32results about How to "Conducive to large-scale industrial application" patented technology

The invention relates to a preparation method of an active carbon loaded catalyst for electrochemically catalyzing and degrading organic wastewater and belongs to the technical field of preparation of catalysts. The preparation method comprises the following steps: preparing an active carbon solid containing a plurality of types of active metal by using a sol-gel method; adding P2O5 powder into the active carbon solid containing the active metal and roasting; sublimating the P2O5 powder into gas at a high temperature; and when the gas is expanded at the high temperature and escapes, generating a plurality of small pores in the active carbon, so that the specific surface area and adsorption capability of the active carbon are improved. According to the preparation method, rare earth metal is used in match with the other active metal so that grains on the surface of the catalyst are uniform and thinned; and meanwhile, the preparation method is combined with a method of adding the P2O5 powder to roast, so that the catalysis efficiency of the prepared active carbon loaded catalyst can be improved by more than 5%-15%. The method has a simple process, is convenient to operate and is low in cost; and in a process of electrochemically catalyzing and degrading the organic wastewater by using the prepared catalyst, other oxidants do not need to be additionally added and the large-scale industrialized application of the preparation method is facilitated.

The invention relates to a novel process for preparing biodiesel through natural oil which has different acid numbers and a rapid esterification / ester interchange reaction with catalysts of minute quantity at an alcohol-oil consolute temperature. The process comprises the following steps of: taking animal and vegetable oil as raw materials, adding the oil and methanol into a reaction kettle according to an alkyd mol ratio of 2 to 1-10 to 1 for rapid esterification, and adding the acid catalyst of minute quality which is 0.01-1 per mille of the weight of the oil with reaction conditions of 120-200 DEG C, 2.0-8.0Mpa, and 10-30min; after neutralization deacidification, adding refined oil and methane into a high-pressure reaction kettle according to a mol ratio of 1 to 6-1 to 20 for rapid ester interchange, and adding a base catalyst of minute quality which is 0.01-1 per mille of the weight of the refined oil with reaction conditions of 140-200 DEG C, 2.0-8.0Mpa, and 5-20min; carrying out the sedimentation or centrifuge of a reaction product, and generating a qualified biodiesel product after removing methane through upper layer liquid phase distillation. The process uses minute quantity of catalysts and does not need separation with quick reaction and simple procedure without pollution and corrosion. The process has the advantages of mild conditions, environmental protection and remarkable efficiency.

The invention provides an electrochemical reactor and a method for electrocatalytically removing chloride ions and relates to the technical field of wastewater treatment. The anode of the electrochemical reactor comprises a net basket made of insoluble metal and a Ru-Ti-AC catalytic material filling the net basket, and a carbon rod or a metal wire is led out of the middle of the anode and connected to the positive pole of a power supply; a cathode comprises multiple metal plates or metal nets arranged at intervals, the interval between every two adjacent metal plates or metal nets is 4-6 cm, and the cathode is connected to the negative pole of the power supply through a wire. The electrochemical reactor is high in electrolytic efficiency and high in chloride ion degradation rate. The method for electrocatalytically removing the chloride ions is implemented with adoption of the electrochemical reactor. To-be-treated wastewater is introduced into a reaction tank of the electrochemical reactor and submerges the anode and the cathode, constant current is applied between the anode and the cathode, the wastewater is stirred continuously, and a reaction is performed for 0.1-2 h. The method is convenient to operate and beneficial to large-scale industrial application.

Disclosed is a graphite modification method. The graphite modification method comprises the steps of performing ball milling on graphite powder, grinding balls and a ball grinding medium at the mass ratio of 1:(1-10):(7-50) at the rotary speed of 650-1,200r / min for 2-48h. The graphite / silicon dioxide porous electrode and the graphite / silicon composite material prepared from graphite obtained by the modification method provided by the invention obtain excellent electrochemical performance.

