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34results about How to "Adjustable expansion coefficient" patented technology

Glass-ceramics used as ultrahard material grinding wheel bond and preparation method thereof

The invention relates to a microcrystal glass and preparation method used as super-hard grinding wheel bond, which adopts the method that: quartz, boracic acid, alumina, zinc oxide, lithium carbonate, sodium carbonate, potassium carbonate and magnesium carbonate are used as basic glass materials and sodium fluorosilicate is used as nucleation agent, the materials are smelted to form the glass that is quenched and then smashed to glass powder; the glass powder is pressed, molded, and sintered, and crystallized under certain temperature so as to obtain the microcrystal glass; the main crystal phase of the microcrystal glass is fluorophlogopite, the microcrystal is a hexagonal flake structure, the size of the microcrystal is 1um-2um. The microcrystal glass can be used as super-hard grinding wheel bond in place of ceramic so as to improve the strength of super-hard grinding wheel greatly, thereby improving speed and service life of grinding wheel; the invention also has integrated with excellent performances of glass and porcelain enamel, such as wear-resistant, anti-corrosion, good anti-oxidation, excellent electrical property, adjustable expansion coefficient, and good thermal stability. The invention can widely be applied as structural materials, optical materials, and architecture materials.
Owner:HUNAN UNIV

Steel blank grinding abrasion wheel adopting microcrystal ceramic bonding agents

The invention relates to a steel blank grinding abrasion wheel adopting microcrystal ceramic bonding agents, which is in a structure made of polycrystalline solid materials with the coexistence of glass and crystals and adopts the bonding agents of clay, feldspar, boron-containing microcrystal glass, pyrophyllite and soapstone to be made into high-intensity and low-shrinkage engineering ceramic bonding agents, good performance of the glass and the ceramics such as high mechnical intensity, wear resistance, corrosion resistance and the like are integrated, then, the glass and the ceramics are combined with mixed grinding materials, a molding pressing method is adopted for the high-pressure double-side pressing process forming, the low-temperature firing is adopted, the positive pressure reducing atmosphere heat simulation crystallization is adopted at the 800 DEG C heat insulation section, and the mixed grinding material and micro porous glass phase high-intensity microcrystal engineering ceramic composite structure is formed, so the intensity and the bonding degree of the steel blank grinding abrasion wheel are greatly improved, the use linear speed of the abrasion wheel is accelerated, and the safety factor is high. The steel blank grinding abrasion wheel belongs to the novel efficient special steel blank grinding abrasion wheel with the characteristics that the intensity andthe hardness are high, the tissue density is uniform, the grinding ratio is great under the condition of high-speed grinding, workpieces can not be damaged through firing, and the automation of iron and steel industries is easy to realize.
Owner:江苏华东砂轮有限公司

Bismuthate low-melting point and lead-free sealing grass and preparation method thereof

The present invention discloses a bismuthate low-melting point and lead-free sealing grass and a preparation method thereof. The bismuthate low-melting point and lead-free sealing grass powder comprises, by mass, 75-90% of base glass and 10-25% of a filler, wherein the filler is a zirconium phosphate salt with an expansion coefficient of -5*10<-6>k<-1>-5*10<-6>k<-1>. The bismuthate low-melting point and lead-free sealing grass of the present invention has characteristics of lead-free property and green environmental protection, can replace the lead-containing glass so as to eliminate the pollution due to the lead, and has excellent chemical stability. The production process is simple and the cost is low. Compared to other filler-doped sealing glass powders, the sealing temperature of the present invention is low, the glass transition temperature of the present invention is 330-370 DEG C, the softening temperature of the present invention is 370-410 DEG C, the sealing temperature of the present invention is less than 450 DEG C. With adjusting the proportion of the filler, the adjustable expansion coefficient can be realized at the low sealing temperature, wherein the adjustment range is (70-90)*10<-7>/DEG C, such that different requirements of the sealing device to the expansion coefficient of the sealing material can be met, and the sealing for VFD, PDP, CRT and other glass products can be directly performed.
Owner:CHINA JILIANG UNIV

Preparation methods of diamond/silicon carbide prefabricated part and diamond/silicon carbide/aluminium compound material

