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78results about How to "Common method" patented technology

Preparation method of fluorescent mesoporous silica-based core-shell nanoscale capsule

The invention belongs to the field of nanoscale composite materials, and specifically, relates to a preparation method of a fluorescent mesoporous silica-based core-shell nanoscale capsule. The fluorescent mesoporous silica-based core-shell nanoscale capsule is characterized in that fluorescent mesoporous silica is prepared into shells; and the shells are coated on core materials with different functions, wherein the core materials comprise ferroferric oxide nanoscale particles, gold nanoscale rods and the like. The preparation method of the fluorescent mesoporous silica-based core-shell nanoscale capsule comprises the following steps that cetyl trimethyl ammonium bromide (CTAB) molecule-protected nanoscale particles with different functions are prepared; silica shells are formed on outer layers of the CTAB molecule-protected nanoscale particles with different functions; silane reagent-coupled fluorescent molecule rhodamine B is added into the CTAB molecule-protected nanoscale particles with the silica shells, and undergoes a copolycondensation reaction with tetraethoxysilane to be fixed on the silica shells; CTAB molecules are removed by washing so that a mesoporous silica structure is formed; and polymine is utilized for external modification and then is etched so that the fluorescent mesoporous silica-based core-shell nanoscale capsule is obtained. The preparation method of the fluorescent mesoporous silica-based core-shell nanoscale capsule has the advantages of simple process, convenience of operation, and more nanoscale capsule product functions. The fluorescent mesoporous silica-based core-shell nanoscale capsule prepared by the preparation method has less toxic and side effects and a size-adjustable cavity, and can be utilized as a carrier of a drug for treating cancers.
Owner:NORTHEAST NORMAL UNIVERSITY

Method for analyzing mixture component

The invention relates to a method for analyzing mixture components mixture component. The method includes the steps of: (1) separating a mixture sample with chromatographic technology to obtain a preliminary chromatogram; (2): carrying out a sampling operation to any zone of the preliminary chromatogram obtained through the step (1) as required to obtain a series of chromatograms in different retention times, wherein the series of chromatograms is called a mixture chromatogram; and (3): with series methods of an entropy minimization algorithm, carrying out a calculation operation with the mixture chromatograms obtained through the step (2) to obtain each reconstructed pure chromatogram and each corresponding pseudo concentration. According to the method of the invention, with the combination of the chromatographic technology with the entropy minimization algorithm, the dependence of component separation in the prior art is mainly overcome and a separation operation is no longer important. Each component in a mixture needs not to be separated out thoroughly and meanwhile prerequisites for using the entropy minimization algorithm are achieved. The method is universal, is quick and high-efficiency and is low in cost. Requirements on operation staffs are not high and the method has a great application prospect.
Owner:广州分子信息科技有限公司

Composite nano-material with nano-particles wrapped by meso-porous silica, and preparation method and application thereof

The invention provides a composite nano-material with nano-particles wrapped by meso-porous silica, and a preparation method and an application thereof. The preparation method comprises the followingsteps: firstly, dispersing nano-particles into an ethanol-water solution, adding ammonium hydroxide to adjust the pH value, dropwise adding an ethanol-water solution of hexadecyltrimethylammonium bromide under the ultrasonic action, continuing ultrasonic treatment, dropwise adding tetraethoxysilane, and purifying to obtain the composite nano material which takes meso-porous silica as a shell and nano-particles as a core and is uniform, stable and controllable in size. Binuclear or trinuclear nanoparticles of different types / functions can be embedded into the same meso-porous silica shell to realize multi-core wrapping, the method is universal, can be expanded to wrapping of more different nano-particles, is green and efficient in preparation process, can be carried out at room temperature,and is hydrophilic in used solvent, low in cost and simple in process, the particle size of the obtained composite nano-material is as low as 50 nm, and the composite nano-material with different sizes can be obtained by adjusting the proportion of used reagents.
Owner:侨欧(江门)新材料科技有限公司

Method for synthesizing upconversion fluorescence hollow nanosphere based on sodium polyacrylate microsphere template synthesis

