43results about How to "Low preparation environment requirements" patented technology

The invention discloses a paclitaxel loaded catenulate nano fiber and a preparation method thereof. At first, catenulate nano fiber is prepared, then paclitaxel is loaded on the beads to form a drug sustain-released system, and thus slow releasing of paclitaxel can be effectively controlled. Furthermore, the biocompatibility is good, the drug encapsulation rate is high, and the activity is strong. The provided dosage form of paclitaxel has the advantages of little side and toxic effect and sustained-release function, and can be applied to preparation of drugs for treating malignant tumors.

The present invention provides a method for preparing a graphene-based chip heat-radiating material, which comprises the steps of: providing a substrate on which horizontal graphene is prepared; placing the substrate in a reaction chamber, after vacuum pumping is performed on the reaction chamber, reducing gas is introduced into the reaction chamber and increasing the temperature to a preset temperature, and then performing plasma preprocessing on the substrate; introducing of the reducing gas is kept and furthermore growing gas is introduced for growing vertical graphene on the surface of the horizontal graphene; and stopping introduction of the growing gas and reducing temperature of the reaction chamber, and then transferring the horizontal graphene and the vertical graphene to the surface of the chip on which heat radiation is to be performed. According to the method, the hot spot heat which is generated by operation of the device is radiated to the surface of the device through the horizontal graphene, and then relatively large specific surface area of the vertical graphene is utilized for radiating heat of a large-power chip in the horizontal direction to surrounding environment through the large specific surface area, thereby improving heat radiating efficiency. The method for preparing the graphene-based chip heat-radiating material has advantages of: simple process, easy operation and low requirement for preparing environment.

The invention discloses a counter electrode material of a sensitized solar battery. The counter electrode material comprises polyacrylonitrile carbon nanofibers and load, and the load is carried on the polyacrylonitrile carbon nanofibers and is one of precious metal, metal carbide, metal nitride or metal oxide. A manufacturing method of the counter electrode material includes the steps of solving polyacrylonitrile in dimethyl formamide, injecting into a high-voltage static spinning machine for spinning, carbonizing to obtain the polyacrylonitrile carbon nanofibers, and enabling the load to be carried on the polyacrylonitrile carbon nanofibers by means of sintering, evaporating or magnetron sputtering so as to obtain the counter electrode material of the sensitized solar battery. The manufacturing method is simple in manufacturing technology, easy to operate and low in cost; the manufactured counter electrode material of the sensitized solar battery is uniform in quality and good in catalytic performance; by means of applying manufactured counter electrodes to the sensitized solar battery, photoelectric converting efficiency can be improved greatly, and industrialized popularization of the sensitized solar battery can be promoted greatly.

The invention relates to a 2D Ti3C2-MXene thin film material, a preparation method thereof and application of the material in an RRAM, and belongs to the technical fields of film preparation and microelectronic functional devices. An MXene film is prepared in the surface of a conductive substrate in a low-temperature one-step solution method, film formation is easy, and the film can be prepared ina large area more easily. The novel 2D material MXene is applied to the memory field instead of a traditional resistive switching material for the first time, the RRAM comprises a hard substrate, a bottom electrode, a resistive switching layer and a top electrode successively from bottom to top, the resistive switching layer is made of the 2D Ti3C2-MXene thin film material and in the thickness of100-450nm, a prepared device, as a nonvolatile memory, can keep the original resistive state when being powered off, and the device is kept stable after multiple continuous cycles, and is resistant to circulation.

The invention discloses a method for preparing a nano-silver / D-cysteine antibacterial coating on the surface of medical metal. The method comprises the steps that the medical metal is sequentially subjected to ultrasonic treatment through acetone, ethyl alcohol and deionized water; a dopamine solution is prepared, the medical metal is put in the dopamine solution for soaking, after the medical metal is taken out, dopamine particles which are not stably attached to the surface are subjected to ultrasonic removal, then the medical metal is put in a silver nitrate solution for soaking, and then apoly-dopamine-nano-silver coating is formed on the surface of medical metal; afterwards, the medical metal loaded with the nano-silver particles is put in a D-cysteine solution for a reaction to obtain the nano-silver / D-cysteine antibacterial coating. The composite nano-structure prepared by means of the method is simple and feasible in technology, and has the functions of efficient spectral bacterial resistance and biomembrance adhesion resistance; meanwhile, the nano-silver / D-cysteine antibacterial coating has good biocompatibility, and has very important application value in developing novel in-vivo implant materials.