The invention provides preparation methods of a diamond / silicon carbide prefabricated part and a diamond / silicon carbide / aluminium compound material. The methods comprise the following steps that 1, silicon carbide powder and diamond powder are mixed according to a mass ratio of 5:2, and after continuous and even mixing, micro diamond powder is obtained; 2, a binder is added into the micro diamondpowder to obtain mixed powder; 3, a diamond prefabricated part green body obtained in last step is subjected to sintering to prepare the diamond / silicon carbide prefabricated part; 4, in a differential-pressure casting furnace, the diamond / silicon carbide prefabricated part is impregnated with aluminium alloy liquid, so that the diamond / silicon carbide / aluminium compound material is obtained. Thediamond / silicon carbide / aluminium compound material prepared through the method has the characters of being low in density, adjustable in expansion coefficient, high in heat conductivity, high in elasticity modulus, good in gas tightness and low in cost, and can be widely applied to the micro-electronics fields of hybrid integrated circuits, millimeter wave / micron wave integrated circuits, multi-chip modules, high current and power IGBT modules and the like.
Owner:XIAN AERONAUTICAL UNIV

Ce-containing low-temperature sealing glass as well as preparation and application method of Ce-containing low-temperature sealing glass

The invention discloses Ce-containing low-temperature sealing glass as well as preparation and application method of the Ce-containing low-temperature sealing glass. The Ce-containing low-temperature sealing glass consists of the following raw materials: B2O3, Bi2O3, ZnO and Ce(NO3)3 in a molar ratio of (10-50):(20-40):(5-30):(0-30). Through the coordination between high-concentration Bi2O3 and B2O3, the softening temperature of glass is lowered, so that low-temperature sealing is realized; Ce<3+> in a glass network prepared by melting quenching is transformed into Ce<4+>, the transformation of Bi<3+> in glass into Bi<5+> is prevented, and the refractive index of glass is stabilized; and Ce not only can further lower the softening temperature of the sealing glass, but also can adjust the expansion factor of the glass so as to remarkably improve the sealing property of the sealing glass. Moreover, Ce remarkably reduces the surface tension of the glass, improves the interface bonding property between the sealing glass and an alloy connector and is applicable to the field of photoelectric materials and other low-temperature precise sealing. According to the invention, the preparation raw materials are simple and easily available, the cost is low, the technology is simple and feasible, and the prepared low-temperature sealing glass has good performance and stable refractive index and meets the conditions of practical utilization and industrialization.
Owner:FUZHOU UNIV

Cement-based grouting material

The invention discloses a cement-based grouting material, and belongs to the technical field of building materials. The cement-based grouting material is prepared according to the following steps: melting asphalt powder, performing high-voltage electrostatic spinningto obtain asphalt raw threads, soaking the asphalt raw threads in a potassium permanganate solution, performing oxidation to obtain oxidized asphalt fibers, mixing nano magnesium oxide, a silane coupling agent and an ethanol solution, performing ultrasonic dispersion, adding the oxidized asphalt fibers, performing mixing under stirring, adding tetraethoxysilane dropwise, performing mixing under stirring, performing filtering, performing washing, performing drying, and performing carbonizing to obtain modified asphalt fibers; mixing aluminum powder and glycerol under stirring, adding wheat gluten powder, performing mixing under stirring, adding water, performing swelling, allowing the obtained material to stand, and performing ultrasonic dispersion to obtain a modified aluminum powder dispersion liquid; and mixing cement, quartz sand, water, a water reducing agent, fly ash, mineral powder, slag, a defoaming agent, a water retaining agent, the modified asphalt fibers and the modified aluminum powder under stirring to obtain the cement-based grouting material. The cement-based grouting material obtained by the technical scheme has the advantages of good fluidity, early-stage strength and expansion performance.
Owner:郭迎庆

Laser welding layer prefabricated part and preparation methods for laser welding layer prefabricated part and aluminum silicon carbide box body