The invention belongs to the field of nanometer composite materials and in particular relates to a preparation method of an upconversion fluorescence hollow nanosphere based on sodium polyacrylate microsphere template synthesis. Sodium polyacrylate microsphere is used as a template for synthesizing multicolor upconversion fluorescence gadolinium trioxide mesoporous hollow nanosphere. The method comprises the following steps of: firstly, adding sodium polyacrylate to a water and isopropanol system to prepare a sodium polyacrylate microsphere; then, enabling rear-earth ions to replace sodium ions for being coordinated with carboxyl of the sodium polyacrylate microsphere to form a polymer precursor shell by using the sodium polyacrylate microsphere as the template through the ion exchange effect of the rear-earth ions and the sodium ions, wherein the polymer precursor shell is repeatedly washed by isopropanol for many times; and finally, roasting the washed polymer precursor for 2 hours at 600 DEG C to obtain the lanthanide series-doped upconversion fluorescence hollow gadolinium trioxide spheres. The method for synthesizing the upconversion fluorescence hollow nanosphere based on sodium polyacrylate microsphere template synthesis is simple and quick, gentle in conditions, green and environment-friendly. Moreover, the method can be used for drug delivering, upconversion fluorescence cell imaging and magnetic resonance imaging. Besides, the method also can be used for catalysts, a chemical reactor, a biological imaging probe and a drug delivery system.
Owner:CHANGCHUN UNIV OF SCI & TECH

Functionally gradient covalent organic framework membrane as well as preparation and application

The invention discloses a functionally gradient covalent organic framework membrane. The functionally gradient covalent organic framework membrane is prepared from polyethersulfone and a covalent organic framework. Preparation steps comprise the following steps: taking 1,3,5-triformylphloroglucinol and hydrazine hydrate as monomers; carrying out condensation polymerization reaction in 1,3,5-trimethylbenzene and an ethanol solvent; washing a product through tetrahydrofuran, acetone and dichloromethane in sequence; then carrying out wet-phase grinding to obtain the covalent organic framework TpHZ; dispersing the covalent organic framework TpHZ into N,N-dimethylformamide and mixing with the polyethersulfone to form a membrane casting solution; adding a certain amount of the volatile solvent tetrahydrofuran; carrying out steps including scraping, non-solvent induced phase separation, surface segregation, immersion, drying and the like on the membrane casting solution to obtain the functionally gradient covalent organic framework membrane. The functionally gradient covalent organic framework membrane has the advantages of simple and convenient preparation process, strong controllability, easiness for obtaining the raw materials and common method. The prepared membrane is used for realizing pervaporization of an ethanol-water solution system and has high permeation flux and high selectivity on water molecules; the composite membrane has good operation stability at high temperature.
Owner:TIANJIN UNIV

Sodium alginate hybrid membrane filled with hollow ZIF-8 nanoparticles as well as preparation and application of sodium alginate hybrid membrane

The invention discloses a sodium alginate hybrid membrane filled with hollow ZIF-8 nanoparticles. The sodium alginate hybrid membrane is prepared from sodium alginate and hollow ZIF-8 according to a mass ratio of 100 to (2-10), wherein the hollow ZIF-8 is prepared from zinc acetate dihydrate and 2-dimethyl imidazole according to a molar ratio of 1 to 1. A preparation method of the sodium alginatehybrid membrane comprises the following steps: firstly, obtaining the hollow ZIF-8 nano particles; then, dispersing the hollow ZIF-8 nanoparticles into deionized water, and mixing the dispersion liquid with sodium alginate to prepare a casting membrane solution; spin-coating a polyacrylonitrile base membrane with the casting membrane solution, drying, crosslinking, and re-drying to obtain the sodium alginate hybrid membrane. The preparation method has the advantages of being simple and convenient in preparation process, high in controllability, easy in obtaining of raw materials, universal inmethod, and the like. The prepared sodium alginate hybrid membrane can be used for pervaporation of an ethanol-aqueous solution system, and has high permeation flux and high selectivity to water molecules; furthermore, the hybrid membrane has good operational stability at the high temperature.
Owner:TIANJIN UNIV

Preparation method of polymeric micelle nanofiltration membrane and application thereof

The invention discloses a preparation method of a polymeric micelle nanofiltration membrane and application thereof, which belongs to the field of porous material separation membranes. The polymer membrane is mainly attached to a macroporous substrate, and a polycarbonate membrane is chosen as the substrate layer. The preparation method of the micelle membrane comprises the following steps: a polymer with an appropriate block proportion and molecular weight is chosen to be dissolved in selective solvent, so that a micelle solution with a specific morphology is formed; the micelle solution is uniformly dispersed, spread onto the macroporous substrate by the vacuum filtration technology and naturally dried, and thereby the block copolymer separation membrane prepared by the dilute micelle solution is obtained. The voids formed between the piled micelles serve as part of membrane pores, thus playing the role of selective separation, while the macroporous substrate of the lower layer helpsincrease the separation efficiency of the membrane. Most of the current methods for preparing polymer membranes are complex and consume a great deal of energy. The membrane production method is universal and simple, the needed cost is low, and moreover, the produced membrane has high separation efficiency, and can be applied to the separation of different sizes of gold nanoparticles.
Owner:NANJING UNIV OF TECH

Method for in-situ construction of multistage nanometer topological structure on titanium-based implant surface based on salt corrosion