The invention relates to the field of lithium ion batteries, and discloses a halogenated solid electrolyte material and a preparation method thereof, a flexible solid electrolyte membrane and a preparation method thereof, a lithium battery and a preparation method thereof. The halogenated solid electrolyte material has a composition shown as a formula I: Li[alpha]M[beta]M'[gamma]A [delta]A'[epsilon], wherein in the formula I, M is selected from a group IIIB element and / or a group IIIA element, and M' is selected from at least one of a group IIA element, a group IB element, a group IIB element,a group IVB element, a group VIII element and a group VIII element; wherein A is selected from at least one of F-, Cl-, Br- and I-; wherein A' is selected from SO4<2> and / or SiO3<2->, 1 < = alpha < =3, 0 < = beta < = 1, 0 < = gamma < = 2, 0 < delta < = 6, and 0 < = epsilon < = 1. The halide solid-state electrolyte solid-state lithium battery prepared based on the solvent-free method has relatively high specific capacity and cycling stability.

The invention discloses an anti-oxidation treatment method for sintering a nd-fe-b material and an antioxidant. The anti-oxidation treatment method comprises the following steps of: in a jet milling stage, injecting the antioxidant into the nd-fe-b material in a spray manner, wherein the antioxidant is evenly coated by magnetic powder during jet milling; sealing and mixing the powder under an air condition; carrying out compression molding in an air atmosphere; and sintering under a low vacuum condition to obtain a blank. Anti-oxidation auxiliaries used are benzotriazole and petroleum ether the volume ratios of which are respectively 0.05-5% and 99.95-95%. According to the invention, requirements for preparation environment are reduced, the preparation is simple and flexible, energy saving and consumption reduction effects are achieved, and a finished magnet has properties similar to those of materials prepared in a non-air atmosphere.

The invention discloses a method for pre-lithiation of a silicon-based negative electrode material. The method comprises the following steps: dissolving aromatic hydrocarbon organic matters in organicether to prepare an aromatic hydrocarbon-containing solution, putting a lithium sheet into the solution, and reacting aromatic hydrocarbon with the lithium sheet to obtain a precursor solution of aromatic hydrocarbon lithium salt; then adding the silicon-based negative electrode material into the precursor solution to obtain a turbid liquid, and carrying out a pre-lithiation reaction; and standing for a period of time, drying the turbid liquid under the protection of an inert atmosphere, and calcining to obtain the pre-lithiated silicon-based negative electrode material. The method has the advantages that the preparation is simple, the silicon-based material can be effectively pre-lithiated, and the first efficiency is greatly improved.

The invention discloses a light emitting device manufacturing method, which belongs to the technical field of dissolvable flexible electronic devices. A light emitting device comprises a dissolvable lower electrode, a dissolvable light emitting functional layer and a dissolvable lower electrode. Specifically, silver nanowire-polyvinyl alcohol is used as the lower electrode. A phosphor light emitting functional layer and a silver nanowire-polyvinyl pyrrolidone upper electrode are on the upper layer of the lower electrode. According to the invention, the sandwich light emitting device structureof a light emitting layer is added between upper and lower electrodes; the device is prepared by an all-solution method without large-scale equipment such as high vacuum evaporation magnetron sputtering; the preparation process is simple, and the cost is low; and the dissolvable device has the advantages of stable light emission, low energy consumption, recyclability, environmental protection andthe like.