Synthesis of boron-contained silicone is carried out by taking magnesium block as cathode-anode, polymerizing silane dihalide or allyl chloride trihalide in butylene oxide solution and synthesizing to obtain the final product. It's simple, safe and controllable. It has gentle reactive condition and decreases C / C composite material high-temperature anti-oxidant performance and can be used as ceramic precursor.

The invention provides a Ru-Ti-AC catalytic material and a preparation method thereof and relates to the field of activated carbon supported catalysts. The preparation method comprises the steps that activated carbon is soaked with an acidic aqueous solution, is washed with water and is dried to obtain pretreated activated carbon; the pretreated activated carbon is mixed with ruthenium chloride, butyl titanate, citric acid and a solvent, and even stirring is performed to obtain a mixed reaction solution, a pH value of the mixed reaction solution is regulated, and then reaction is performed at the temperature of 92-95 DEG C to obtain slurry; the slurry is evaporated to be dry at the temperature of 125-135 DEG C, a solid is obtained, and drying is performed to obtain an activated carbon solid; Na2CO3 powder is added to the activated carbon solid, even mixing is performed, calcination is performed at the temperature of 750-850 DEG C, and cooling is performed to obtain the material. The preparation method is simple in process, convenient to operate and low in cost, the prepared Ru-Ti-AC catalytic material can be used for electrical catalytic degradation of chloride ion wastewater, additional other oxidizing agents are not needed, the electrolytic efficiency is high, the chloride ion degradation rate is high, and large-scale industrialized application is promoted.

The invention belongs to the technical field of solid waste pollution control and recycling, and provides a plasma etching enhanced ternary mixed plastic flotation separation method. The method comprises seven core process links including pretreatment 1, pretreatment 2, plasma etching 1, a flotation unit 1, pretreatment 3, plasma etching 2 and a flotation unit 2. The seven process links are sequentially connected in series and can be continuously operated on line; ternary mixed plastic fed in the pretreatment step 1 comprises PMMA, PTFE and ABS from different sources; sinking tailings 1 of the flotation unit 1 are the separated PMMA; sinking tailings 2 of the flotation unit 2 are the separated PTFE; and a floating product 2 of the flotation unit 2 is the separated ABS. The method is simple in process, relatively mild in process, free of a high-temperature pressurizing link and high in separation safety and efficiency.

The invention relates to a method for synthesizing boron-containing polysilane. The method of the invention adopts an electrochemical synthesis method, uses magnesium blocks as cathode and anode, and polymerizes dihalogen silane or trihalogen and allyl chloride in tetrahydrofuran solution to synthesize boron-containing polysilane. The boron-containing polysilane obtained by the method of the present invention has mild reaction conditions, is easy to control, is simple and safe to operate, and the prepared boron-containing polysilane can obviously improve the high-temperature oxidation resistance of C / C composite materials, and is a kind of A kind of ceramic precursor with excellent performance. The method of the invention effectively solves the problems existing in the early research, and is beneficial to large-scale industrial application.

The invention belongs to the technical field of solar cell preparation, in particular to a method for preparing a low-cost high-efficiency laminated solar cell. The present invention comprises the following steps in sequence: texturing, pn junction formation, tunneling silicon oxide deposition, phosphorus element doping, annealing, passivation layer growth, patterned opening, conductive layer deposition, electron transport layer formation, perovskite Film formation, hole transport layer formation, antireflection layer formation and electrode preparation. The solar cell prepared by the present invention has a stacked cell structure, which greatly improves the conversion efficiency of the cell, and the top cell of the present invention adopts a very low-cost perovskite cell, and the bottom cell adopts a high-efficiency passivation contact cell , the key and expensive preparation process of the whole battery is all realized by ultra-low-cost printing or spin-coating or ink-jet methods of various chemical slurries, thus greatly reducing the manufacturing cost while greatly improving the conversion efficiency of the battery , which is conducive to large-scale industrial application and realizes parity Internet access.