The invention discloses a method for in-situ construction of a multistage nanometer topological structure on a titanium-based implant surface based on salt corrosion. The method comprises the following steps: immersing pickled titanium or titanium alloy in a phosphate solution for low temperature heating treatment; performing heat treatment on the treated titanium or titanium alloy, washing with water and then drying to obtain a titanium-based implant with a multistage nanostructure formed on the surface. According to the method, salt solution is adopted as a medium to corrode titanium or titanium alloy, the titanium-based implant with the multistage nanostructure formed on the surface after heat treatment is obtained, conditions in the treatment process are mild, and no residue of strong acid or strong alkali exists; the formed multistage nanostructure has excellent biocompatibility, can promote the adhesion and growth of bone-related cells, and is expected to greatly improve the bone integration ability of the implant; the method can also be used in combination with other surface micrometer methods, can be used for constructing a micro-nanometer hybrid topological structure on the surface of the implant, and is expected to produce novel and efficient orthopedic implants and dental implants.
Owner:SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI

Authentication encryption method, verification decryption method and communication method

PendingCN112187446AResistant to IV (initial vector) reuseSafe and Efficient Robust AEAD MethodKey distribution for secure communicationEncryption apparatus with shift registers/memoriesPlaintextCiphertext
The invention relates to an authentication encryption, verification decryption and communication method, belongs to the technical field of communication, and solves the problems that the robustness ispoor and confidentiality and integrity protection cannot be provided for data at the same time in the prior art. The authentication encryption method of the sending end comprises the following steps:generating a reusable initial vector IV; generating a message authentication code Tag1 according to the plaintext P1 and the affiliated data A in combination with the IV and the shared keys K1 and H;generating a key stream Z1 according to the Tag1 and the IV in combination with the shared key K2; and encrypting the plaintext according to Z1, and sending the obtained ciphertext C and the Tag1, Aand IV to a receiving end. The verification and decryption method of the receiving end comprises the following steps: generating a key stream Z2 according to Tag1 and IV in combination with a shared key K2; analyzing the ciphertext C according to Z2 to generate a plaintext P2; generating a message authentication code Tag2 according to P2 and IV in combination with the shared key K1 and H; and judging whether the Tag1 and the Tag2 are consistent or not, and if so, outputting a plaintext P2. The method provided by the invention has strong robustness, and realizes anti-IV reuse and encryption anddecryption with affiliated data.
Owner:XINGTANG TELECOMM TECH CO LTD

Design method of toe-in control arm

The embodiment of the invention discloses a design method of a toe-in control arm. The design method comprises the following steps: analyzing the performance of a toe-in control arm of a reference vehicle to obtain a performance constraint parameter; determining a design space of an extrusion section of the toe-in control arm to be designed, and performing topological optimization on the extrusionsection based on the performance constraint parameters to obtain a material distribution form of the extrusion section; performing three-dimensional expansion along the thickness direction of the extrusion section to obtain a primary toe-in control arm; optimizing the appearance and the size of the primary toe-in control arm based on the performance constraint parameters to obtain a second toe-incontrol arm; carrying out process analysis on the second-edition toe-in control arm, and continuously adjusting structural parameters of the second-edition toe-in control arm according to an analysisresult to obtain a third-edition toe-in control arm; and performing performance analysis on the third-edition toe-in control arm to obtain performance parameters, and if the performance parameters are qualified, determining the third-edition toe-in control arm as a target toe-in control arm. And the light weight of the toe-in control arm can be effectively realized.
Owner:CHINA FIRST AUTOMOBILE

Preparation method and application of vertically-oriented magnetic nanosheet/sodium alginate composite membrane

The invention discloses a preparation method of a vertical orientation magnetic nanosheet/sodium alginate composite membrane. By means of the magnetic field responsiveness of a magnetic nanosheet, a vertical orientation structure is formed in a magnetic field so as to prepare a high-performance pervaporation composite membrane; wherein the magnetic nanosheets comprise nanosheets with intrinsic magnetic responsiveness or other nanosheets which generate magnetic responsiveness by loading magnetic response particles. The preparation method specifically comprises the following steps: uniformly dispersing magnetic nanosheets, physically blending the dispersion with sodium alginate to form a membrane casting solution, carrying out standing treatment for defoaming, spin-coating the membrane casting solution on a polyacrylonitrile ultrafiltration membrane, drying the composite membrane in a magnetic field at room temperature, and carrying out crosslinking treatment to obtain the magnetic nanosheet/sodium alginate composite membrane with vertical orientation. The preparation method is simple and controllable, and the raw materials are cheap and easily available. The composite membrane is suitable for pervaporation ethanol dehydration, has high permeation flux and high selectivity to water molecules, and has good operation stability at high temperature.
Owner:TIANJIN UNIV
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