39 results about "Electron energy spectrum" patented technology

To provide a photoresponsive material that solves at least one of the problems of conventional technology. [Solution] The material has a crystalline structure formed by crosslinking at least one lanthanide with an organic group having 1 to 3 carbon atoms, wherein the organic group contains at least carbon atoms which may be partially or entirely substituted with other nonmetallic carbon group elements, and oxygen atoms which may be partially or entirely substituted with other nonmetallic oxygen group elements. A photoresponsive material having a peak component in the range of 533 eV to 534 eV in the O1s spectrum obtained by hard X-ray photoelectron spectroscopy.

The present invention relates to a solid electrolyte comprising: a sulfide-based lithium ion conductive compound; and a coating layer surrounding the entire surface of the sulfide-based lithium ion conductive compound in the form of a thin film and containing an aluminum compound, wherein, in X-ray photoelectron spectroscopy (XPS) analysis, a first peak appears in a region with a binding energy of 73 to 74 eV and a second peak appears in a region with a binding energy of 75 to 76 eV.

A silicon-carbon composite material, a negative electrode sheet, and a secondary battery. The silicon-carbon composite material comprises elemental silicon and silicon nitride. The silicon-carbon composite material satisfies: 2≤α≤3, wherein the value of α represents the peak intensity ratio of ISi2p to IN1s, and ISi2p and IN1s are respectively the intensities of the characteristic peaks of the silicon-carbon composite material at 103±0.5 eV and 399±0.5 eV in an X-ray photoelectron spectrum. The silicon-carbon composite material has a relatively high specific capacity, and can also achieve good rate capability, cycling performance and expansion performance.

A positive electrode active material for lithium-ion secondary batteries that offers high capacity and excellent charge-discharge cycle characteristics. provide. [Solution] A device containing lithium, cobalt, magnesium, oxygen, and fluorine, C Rietveld analysis was performed on the patterns obtained by powder X-ray diffraction using uKα1 rays. When this occurs, the crystal structure has a space group of R-3m, and the lattice constant of the a-axis is 2.814. Greater than ×10⁻¹⁰ m and less than 2.817 × 10⁻¹⁰ m, and c-axis The lattice constant is greater than 14.05 × 10⁻¹⁰ m, which is 14.07 × 10⁻¹⁰. When m is smaller and analyzed by X-ray photoelectron spectroscopy, the magnesium concentration when the cobalt concentration is set to 1 is... The positive electrode active material has a relative um concentration of 1.6 to 6.0.

This invention relates to the field of nanomaterials, specifically to a metal-organic framework composite material, its preparation method, applications, and a method for oxidative removal of organic sulfur from fuel oil. The composite material comprises Ce-MOF nanomaterials and MnO2 nanomaterials, wherein the weight ratio of MnO2 nanomaterials to Ce-MOF nanomaterials is 1:(13-15). In the X-ray photoelectron spectrum of the composite material, a characteristic peak exists at 530 eV for the O 1s spectrum. The composite material of this invention exhibits good synergistic effects between MnO2 nanomaterials and Ce-MOF nanomaterials, demonstrating excellent catalytic activity and stability.

The positive electrode active material of the present invention comprises lithium nickel-based oxide particles in the form of single particles consisting of a single nodule or pseudo-single particles as a complex of 30 or fewer nodules, and a coating containing cobalt formed on the surface of the lithium nickel-based oxide particles, wherein, when the positive electrode active material is analyzed by X-ray photoelectron spectroscopy (XPS), the XPS (Co / Ni) atomic ratio of Co to Ni is 0.15 or more, when the positive electrode active material is analyzed by Auger electron spectroscopy (AES), the standard deviation of the AES (Co / Ni) atomic ratio of Co to Ni is 0.80 or less, and the residual Li2CO3 content of the positive electrode active material is 0.50% by weight or less.

The present invention relates to colloidal silica useful as abrasive particles. Specifically, the colloidal silica has a first peak at 533 ± 0.5 eV and a second peak at 534 ± 0.5 eV in a spectrum obtained by X-ray photoelectron spectroscopy (XPS), the first peak having an intensity greater than that of the second peak, and has a first scattering peak at 465 ± 35 cm-1 and a second scattering peak due to amorphous silica at 1360 ± 30 cm-1 in a spectrum obtained by Raman spectroscopy.