The invention discloses a laser welding layer prefabricated part and preparation methods for the laser welding layer prefabricated part and an aluminum silicon carbide box body. The preparation methodfor the aluminum silicon carbide box body comprises the steps that 1, the laser welding layer prefabricated part is prepared; 2, the laser welding layer prefabricated part and a silicon carbide prefabricated part are laminated and matched; 3, an aluminum silicon carbide green body with the laser welding layer is prepared through vacuum air pressure infiltration; and 4, machining is carried out. The laser welding layer prefabricated part is formed by pressing particle-reinforced aluminum alloy powder, specifically, aluminum alloy powder is placed in a graphite mold, the graphite mold comprisesa female mold and a male mold, the aluminum alloy powder is laid at the bottom of the female mold, a hydraulic machine applies pressure of 0.5-2 MPa to the aluminum alloy powder in the female mold through the male mold and maintains the pressure to form the laser welding layer prefabricated part, wherein the particle size of the particle-reinforced aluminum alloy powder is 10-200 microns. A laserwelding layer is designed at the upper end of the aluminum silicon carbide box body, so that the laser welding problem between the aluminum silicon carbide box body and a cover plate is effectively solved, and the air tightness of the box body after sealing welding is ensured.
Owner:SOUTHWEST CHINA RES INST OF ELECTRONICS EQUIP

High-temperature-resistant coating for automotive upholstery and preparation method of high-temperature-resistant coating

The invention belongs to the technical field of high-temperature-resistant coatings, and particularly relates to a high-temperature-resistant coating for automotive upholstery and a preparation methodthereof. The high-temperature-resistant coating is prepared from, by weight, 30-60 parts of organic silicon resin, 4-7 parts of epoxy resin, 3-5 parts of amino resin, 6-10 parts of nano zirconium oxide dispersion liquid, 1-3 parts of aluminum tripolyphosphate, 13-15 parts of low-melting-glass powder, 3-8 parts of talcum powder, and 2-5 parts of mica powder. The heat resistance of the prepared high-temperature-resistant coating is obviously improved, the high-temperature-resistant coating can resist the high temperature of 500 DEG C, the coating has high strength and good high-temperature resistance and wear resistance by adding the nano zirconium oxide dispersion liquid component, and the coating has excellent weather resistance and corrosion resistance by adding the aluminum tripolyphosphate and the low-melting-point glass powder component; and by adding the barium sulfate and the nano zirconium diboride, the wear resistance, the high temperature resistance and the corrosion resistance of the coating are further improved, and the comprehensive performance is excellent.
Owner:清远威凛材料科技有限公司

High-strength corrosion-resistant glass glaze for automobiles and preparation method of high-strength corrosion-resistant glass glaze

The invention discloses a high-strength corrosion-resistant glass glaze for automobiles and a preparation method of the high-strength corrosion-resistant glass glaze, and relates to the field of glass glaze. A lead-free environment-friendly low-melting-point glass flux is prepared by researching a ternary glass system and introducing lead-free low-melting-point raw materials to serve as a glass binder, so that the melting temperature of the glass flux is reduced, low-melting-point glass powder is induced to crystallize when the automobile glass is tempered by pre-crystallizing the bismuth silicate crystal nucleus, the tempered glass glaze layer has good adhesion resistance and acid resistance, the copper chromite black is added as a black agent, the copper chromite black has good black hue, the advantages of excellent durability, high temperature resistance, very stable chemical properties, light resistance, weather resistance, acid-base resistance, solvent resistance, no migration, easy dispersion and the like are achieved, and the expansion coefficient can be regulated by introducing the low-expansion-coefficient raw material into the low-melting-point glass system so as to achieve the high adaptability with the automobile glass.
Owner:JIANGSU BAIFU TECH CO LTD

A kind of CE-containing low-temperature sealing glass and its preparation and use method

ActiveCN106495487BLow softening temperatureAchieve low temperature sealingHigh concentrationExpansion factor
The invention discloses Ce-containing low-temperature sealing glass as well as preparation and application method of the Ce-containing low-temperature sealing glass. The Ce-containing low-temperature sealing glass consists of the following raw materials: B2O3, Bi2O3, ZnO and Ce(NO3)3 in a molar ratio of (10-50):(20-40):(5-30):(0-30). Through the coordination between high-concentration Bi2O3 and B2O3, the softening temperature of glass is lowered, so that low-temperature sealing is realized; Ce<3+> in a glass network prepared by melting quenching is transformed into Ce<4+>, the transformation of Bi<3+> in glass into Bi<5+> is prevented, and the refractive index of glass is stabilized; and Ce not only can further lower the softening temperature of the sealing glass, but also can adjust the expansion factor of the glass so as to remarkably improve the sealing property of the sealing glass. Moreover, Ce remarkably reduces the surface tension of the glass, improves the interface bonding property between the sealing glass and an alloy connector and is applicable to the field of photoelectric materials and other low-temperature precise sealing. According to the invention, the preparation raw materials are simple and easily available, the cost is low, the technology is simple and feasible, and the prepared low-temperature sealing glass has good performance and stable refractive index and meets the conditions of practical utilization and industrialization.
Owner:FUZHOU UNIV

