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57results about How to "Small mismatch" patented technology

Method for microwave-assisted preparation of CdTeSeS/ZnTe core-shell quantum dot in water

The invention relates to a method for microwave-assisted preparation of a CdTeSeS / ZnTe core-shell quantum dot in water. The method comprises the following steps: 1) preparing a sodium elenosulfate solution; 2) preparing a cadmium chloride solution; 3) adding mercaptopropionic acid into the cadmium chloride solution; 4) adjusting the pH value of the solution; 5) dissolving a sodium tellurite crystal in the solution and simultaneously adding potassium borohydride and the sodium elenosulfate solution; 6) subjecting a mixture obtained in the step 6) to heating reaction in a microwave digestion furnace; 7) carrying out cooling to room temperature and adding isopropanol for purification so as to obtain CdTeSeS quantum dot gel; and 8) preparing a mixed solution of the cadmium chloride solution, the mercaptopropionic acid and the sodium tellurite crystal, dissolving the CdTeSeS quantum dot gel in the mixed solution anew, adding potassium borohydride and successively carrying out heating reaction in the microwave digestion furnace, cooling to room temperature, addition of isopropanol for purification and drying with a lyophilizer so as to obtain solid powder of the CdTeSeS / ZnTe core-shell quantum dot. The method is fast and simple and has easily controllable technological parameters and a low price; and the synthesized quantum dot has uniform particle size distribution, high stability, high fluorescence quantum yield and wide emission spectrum.
Owner:天门市天宝化工科技有限公司

Spiral bevel gear tooth surface Ease-off modification design method based on minimum meshing impact

The invention relates to a spiral bevel gear tooth surface Ease-off modification design method based on minimum meshing impact. According to the method, a small gear tooth surface completely conjugated with a large gear is derived according to a meshing principle, free Ease-off curved surface design is performed according to an inter-tooth gap and tooth surface normal gap generation principle, andthe free Ease-off curved surface design is superposed with a conjugated tooth surface to represent a small gear modification tooth surface. A spiral bevel gear meshing impact model considering gear tooth loading deformation is established; based on gear tooth TCA and LTCA technologies, the actual meshing point position and rigidity of meshing gear teeth are accurately calculated, the actual meshing point is obtained after a theoretical meshing point position vector of a driven wheel rotates by a small angle under a meshing coordinate system, and the theoretical meshing position is determinedby an intersection point of a geometric transmission error curve and a bearing transmission error curve. The minimum maximum meshing impact force and the minimum tooth surface maximum load are taken as optimization targets to obtain an optimal target modified tooth surface. According to the method, the meshing impact force is reduced while the strength is improved under the small adaptation amount, and a theoretical basis is provided for subsequent spiral bevel gear dynamic analysis.
Owner:CHANGAN UNIV

Base pitch error-considered free modification spiral gear bearing contact analysis method

The invention discloses a base pitch error-considered free modification spiral bevel gear bearing contact analysis method, which comprises the steps of designing a free Ease-off curved surface according to a tooth gap and a tooth surface normal gap generation principle, and superposing the free Ease-off curved surface with a conjugate tooth surface to represent a small gear modification tooth surface; calculating the initial clearance of the tooth surface of a single tooth from an engaging-in contact position to an engaging-out contact position according to a TCA technology; superposing the relative base pitch errors of the simultaneous meshing tooth pairs to the initial clearances of the tooth pairs; completing input data processing of the LTCA method of a certain meshing position in a meshing period, and extracting bearing deformation of the corresponding position in the meshing period and contact position loads of different tooth pairs through LTCA calculation, wherein due to the fact that base pitch errors are unequal, the loads of the different meshing positions of a single tooth need to be obtained through multiple times of cyclic calculation; and finally, applying a machinelearning method (EML) to regression fitting of budget of specific working condition bearing deformation under any random error, and providing a more scientific theoretical basis method for high-performance tooth surface dynamic analysis.
Owner:CHANGAN UNIV

Polycrystalline silicon thin film and method for preparing polycrystalline silicon thin film by amorphous silicon low-temperature induction

The invention discloses a method for preparing a polycrystalline silicon thin film by amorphous silicon low-temperature induction, belonging to the technical field of thin-film solar battery. The method overcomes the disadvantage of slow crystallization rate of the existing metal induction method. According to the invention, a titanium silicide nano-wire layer and an amorphous silicon thin film layer are sequentially deposited on a substrate from bottom to top, wherein the titanium silicide nano-wire layer induces the amorphous silicon thin film layer to form a polycrystalline silicon thin film layer, thereby forming a polycrystalline silicon thin film having a three-layer composite structure consisting of the substrate, a transition layer with coexisting titanium silicide nano-wire and polycrystalline silicon thin film, and the polycrystalline silicon thin film layer. On one hand, the crystallization of the amorphous silicon thin film can be induced at a lower crystallization temperature easily since the titanium silicide nano-wire is used as an inducer; on the other hand, the titanium silicide nano-wire with a huge specific surface area can increase the contact area between the induction layer and the amorphous silicon, thereby increasing the nucleation number in the initial crystallization stage of the amorphous silicon and greatly improving the crystallization rate; and the entire crystallization process is completed in 2 to 4 hours.
Owner:HANGZHOU AMPLESUN SOLAR TECH

A kind of epitaxial growth method of yttrium iron garnet film

An epitaxial growth method of a yttrium iron garnet film comprises the following steps: vacuumizing a vacuum cavity with a treated yttrium iron garnet substrate to be 8.6+ / -1*10-6 Pa, and heating the yttrium iron garnet substrate to the constant temperature which is 736 DEG C; in a heating process, feeding ozone when heating to the temperature of 250 DEG C; after heating to the temperature of 736 DEG C, maintaining air pressure of the vacuum cavity, adjusting the mass fraction of the ozone to be 40%, meanwhile insulating for half a hour, and starting a reflective high-energy electron diffraction instrument (RHEED) to adjust so as to obtain diffraction spots of a substrate; maintaining real-time and in-situ monitoring of the RHEED in the whole process, and focusing laser onto a YIG target through a lens by using a KrF excimer laser of which the wavelength is 248 nm; after growth of the film is finished, maintaining the temperature of the substrate unchanged, annealing in situ for 15 minutes, then naturally cooling the film to the temperature about 250 DEG C, stopping protective gas and cooling to the room temperature. The obtained YIG film has uniform components, is controllable in thickness and good in process repeatability, and has high preparation efficiency.
Owner:NANJING UNIV
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