The present invention relates to a coated positive electrode active material, having a composition comprising Li, M, and O, wherein M comprises: Ni in a content x, wherein 40 at% ≤ x < 100 at%, relative to M; Mn in a content y, wherein 0 at% < y ≤ 35 at%; Co in a content z, wherein 0 at% < z ≤ 30 at%; D in a content d, wherein 0.0 at% ≤ a d ≤ 2 5.0 at%, wherein D is at least one element selected from Al, B, Co, Cu, Mn, Mo, Sr, Ti, V, W, Y, Zn and Zr; and coating element Si in a content b, wherein 0.000 at% < b ≤ 2.000 at%, and coating element P in a content c, wherein 0.000 at% < c ≤ 2.000 at%; and having a content SiXPS such that the ratio SiXPS / b ranges from 90 to 340, and having a content PXPS such that the ratio PXPS / c ranges from 45 to 250, wherein PXPS and SiXPS are respectively contents of P and Si in at% relative to M measured by X-ray Photoelectron Spectroscopy XPS.

This application discloses a method and system for assessing displacement damage of solar panels in a space environment, enabling rapid assessment of spatial displacement damage to solar panels in space and improving accuracy and practicality. The method includes: acquiring basic energy spectrum data; performing energy spectrum fitting on the electron and proton energy spectra in the basic energy spectrum data to generate electron and proton energy flux curves; establishing a first model based on the structure of the solar panel; simulating multiple transmission energy spectra of electrons and protons with different incident thicknesses on upper and lower glass cover sheets based on the first model and the electron and proton energy flux curves, and generating an energy spectrum database; and generating assessment results of the displacement damage of the solar panel under space environment based on assessment commands and the energy spectrum database.

To provide a gas barrier film that has good and stable water vapor barrier properties while incorporating a gas barrier layer containing silicon dioxide. [Solution] The gas barrier film according to the present invention comprises a substrate layer and a gas barrier layer made of an inorganic oxide containing Si, Bi, and O, provided on one or both sides of the substrate layer, wherein the surface of the gas barrier layer is measured by X-ray photoelectron spectroscopy, and Si 2p Peak, Bi 4f7 / 2 Peak and O 1s The Bi / (Si+Bi) ratio, calculated using the peak area intensity, is between 0.10 and 0.80, and the O / (Si+Bi) ratio is between 1.00 and 1.80.

To provide a gas barrier film that has good and stable water vapor barrier properties while incorporating a gas barrier layer containing silicon dioxide. [Solution] The gas barrier film according to the present invention comprises a substrate layer and a gas barrier layer made of an inorganic oxide containing Si, Ga, and O, provided on one or both sides of the substrate layer, wherein the surface of the gas barrier layer is measured by X-ray photoelectron spectroscopy, and Si 2p Peak, Ga 3d Peak and O 1s The Ga / (Si+Ga) ratio, calculated using the peak area intensity, is between 0.05 and 0.80, and the O / (Si+Ga) ratio is between 1.00 and 1.80.

The present invention provides a carbon catalyst, an electrode, and a cell that combine high catalytic activity and high durability. The carbon catalyst has an L / La ratio of 18 or more, which is the ratio of the average carbon network plane size L obtained by temperature-induced desorption analysis capable of raising the temperature up to 1,600° to the crystallite size La obtained from a diffraction peak where the diffraction angle (2θ) in the X-ray diffraction pattern obtained by powder X-ray diffraction using CuKα rays is around 43°, and a ratio of the halogen atom concentration (atomic%) to the carbon atom concentration (atomic%) obtained by X-ray photoelectron spectroscopy is 0.0005 or more.

This invention relates to the field of carbon capture material preparation technology, and specifically discloses a calcium silicate material for carbon capture. The calcium silicate material is a microsphere structure assembled from nanosheets, with a diameter of 1 μm to 10 μm and a thickness of 10 nm to 50 nm. The molar ratio of calcium to silicon in the calcium silicate material is 1.5:1 to 2.2:1, and the specific surface area is 50 m² / g to 300 m² / g. The surface of the calcium silicate material contains calcium carbonate nanodomains, and its X-ray photoelectron spectroscopy spectrum shows a C1s characteristic peak of carbonate ions at 289.5 eV ± 0.3 eV. This calcium silicate material for carbon capture exhibits excellent CO2 adsorption capacity under mild conditions, far superior to conventional particulate calcium silicate. Furthermore, the presence of calcium carbonate nanodomains on the material surface combines the high capacity of calcium silicate with the rapid kinetics of calcium carbonate to form a synergistic adsorption effect, significantly improving carbon capture performance.