The invention belongs to the technical field of organic photoelectric materials, and discloses a carboxyl-containing organic photoelectric material, a preparation method and an application thereof. The present invention selectively removes the ester group alkyl group in the organic polymer optoelectronic material, retains a part of the alkyl group, and the obtained polymer material has both carboxylic acid group and lipophilic alkyl group, which is beneficial to improve the hydrogen bond interaction between molecules. Function, reduce the content of insulating alkyl in the material, improve the charge mobility of the material, and improve the performance of the device.

The invention provides an electrochemical reactor and a method for electrocatalytically removing chloride ions and relates to the technical field of wastewater treatment. The anode of the electrochemical reactor comprises a net basket made of insoluble metal and a Ru-Ti-AC catalytic material filling the net basket, and a carbon rod or a metal wire is led out of the middle of the anode and connected to the positive pole of a power supply; a cathode comprises multiple metal plates or metal nets arranged at intervals, the interval between every two adjacent metal plates or metal nets is 4-6 cm, and the cathode is connected to the negative pole of the power supply through a wire. The electrochemical reactor is high in electrolytic efficiency and high in chloride ion degradation rate. The method for electrocatalytically removing the chloride ions is implemented with adoption of the electrochemical reactor. To-be-treated wastewater is introduced into a reaction tank of the electrochemical reactor and submerges the anode and the cathode, constant current is applied between the anode and the cathode, the wastewater is stirred continuously, and a reaction is performed for 0.1-2 h. The method is convenient to operate and beneficial to large-scale industrial application.

The invention relates to a preparation method of double bond-containing polysilane. The method of the invention adopts an electrochemical synthesis method, uses a magnesium block as an anode and cathode, and polymerizes methyltrichlorosilane and allyl chloride in a tetrahydrofuran solution to synthesize polysilane with a double bond. The double bond-containing polysilane obtained by the method of the present invention has mild reaction conditions, is easy to control, is simple and safe to operate, and the obtained double bond-containing polysilane has a high quality retention rate and a relatively high ceramic yield, The ceramic production rate of the precursor can be improved well, the preparation cycle of C / C-SiC is shortened, and the mechanical damage caused to the composite material during the preparation process is reduced. It effectively solves the problems existing in the early research and is conducive to large-scale industrial application.

The display panel provided by the present invention, the electronic equipment including the display panel, and the manufacturing method of the display panel, wherein the display panel includes: an array substrate having a substrate and a driving unit arranged on the substrate, and a light-emitting functional layer arranged on the driving unit The side away from the substrate is electrically connected to the drive unit, the packaging film layer is arranged on the side of the light emitting functional layer away from the array substrate, the polarizing functional layer is arranged on the light output side of the display panel, and the polarizing functional layer includes a coated polarizing layer . The flexible display panel of the present application has fewer film layers and thinner film thickness, which is conducive to the thinning of the flexible display panel, greatly improves the bending performance of the display panel, and avoids display light leakage during flexible bending phenomenon; in addition, the display panel provided by the present application has simple preparation process, low production cost and high production efficiency, which is beneficial to large-scale industrial application.

The invention discloses a polymer capable of rapidly adsorbing low-concentration formaldehyde, and a preparation method thereof. The method comprises the following steps: (1) dissolving beta-cyclodextrin, a ligand and a reaction catalyst into a solvent; (2) carrying out ultrasonic treatment on the mixed solution obtained in the step (1), purging the mixed solution with gas, and then carrying out aheating stirring reaction; and (3) washing the porous beta-cyclodextrin polymer obtained in the step (2), filtering, soaking, activating, and drying to obtain the polymer. The formaldehyde adsorbentbased on beta-cyclodextrin has excellent formaldehyde adsorption performance. Compared with the existing formaldehyde adsorbing material, the formaldehyde adsorbent of the invention has the advantagesthat the adsorption rate and the adsorption amount of low-concentration formaldehyde are greatly increased, the adsorption amount reaches 28.9 mg / g under 10 ppm and is 80 times that of common activecarbon, the adsorption rate is more than 10 times that of the common active carbon, and the requirement for rapid and efficient adsorption of indoor formaldehyde is met, so that the adsorbent has a great potential application prospect in the aspect of indoor low-concentration formaldehyde adsorption.

