The invention discloses a process for preparing high-purity
zirconium oxychloride, which comprises the following steps: pumping crude
zirconium oxychloride solution into a high-level
barrel for later use, and pumping
purified water into an organic regenerative section of an extraction tank; evenly stirring N, N-di (1-methyl heptyl)
acetamide and sulfonated
kerosene in a volume ratio of 1:1-9, and quantitatively pumping the mixture into the extraction tank and pumping the excess into the circular organic high-level
barrel; opening a
discharge valve of the extraction tank to
discharge the circular organic and organic regenerative
wastewater and the extracted crude
zirconium oxychloride solution, testing the discharged solution, extracting the solution through
multiple stages, and discharging the extracted crude
zirconium oxychloride solution from the front end of the extraction tank; concentrating and crystallizing the solution; and putting the crystallized material into a suction filter tank, rinsing the crystallized material, then
drying the rinsed material by a centrifugal
machine, and packing the dried material. The process has the advantages of shortening the process flow, avoiding the introduction of
alcohol reagent in an extraction
system, improving the stability of the extraction
system, reducing the volatility and water
solubility of an extracting agent, reducing the consumption of organic
reagent, improving the
working environment, reducing the treatment difficulty of
wastewater, and saving the production cost.