The invention discloses a device and a method for preparing an anodic aluminum oxide template with large pore diameter, and belongs to the technical field of nanomaterial preparation. The device is provided with an ice water bath tank, a positive side electrolytic bottle, a reverse side electrolytic bottle, an anode and an anode outgoing line, a cathode and a cathode outgoing line, a thermometer, an aluminum sheet clamping suite and a magnetic stirrer; a solution channel of the reverse side electrolytic bottle and a solution channel of the positive side electrolytic bottle are in dead locking connection to form an integrated electrolytic bottle through the aluminum sheet clamping suite, an aluminum sheet is used as the anode, and a platinum electrode is used as the cathode; the pore-diameter anodic aluminum oxide template adopts a secondary anodic oxidation method, and citric acid as a stabilizer is mixed in a phosphoric acid with extremely low concentration to prepare a highly-ordered large plate; the cathode extends into the positive side electrolytic bottle, the magnetic stirrer is used for stirring, and the whole process of oxidation and post treatment is completed through replacement of solutions in the two electrolytic bottles. The device and the method have the advantages of simple operation, convenient flow, and easy observation, and the device is the anodic aluminum oxide template preparation device which can independently accomplish the oxidation process and all subsequent steps.

The invention relates to an infrared quantum dot layer and a preparation method thereof, and an infrared detector and a preparation method thereof, and the preparation method of the infrared quantum dot layer comprises the steps: dissolving a first-type primer of a first dosage and a first-type primer of a second dosage in a first ligand solution, and correspondingly obtaining a first-type precursor solution of a first doping concentration and a first-type precursor solution of a second doping concentration, the second dosage is not equal to the first dosage; dissolving a first type of first primer with a second dosage in the first ligand solution to obtain a first type of precursor solution with a second doping concentration; and correspondingly obtaining infrared quantum dots with different doping concentrations based on the first type precursor solution and the second type precursor solution with different doping concentrations, and further forming a first infrared quantum dot sub-layer and a second infrared quantum dot sub-layer so as to construct the in-band transition type PN junction. Therefore, the in-band transition type infrared quantum dot layer is formed, and the detection accuracy can be improved; and based on a solution method for preparation, the method is simple, the process difficulty is relatively low, and the cost is relatively low.

The invention relates to a metal lithium negative electrode for a lithium battery. The metal lithium negative electrode comprises a metal lithium substrate and a compact inorganic compound surface layer, wherein the metal lithium substrate comprises metal lithium and alloy thereof, and the inorganic compound surface layer is a metal compound which can be subjected to an in-situ oxidation-reductionreaction with the metal lithium in an electrolyte to generate a lithium compound and nano metal particle composite structure. The compact inorganic surface layer of the metal lithium negative electrode can spontaneously react with metal lithium when electrolyte is injected into the battery; a lithium compound phase with high ionic conductivity is generated; meanwhile, nano metal particle phases which are uniformly distributed are generated in the lithium compound phase, and the inorganic surface layer has an electronic conductivity characteristic due to nano metal particles, so a continuous non-porous complex-phase structure compact inorganic surface layer with an ion and electron mixed conductivity characteristic is formed. When the metal lithium with the inorganic surface layer is usedin a lithium battery, the side reaction of the metal lithium can be effectively inhibited, the safety of the battery is improved, and the cycle life is prolonged.

The invention relates to the technical field of medicine and discloses a preparation method of 5-bromine-7-azaindole. The preparation method of the 5-bromine-7-azaindole comprises the following steps:preparing 200 to 500 mg of 2-aminopyridine, 100 to 150 mg of dimethylsulfoxide, 500 to 800 g of sodium carbonate solution, 100 to 200 mg of 7-azaindole, 500 to 700 mg of anhydrous sodium sulfate, 50to 60 mg of N-bromo-succinimide, 20 to 30 mg of ethyl acetate, 600 to 800 mg of bromine, 100 to 300 mg of alcohol solvent and 600 to 800 mg of dihydro-7-azaindole-2-sodium sulfonate, taking 200 to 500mg of 2-aminopyridine and 100 to 200 mg of 7-azaindole by a user, heating for future use, and taking out the heated 200 to 500 mg of 2-aminopyridine and 100 to 200 mg of 7-azaindole. According to thepreparation method of the 5-bromine-7-azaindole, the 5-bromine-7-azaindole crude product can be prepared by four steps; the preparation method is simple, low in operation difficulty and low requirement on the preparation environment; the user invests small cost to gain great harvest, the trouble of the user is avoided and preparation of the user is facilitated.