A kind of glass-ceramic solder and its preparation method and method for connecting ferrite

The invention discloses microcrystalline glass brazing filler metal, a preparation method thereof and a method for connecting ferrite and belongs to the technical field of ferrite brazing connection.The microcrystalline glass brazing filler metal, the preparation method thereof and the method for connecting the ferrite aim to solve the problem that due to long-time use, the performance stabilityof a microwave ferrite device is affected. The brazing filler metal (20-x) Li2O-xY2O3-35Fe2O3-(20-y)BaO-25SiO2-yCr2O3 is prepared by adopting a fusing-cold quenching method. The method for connectingthe ferrite includes the steps that yttrium ferrite is pretreated, the microcrystalline glass brazing filler metal is adjusted to be in a uniform paste shape with terpilenol, and then the portion between to-be-connected faces of the pretreated yttrium ferrite is uniformly coated with the microcrystalline glass brazing filler metal in a silk-screen printing method to form a to-be-welded part, and drying is performed; and then pressure is applied to the to-be-welded part, brazing treatment is performed, cooling with a furnace is performed, and then ferrite connection is completed. Strength of aconnection joint acquired through the microcrystalline glass brazing filler metal is high and is (90-100MPa), the thermal stability and the corrosion resistance of the joint are improved, and therefore the service life of the ferrite device is prolonged, and the using period stability of the ferrite device is improved.
Owner:HARBIN INST OF TECH

Chemical slip casting strengthening material and preparation method thereof

The invention relates to a chemical slip casting strengthening material and a preparation method thereof. A chemical slip casting strengthening material with two components (component A and component B) is provided, thus effectively solving the problems existing in conventional chemical slip casting materials, such as slow polyurethane polymerization, poor flame retardation and environment pollution. When the chemical slip casting material is used, the component A, i.e. phenolic resin, and the component B, i.e. curing agent, are mixed according to a weight ratio of 1:1. The phenolic resin is obtained by firstly mixing phenol and formaldehyde according to a weight ratio of 1:1.3-1.5, then adding the catalyst NaOH, heating the mixture to a temperature of 90-100 DEG C, causing the reaction to last 4-6 hours, carrying out neutralization and dehydration, cooling the mixture to 25 DEG C and adding foaming agent and surfactant for full mixing. The curing agent consists of 0.6-1.0 part of p-toluenesulfonic acid by weight, 0.8-1.3 parts of phosphoric acid by weight, 0.5-1.0 part of hydrochloric acid by weight and 0.1 part of ethylene glycol by weight. The chemical slip casting material needs a short time for solidification, has an inflaming retarding oxygen index higher than or equal to 54, and is suitable for the slip casting strengthening engineering of a mine, as well as the seepage-proofing, leaking stoppage and strengthening work of an ordinary underground engineering or a water conservancy engineering.
Owner:廊坊鑫美源化工建材有限公司

A kind of laser welding layer preform and preparation method thereof and aluminum silicon carbide box body

The invention discloses a laser welding layer preform and a method for preparing the same and an aluminum silicon carbide box body, comprising steps 1: preparing a laser welding layer preform; step 2: laminating and matching the laser welding layer preform and the silicon carbide preform ; Step 3: vacuum pressure infiltration to prepare an aluminum silicon carbide body with a laser welding layer; Step 4: perform mechanical processing; the laser welding layer preform is pressed from particle-reinforced aluminum alloy powder, specifically the The aluminum alloy powder is placed in a graphite mold, and the graphite mold includes a concave mold and a convex mold, the aluminum alloy powder is spread on the bottom of the concave mold, and the hydraulic press applies 0.5-2MPa to the aluminum alloy powder in the concave mold through the convex mold. The particle size of the particle-enhanced aluminum alloy powder is 10-200 μm, and the laser welding layer is designed on the upper end of the aluminum silicon carbide box to effectively solve the problem of aluminum carbonization. The laser welding problem between the silicon box body and the cover plate ensures the airtightness of the box body after sealing and welding.
Owner:SOUTHWEST CHINA RES INST OF ELECTRONICS EQUIP
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