The present invention provides a mask blank that has high light resistance to exposure light including wavelengths in the ultraviolet region, high chemical resistance, and can form a good transfer pattern. [Solution] A mask blank comprising a translucent substrate and a thin film for pattern formation provided on the main surface of the translucent substrate, wherein the thin film contains titanium, silicon, and nitrogen, and the photoelectron intensity at a binding energy of 455 eV in the Ti2p narrow spectrum obtained by analyzing the internal region of the thin film by X-ray photoelectron spectroscopy is P N The photoelectron intensity at a binding energy of 10² eV in the Si2p narrow spectrum is P S When P N / P S The relationship is greater than 1.18, the internal region is the region excluding the vicinity region on the translucent substrate side of the thin film and the surface region on the opposite side of the translucent substrate, and the nitrogen content in the internal region is 30 atomic percent or more.

A protective layer (5) is formed of an inorganic material, and one surface of an electrode (1) in the thickness direction includes the protective layer (5). In the measurement of the atomic composition by Auger electron spectroscopy on one surface of the electrode (1) in the thickness direction, the proportion of elements derived from the inorganic material is 30 atom% or less.

A stretchable substrate having a first main surface and a second main surface facing opposite of each other, wherein the stretchable substrate satisfies at least one of (1) to (4): (1) at least either the first main surface or the second main surface has an oxygen atomic proportion of 5 at % or more with respect to all atoms as measured by X-ray photoelectron spectroscopy; (2) the first main surface or the second main surface has an arithmetic average surface roughness of 6 μm or more as measured with a laser microscope; (3) at least either the first main surface or the second main surface includes a metal-containing portion containing a metal atom; or (4) a metal-containing region containing a metal atom that is positioned along at least either the first main surface or the second main surface.

The application provides a negative electrode material and a battery, the negative electrode material comprising an inner core and a carbon layer on at least part of the surface of the inner core, wherein the inner core comprises graphite; the negative electrode material comprises a doping element, the mass percentage of the doping element being less than or equal to 1%; the doping element comprises P and O; the negative electrode material is tested by X-ray photoelectron spectroscopy analysis, and the negative electrode material has P-C chemical bonds and P-O chemical bonds; wherein the area ratio of the characteristic peaks of the P-C chemical bonds and the P-O chemical bonds is A, A=(25-65):(75-35). The negative electrode material provided by the application can comprehensively improve the reversible capacity, thermal stability and cycle performance of the negative electrode material.

A catalyst for a fuel cell, which includes a support and intermetallic compound particles supported on the support, wherein the intermetallic compound particles include a noble metal and a transition metal. There is a peak indicating a superlattice in a spectrum obtained by X-ray diffraction analysis, and a decrease in the position of the peak of the binding energy of the noble metal of the catalyst including the intermetallic compound particles is 0.1 eV or more based on the peak of the binding energy of the noble metal of the catalyst including irregular alloy particles of the same noble metal-transition metal component obtained by X-ray photoelectron spectroscopy.

An electrode which includes nanoparticles of a carbon-doped tin oxide of formula C—SnO2-x where x=is from 0.001 to 0.1, having surface oxygen vacancies. The electrode includes a fluorine-doped tin oxide substrate. A film of the nanoparticles is present on at least one surface of the fluorine-doped tin oxide substrate. The surface oxygen vacancies correspond to an O 1s peak shift of 0.5-2 eV in the X-ray photoelectron spectroscopy (XPS) for C—SnO2-x compared to C—SnO2 without surface oxygen vacancies.

The application belongs to the field of catalyst hydrolysis hydrogen production reaction, discloses a preparation method and application of Pt-Fe / tourmaline catalyst composite material, and applies it to sodium borohydride (NaBH4) hydrolysis hydrogen production; the catalyst forms metal-support interaction with the carrier tourmaline based on the synergistic mechanism between the bimetallic and makes NaBH4 produce hydrogen efficiently; the preparation method comprises the following steps: (1) preparing Pt / tourmaline catalyst solution by using in-situ reduction method; (2) adding metal iron precursor into the solution to prepare Pt-Fe / tourmaline composite catalyst suspension. The obtained suspension is filtered, washed and dried to obtain Pt-Fe / tourmaline catalyst. The application uses simple in-situ reduction method to prepare Pt-Fe / tourmaline catalyst composite material, and uses transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS) and other means to characterize the preparation completion and catalytic sodium borohydride hydrolysis performance, and obtains a kind of process simple, low energy consumption, pollution-free, efficient hydrogen production and low cost characteristics; the prepared Pt and Fe nanoparticles have small particle size and good dispersion uniformity, and have good application prospect.

A substrate joined body including: a first substrate; a second substrate; an organic film that comprises silicon and carbon and joins the first substrate and the second substrate; and a protective film that comprises an inorganic element and is formed over the organic film from at least a part of the surface of the first substrate and at least a part of the surface of the second substrate, wherein the protective film comprises a region in which the ratio of carbon to silicon based on atomic percentage is from 0.0 to 5.0 in a region within 50 nm in a thickness direction from a surface of the organic film on the protective film side, when the surface is measured by X-ray photoelectron spectroscopy.