The invention discloses a light-emitting device capable of being circularly prepared and a preparation method. The light emitting device includes an insoluble bottom electrode, a soluble intermediatelight emitting layer, and an insoluble top electrode. Specifically, a non-water-soluble polymer-silver nanowire composite film is adopted as a bottom electrode, and the surface of the bottom electrodeis coated with a soluble fluorescent powder light-emitting functional layer and an insoluble polymer-silver nanowire composite film top electrode. The light-emitting functional layer is mingled in the upper electrode and the lower electrode to form the sandwich structure device, the light-emitting device has the advantages of being simple in structure, prepared through an all-solution method, environmentally friendly, low in cost and the like; and meanwhile the device has the advantages of being capable of being circularly machined, good in mechanical flexibility, stable in light emitting, multi-color in light emitting and the like and has wide application prospects.

The invention relates to the technical field of pesticide preparation and discloses a preparation technology for a pure traditional Chinese medicine herbicide. The preparation technology is characterized by comprising the following processes: weighting, cooking, filtering, distilling, concentrating, refluxing and extracting eleven traditional Chinese medicinal materials, including camphor tree leaves, saponin, garlic, tea seed cake, alangium platanifolium, simarouba, gastrodia elata, radix sophorae flavescentis, orpiment, ailanthus altissima swingleh leaves and coptis chinensis. The preparation technology provided by the invention is simple, has low demand on preparation environment and is harmless to environment and human body. The prepared pure traditional Chinese medicine herbicide is capable of effectively preventing and controlling various weeds, is harmless to farmland and crops, has an excellent weeding effect and can be widely popularized and applied.

The invention discloses a method for preparing a hollow microneedle through an ultraviolet-curing process using a soluble fiber as a core material. The method can be carried out at the room temperature, and the preparation time is short, which is advantageous for preparing a hollow microneedle array quickly and batchwise. Compared with an existing hollow microneedle preparation method, an ultraviolet-curing molding method is adopted to avoid a heating and melting process of a polymer material, a high temperature condition is not required, and requirements for a preparation environment are low;the ultraviolet-curing process has a short molding time, and the microneedle can be formed by 2-3 minute exposure of a photoresist in an ultraviolet light, which greatly shortens the preparation cycle; the hollow part of the microneedle adopts a molding method of using the soluble PVA fiber as the core material, due to the characteristic that the soluble PVA fiber can be dissolved in the water, so that the molding process of the hollow part becomes simple and fast, and the molding difficulty of the hollow microneedle is reduced.

The present invention provides a method for preparing a graphene-based chip heat-radiating material, which comprises the steps of: providing a substrate on which horizontal graphene is prepared; placing the substrate in a reaction chamber, after vacuum pumping is performed on the reaction chamber, reducing gas is introduced into the reaction chamber and increasing the temperature to a preset temperature, and then performing plasma preprocessing on the substrate; introducing of the reducing gas is kept and furthermore growing gas is introduced for growing vertical graphene on the surface of the horizontal graphene; and stopping introduction of the growing gas and reducing temperature of the reaction chamber, and then transferring the horizontal graphene and the vertical graphene to the surface of the chip on which heat radiation is to be performed. According to the method, the hot spot heat which is generated by operation of the device is radiated to the surface of the device through the horizontal graphene, and then relatively large specific surface area of the vertical graphene is utilized for radiating heat of a large-power chip in the horizontal direction to surrounding environment through the large specific surface area, thereby improving heat radiating efficiency. The method for preparing the graphene-based chip heat-radiating material has advantages of: simple process, easy operation and low requirement for preparing environment.