The invention provides a preparation method of a catalyst used for electrical catalytic degradation of organic wastewater and relates to a preparation method of a wastewater treatment catalyst. The preparation method comprises the following steps: carrying out pretreatment on a coal-based activated carbon carrier, namely washing the activated carbon carrier to be neutral with deionized water, cooling, then washing to be neutral, carrying out ultrasonic cleaning for 20 minutes, and finally drying at the temperature of 80 DEG C for later use; and preparing a catalyst by adopting an in situ precipitation method, namely dispersing the pretreated coal-based activated carbon powder and amorphous Fe78Si13B9 powder into distilled water and putting in a three-mouth flask, under the protection of nitrogen atmosphere, adding 10-30ml of FeSO4.7H2O solution with the concentration of 1mol / L, alternately washing with ethanol for five times, carrying out vacuum drying for 12 hours by virtue of a drying oven, grinding a dried reaction product in a mortar, and screening by virtue of a 200-mesh sieve, so that a coal-based activated carbon supported amorphous Fe78Si13B9 / nano Fe3O4 catalyst is obtained. The prepared catalyst integrates adsorption, catalysis, internal electrolysis and magnetic separation into a whole, and solves the problems that the catalyst is difficult to separate and recycle and efficient removal of an organic matter is difficult.

The invention discloses a two-component silicone gel for high-power IGBT packaging and a preparation method. The silicone gel is made by mixing components A and B, wherein: the A component is made by mixing the following components in parts by weight: 100 parts of vinyl silicone oil, 0.02-1 part of platinum catalyst ; The B component is composed of the following components in parts by weight: 70-90 parts of vinyl silicone oil, 10-30 parts of chain extender (hydrogen-containing silicone oil at the end), 10-30 parts of cross-linking agent (side-chain hydrogen-containing silicone oil ) 0.5-5 parts, inhibitor 0.1-1 part, antioxidant 0.05-0.5 part. When in use, stir and mix components A and B at a weight ratio of 1:1, and solidify to obtain the product. The invention adopts high-purity silicone oil as raw material, has good thermal stability, low volatile content and high dielectric strength, and can meet the use requirements of high-power IGBT modules.

The invention relates to an activated rust layer rust converting agent for electric transmission and transformation equipment and a preparation method and application of the rust converting agent and belongs to the technical field of corrosion prevention of special materials. The rust converting agent disclosed by the invention is prepared from the following components in parts by mass: 8-15 parts of phosphoric acid, 1-3 parts of citric acid, 0.5-3 parts of oxalic acid, 0.1-0.5 parts of thiourea, 0.1-0.5 parts of triethanolamine, 1-2 parts of zinc oxide, 5-8 parts of zinc dihydrogen phosphate, 0.1-1 parts of molybdate, 0.1-1 parts of hydrochloride, 0.5-1 parts of emulsifier, 0.5-1 parts of hydrofluoride, 0.5-1 parts of sodium benzoate, and 70-80 parts of deionized water. The components are added to a container according to proportion and mechanically stirred to be uniform, a product can be obtained after the reaction is completed and the solution is transparent and has not impurities, and in use, the rust converting agent can be brushed before a paint is coated. The rust converting agent is reasonable in component design and simple in preparation process, and the obtained rust converting agent has excellent performances, is wide in application scope and is convenient for large-scale production and application.

Embodiments of the present invention provide a display panel, a manufacturing method thereof, and an electronic device, which improve an existing packaging module of a display panel. Both the display panel and the electronic device include: a substrate, a light-emitting functional layer is disposed on the substrate, a first inorganic encapsulation layer disposed on the light-emitting functional layer, a polarizing layer disposed on the first inorganic encapsulation layer, The second inorganic encapsulation layer disposed on the polarizing layer improves the encapsulation performance of the flexible display panel by arranging the polarizing layer in the encapsulation structure; in addition, the preparation method of the display panel provided by the application adopts a process integration method, and the process The method is simple, low in production cost and high in production efficiency, and is conducive to large-scale industrial application.