This invention provides an Al bonding line or Al bonding strip that exhibits good temperature cycling reliability and good first-joint strength, as required in next-generation SiC power semiconductor devices, even during high-temperature temperature cycling tests. The Al bonding line or Al bonding strip contains 3.0% by mass or more and 20.0% by mass of Si. When the Si concentration (atomic %) in the depth direction from the surface of the Al bonding line or Al bonding strip is measured by X-ray photoelectron spectroscopy (XPS), the ratio of the average Si concentration Ca in region a (depth of 5 nm to 50 nm from the surface) to the average Si concentration Cb in region b (depth of 800 nm to 1200 nm from the surface) is 0.03 or more and 0.5 or less.

Provided is a substrate with a conductive film capable of suppressing a change in flatness in a reflective mask with a conductive film for EUV lithography and a reflective mask blank with a conductive film for EUV lithography.The substrate with a conductive film comprises: a substrate having two main surfaces; and a conductive film disposed on one of the main surfaces of the substrate. The conductive film comprises an outermost layer disposed on an outermost surface of the conductive film on a side opposite to the substrate, and a conductive layer disposed between the outermost layer and the substrate. The outermost layer comprises a metal (M), boron (B), and oxygen (O). The outermost layer has a maximum peak at binding energy of 190 eV or more and 195 eV or less in a B1s narrow spectrum obtained by analysis by X-ray photoelectron spectroscopy.

The present invention aims to provide a laminate having a cured film with high liquid repellency, easy separation coating of a wavelength conversion layer after being formed into a partition wall pattern, and high adhesion to an inorganic film such as SiO2, SiN of an upper layer. The present invention is a laminate characterized by being a laminate having a substrate and a cured film obtained by curing a resin composition, wherein in X-ray photoelectron spectroscopy (XPS analysis) of the upper surface of the cured film, no peak derived from fluorine atom F1s is observed, and the surface free energy of the upper surface of the cured film is 10 mN / m or more and 29 mN / m or less.

In the present disclosure, a positive electrode layer used in an all-solid-state battery includes a positive electrode active material, a sulfide solid electrolyte, and a coated sulfide solid electrolyte having a coating layer covering a surface of the sulfide solid electrolyte and containing a metal sulfate, and in an S2p spectrum obtained by X-ray photoelectron spectroscopy (XPS) on the coated sulfide solid electrolyte, a ratio (P2 / P1) of an intensity P2 of a peak appearing near 163 eV to an intensity P1 of a peak appearing near 167 eV is 0.15 or more and less than 0.36, thereby solving the above problem.

The present application provides a film formed using a liquid crystal composition containing a leveling agent having a silicon atom, which has excellent adhesion to an adjacent layer. The film of the present application is a film formed using a liquid crystal composition containing a liquid crystal compound and a leveling agent containing a silicon atom, wherein, in the inner-shell photoelectron spectrum of Si2p obtained by measuring the surface of the film by X-ray photoelectron spectroscopy, the binding energy of the peak top is 102.0 eV or more, or a silicon atom bonded to four oxygen atoms is present on the surface of the film.

This electrode (1) comprises a substrate film (2) and a conductive carbon layer (4) in this order toward one side in the thickness direction. The electrode (1) satisfies expression (1).　Expression (1): 0.30<N / O<4.00 (In expression (1), N represents the content of nitrogen atoms in the conductive carbon layer, as measured by X-ray photoelectron spectroscopy at a photoelectron extraction angle of 90º with respect to one surface of the conductive carbon layer in the thickness direction, and O represents the content of oxygen atoms in the conductive carbon layer, as measured by X-ray photoelectron spectroscopy at a photoelectron extraction angle of 90º with respect to one surface of the conductive carbon layer in the thickness direction.)

The present invention is characterized in that: a composite metal oxide includes at least a transition metal, and contains S and two or more elements selected from the group consisting of Li, Na, B, Ni, Mg, Al, Si, P, K, Ti, Mn, Fe, Co, Zr, Nb, Mo, Sn, W, Ca, Sr, and Bi; in secondary particles, the proportion of primary particles having an aspect ratio of at least 2 is at least 40%; a modified compound including a compound containing S is present on the surface of each of the primary particles; the content of S contained in the composite metal oxide satisfies 0.1 mol%≤S content≤3 mol%; and an S 2p spectrum by X-ray photoelectron spectroscopy has a first peak having a vertex at 170±2 eV and a second peak having a vertex at 167±2 eV.