The invention discloses a grating preparation method and a grating, and the grating preparation method comprises the steps: sequentially forming material layers on a substrate through a thermoplasticmaterial, and enabling the adjacent material layers to be made of different materials; after each material layer is formed, obtaining the temperature of the currently formed material layer; when the temperature is lower than a preset temperature corresponding to the currently formed material layer, forming a next material layer on the currently formed material layer; when the total thickness of the material layers reaches a preset thickness, separating the substrate from a stacked material composed of the plurality of material layers; and cutting the stacked material to obtain the grating. Theinvention provides a grating preparation method and a grating, and aims to solve the problem of poor stability of grating preparation in the prior art.

The invention discloses a sensitized solar cell counter electrode material, comprising polyacrylonitrile carbon nanofibers and loads, the loads are loaded on the polyacrylonitrile carbon nanofibers, and the loads are noble metals, metal carbonized One of the compounds, metal nitrides or metal oxides; the preparation method is to dissolve polyacrylonitrile in dimethylformamide, inject it into a high-voltage electrospinning machine for spinning, and carbonize it to obtain polyacrylonitrile carbon nano Fiber: loading the load on the polyacrylonitrile carbon nanofiber through sintering, vapor deposition or magnetron sputtering to prepare a sensitized solar cell counter electrode material. The preparation process provided by the present invention is simple, easy to operate, and low in cost. The prepared solar cell counter electrode material has uniform texture and good catalytic performance. Using the prepared counter electrode in a sensitized solar cell can effectively improve the photoelectric conversion efficiency. It has played a great role in promoting the industrialization of sensitized solar cells.

The invention relates to a preparation method of polyamide-imide copolymer fiber, which belongs to the technical field of spinning fiber, comprising (1) dissolving trimellitic anhydride and dianhydride monomers in an aprotic polar solvent, under nitrogen protection, Stir at low temperature to obtain a mixed solution; add diphenylmethane diisocyanate monomer in batches, and gradually heat up to 130-180°C to obtain a copolymerized modified polyamide-imide spinning stock solution; (2) polyamide-imide After vacuum defoaming and filtration, the spinning stock solution passes through the spinneret and enters the primary coagulation bath to obtain primary fibers, and then passes through the secondary coagulation bath, hot water drawing, washing, drying, oiling, and dry heat drawing Stretching, heat setting, cooling and oiling and winding to obtain polyamide-imide copolymer fibers. The preparation method of the invention has simple process, and the intermediate acid is easy to store, and the prepared polyamide-imide copolymer fiber has the characteristics of high strength and excellent ultraviolet aging resistance.

The invention discloses a preparation method of a light-emitting device, and belongs to the technical field of dissolvable flexible electronic devices. The light-emitting device includes: a dissolvable lower electrode, a dissolvable light-emitting functional layer and a dissolvable lower electrode. Specifically, silver nanowire-polyvinyl alcohol is used as the lower electrode, and the upper layer of the lower electrode is a fluorescent powder light-emitting functional layer and a silver nanowire-polyvinylpyrrolidone upper electrode. The present invention adopts a sandwich light-emitting device structure in which a layer of light-emitting layers is added to the upper and lower electrodes, and adopts a full-solution method to prepare the device without requiring large-scale equipment such as high-vacuum evaporation magnetron sputtering, and the preparation process is simple and low in cost. The soluble device has the advantages of stable light emission, low energy consumption, recyclability, environmental protection and the like.

The invention provides a new method for preparing a hydrophobic material. The method comprises following steps: firstly, surface micro / nano porous structural preparing, wherein a workpiece subject to conventional pretreatment is cleaned for standby application, the arc treatment technology is adopted for obtaining a roughening micro / nano porous surface on the surface of the workpiece; secondly, hydrophobic treatment(fluoroalkyl silane modification treatment), wherein a sample subject to arc treatment is immersed in a fluoroalkyl silane isopropyl alcohol solution, the sample is taken out and is naturally dried under the room temperature condition, and the superhydrophobic surface can be obtained. Arc welding is used for generating the strong and durable gas discharge phenomenon between the workpiece and two electrodes of a welding rod so as to form the micro / nano porous surface, meanwhile, in combination with the fluoroalkyl silane low-surface energy substance, modification is carried out, two general methods are combined together, a new thinking is provided for preparation of the high-performance hydrophobic surface, and the new preparing method has the beneficial effects of being energy-saving, rapid, low in cost, low in preparing environment requirement, easy to operate and the like.

