric. According to the method,a step of removing hydrogen peroxide is saved, so that the process time can be greatly saved, the water consumption is reduced, and the emission of noxious substances is reduced; the prepared white fabric is free of acidity and less in storage color change, and has a pH value stabilized in an acceptability limit from 5.5 to 7.0, and the whiteness improved by 1 to 2 or more compared with a traditional process; when preparing the white fabric with the same whiteness, the dosage of the fluorescent whitening agent can be saved by 10 to 40 percent, so that the economic benefits of enterprises canbe greatly improved.
Owner:PACIFIC (PANYU) TEXTILES LTD

Method for preparing low-temperature-resistant palm oil with high iodine value

The invention relates to a method for preparing low-temperature-resistant palm oil with high iodine value. The method comprises the following steps: (1) heating palm oil with iodine value higher than 60 at a temperature of 60-80 DEG C while stirring to completely dissolve the palm oil, then, cooling to minus 10 to 0 DEG C, and maintaining the temperature; heating up to 3-6 DEG C and maintaining the temperature; cooling to 4-8 DEG C and maintaining the temperature; and (2) transferring the palm oil obtained in the step (1) into separation equipment, centrifugally separating the palm oil at minus 15 to minus 5 DEG C until the grease is divided into a solid phase and a liquid phase, and extracting the liquid phase to obtain a palm oil product. The method for preparing low-temperature-resistant palm oil with high iodine value provided by the invention can be used for obtaining low-temperature-resistant palm oil product with iodine value higher than 75. Since such novel substances as a crystallization inhibitor, a crystallization solvent and the like are not introduced into the method provided by the invention, the separation efficiency and the separation effect are improved and the operation time of the process is greatly shortened; and no wastewater is generated in the process, the safety is good, the energy consumption in the process is low and the quality of the final product is good, so that the application prospect is wide.
Owner:TIANJIN UNIV
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