The invention belongs to the technical field of pharmaceutical preparations, and particularly relates to a sacubitril valsartan sodium pharmaceutical composition and a preparation method of the sacubitril valsartan sodium pharmaceutical composition. The preparation method comprises the following steps: adopting a solvent individually granulated through a wet method by using acetone at the specificproportion as the raw material, then mixing and granulating, drying a granulated particle in combination with drying under reduced pressure at the lower temperature, the process with excellent repeatability is obtained when the scale is enlarged / reduced, and a drug is guaranteed not to be damaged in the preparation process. The stability and the uniformity of the obtained pharmaceutical preparation are excellent, and the pharmaceutical preparation is favorable for the excellent promotion of the drug to the treatment of congestive heart failure, high blood pressure and the like.

The invention provides a Fe-Co-AC catalytic material and a preparation method thereof and relates to the field of activated carbon supported catalysts. The preparation method comprises the steps that activated carbon is soaked with an acidic aqueous solution, is washed with water and is dried to obtain pretreated activated carbon; the pretreated activated carbon is mixed with a ferric nitrate solution, a cobalt nitrate solution and citric acid and is stirred evenly to obtain a mixed reaction solution; the pH value of the mixed reaction solution is regulated, and then reaction is performed at the temperature of 70-90 DEG C to obtain slurry; the slurry is evaporated to dryness at the temperature of 100-120 DEG C, and a solid is obtained and is dried to obtain an activated carbon solid; P2O5 solid powder is added to the activated carbon solid and is evenly mixed, and the mixed is roasted at the temperature of 300-700 DEG C and is cooled. The preparation method is simple in process, convenient to operate and low in cost, the prepared Fe-Co-AC catalytic material can be used for electrocatalytic degradation of chloride ion wastewater without adding of other oxidizing agents, is high in electrolysis efficiency, high in chlorine ion degradation rate and suitable for large-scale industrial application.

The invention relates to a preparation method of an active carbon loaded catalyst for electrochemically catalyzing and degrading organic wastewater and belongs to the technical field of preparation of catalysts. The preparation method comprises the following steps: preparing an active carbon solid containing a plurality of types of active metal by using a sol-gel method; adding P2O5 powder into the active carbon solid containing the active metal and roasting; sublimating the P2O5 powder into gas at a high temperature; and when the gas is expanded at the high temperature and escapes, generating a plurality of small pores in the active carbon, so that the specific surface area and adsorption capability of the active carbon are improved. According to the preparation method, rare earth metal is used in match with the other active metal so that grains on the surface of the catalyst are uniform and thinned; and meanwhile, the preparation method is combined with a method of adding the P2O5 powder to roast, so that the catalysis efficiency of the prepared active carbon loaded catalyst can be improved by more than 5%-15%. The method has a simple process, is convenient to operate and is low in cost; and in a process of electrochemically catalyzing and degrading the organic wastewater by using the prepared catalyst, other oxidants do not need to be additionally added and the large-scale industrialized application of the preparation method is facilitated.

The invention discloses a method for preparing 4-amino-N-[(2R,3S)-3-amino-2-hydroxy-4-benzene butyl]-N-isobutyl benzsulfamide. The method comprises the following steps: S1: enabling L-phenylalanine and diazomethane to react to obtain a diazo methyl ketone intermediate product, and enabling the diazo methyl ketone intermediate product and haloid acid to react to obtain a compound A; S2, conducting carbonyl deoxidation on the compound A to obtain a compound B; S3, under the existence of iso-butylamine, conducting cyclization reaction and ring-opening reaction on the compound B in sequence to obtain a compound C; S4, enabling the compound C and nitrobenzenesulfonyl chloride to react to obtain a compound D; S5, conducting nitro reduction on the compound D to obtain the 4-amino-N-[(2R,3S)-3-amino-2-hydroxy-4-benzene butyl]-N-isobutyl benzsulfamide. The method is simple in course, low in cost, mild in condition, and higher in intermediate product stability, and is beneficial for industrial application.