The invention discloses a preparation method of metallic molybdenum nanosheets. The method comprises the following steps: placing a molybdenum source in a tube furnace, exhausting the air in the quartz tube, then introducing a carrier gas, reacting in a heat preservation state after heating up, cooling to room temperature after the reaction, and obtaining the metal molybdenum nanometer piece. The prepared metal molybdenum nanosheets are flake-like; macroscopically, they are fluffy and sponge-like, and microscopically, they have irregular edge morphology, with a size of 0.1-2 μm and a thickness of <100 nm. The preparation method of the invention has the advantages of simple process, convenient operation, cheap and easy-to-obtain raw materials, good repeatability, high efficiency, easy realization of large-scale preparation and production, low requirements on the preparation environment, and good application and industrialization prospects.

The present invention relates to a kind of AlMgB 14 A method for preparing a ceramic material powder, comprising: using absolute ethanol as a solvent, ball milling and mixing raw material powders to obtain a mixed slurry, wherein the raw material powders include a mass ratio of 1:(1.2~1.4):(3.6~ 4.2) Al powder, MgB 2 powder and boron powder; and drying the mixed slurry, pre-pressing to obtain a block, and then sintering under a protective atmosphere.

The invention discloses an anti-oxidation treatment method for sintering a nd-fe-b material and an antioxidant. The anti-oxidation treatment method comprises the following steps of: in a jet milling stage, injecting the antioxidant into the nd-fe-b material in a spray manner, wherein the antioxidant is evenly coated by magnetic powder during jet milling; sealing and mixing the powder under an air condition; carrying out compression molding in an air atmosphere; and sintering under a low vacuum condition to obtain a blank. Anti-oxidation auxiliaries used are benzotriazole and petroleum ether the volume ratios of which are respectively 0.05-5% and 99.95-95%. According to the invention, requirements for preparation environment are reduced, the preparation is simple and flexible, energy saving and consumption reduction effects are achieved, and a finished magnet has properties similar to those of materials prepared in a non-air atmosphere.

The invention relates to a method for activating graphite felt electrodes etched by nickel salts. Using graphite felt as a base material, the surface of the graphite felt is etched by coating nickel salt and sintering at elevated temperatures in stages, and a large amount of oxygen functional groups and catalyst nickel are introduced to obtain Active graphite felt electrodes for flow batteries etched by nickel salts. The advantages are: the invention is simple and quick to operate, low in price, and has relatively low requirements on the preparation environment, thereby reducing the preparation cost of the liquid flow battery. The active graphite felt prepared by the method of the invention is used as the electrode of the iron-chromium flow battery, the efficiency of the battery is improved, and the capacity loss is reduced, so that the electrochemical performance and stability of the iron-chromium flow battery are improved.

The invention relates to the technical field of pesticide preparation, and discloses a preparation method of a traditional Chinese medicine compound herbicide, which is characterized in that the traditional Chinese medicine compound herbicide is prepared from 11 traditional Chinese medicinal materials including camphor tree leaves, Chinese honeylocust fruits, garlic, tea seed cakes, alangium chinense, quassia bark, gastrodia elata, radix sophorae flavescentis, orpiment, ailanthus altissima leaves and coptis chinensis through weighing, decocting, filtering, distillation concentration and refluxextraction. The preparation process is simple, the preparation environment requirement is low, and no harm is caused to the environment and the human body. The prepared pure traditional Chinese medicine herbicide can effectively prevent and treat various weeds, does not cause harm to farmlands and crops, has a good weeding effect and can be widely popularized and applied.