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31results about How to "Avoid reunion situations" patented technology

Alloy powder homogenizing treatment method for flux-cored wire

The invention discloses an alloy powder homogenizing treatment method for a flux-cored wire. The alloy powder homogenizing treatment method comprises the following steps of: S1, keeping the basic requirements for the grain size of used primary raw material powder, and keeping the grain size of a to-be-added little secondary powder raw material to be smaller than 100 meshes, thereby forming a powdered raw material; S2, adopting a pelletizing adhesive which is a sodium silicate solution diluted by adding water, wherein the pelletizing adhesive needs to add with 20-70% of water to dilute for use;S3, adding the adhesive and the powdered raw material into a stirrer to stir, wherein adding amount of the adhesive and weight percentage of the powdered raw material are smaller than 30%; S4, uniformly mixing the adhesive with the powdered raw material to obtain a mixture, then, taking out the mixture to spread on a heat-resistant steel disc to sinter and dry; and S5, crushing and sieving to a required mesh number, using a 40-50-mesh screen to screen, thereby completing a pelletizing process for the screened powder. The alloy powder homogenizing treatment method realizes modifying flux-coredwire powder, and further improves uniformity of the added alloy, so that the expected grain refinement or other metallurgical effects are achieved.
Owner:SUZHOU U P WEAR RESISTANCE COMPOUND MATERIALS

High-conductivity lithium iron phosphate powder and preparation method thereof

The invention discloses high-conductivity lithium iron phosphate powder and a preparation method thereof. The preparation method comprises the steps as follows: 1) formation of precursor of high-conductivity lithium iron phosphate: a lithium hydroxide solution is stirred and mixed with phosphoric acid; a graphene oxide dispersion liquid is added and stirred; iron sulfate heptahydrate is added and stirred, and a uniform mixture is obtained; the mixture is filtered, washed and dried, and black powder, namely, the precursor of the high-conductivity lithium iron phosphate, is obtained; 2) formation of high-conductivity lithium iron phosphate powder: the precursor, obtained in the step 1), of high-conductivity lithium iron phosphate and lithium carbonate are subjected to ball milling and uniformly mixed, the mixture is calcined in the atmosphere of inert gas, and the high-conductivity lithium iron phosphate powder is obtained. The lithium iron phosphate powder prepared with the method has high conductivity, large specific surface area and higher compaction density, has the particle size of 0.5-1 mu m, has 1-5 layers of graphene and has the iron-phosphorous ratio of 0.95-1.05, and a produced pole piece has the surface resistance of 60 omega and has wide application prospects in the lithium ion battery field.
Owner:THE SIXTH ELEMENT CHANGZHOU MATERIALS TECH

Adsorption arsenic removal catalyst and preparation method thereof

The invention discloses a catalytic cracking gasoline adsorption dearsenification catalyst with large specific surface area, hierarchical pore distribution and high dearsenification performance and a preparation method thereof, and the method comprises the following steps: 1) mixing active carbon and pseudo-boehmite in proportion, grinding, stirring, adding a pore-enlarging agent and an acid solution, extruding into strips, drying, and roasting under an anaerobic condition to prepare a carbon-alumina composite carrier; (2) adjusting the pH value of the metal precursor solution, and impregnating the solution containing the active metal precursor into the carrier by adopting an isovolumetric saturated impregnation method; and 3) drying the catalyst, and roasting in an oxygen-free environment to obtain the finished product catalyst. The carrier with a composite pore channel structure can improve diffusion, reaction and escape of reactant molecules in pore channels, and the reaction efficiency is improved; metal with partially filled d tracks is selected as active metal, so that the acting force between the arsenide and the metal can be improved, and the arsenide is deeply removed; the pH value of the metal precursor solution is adjusted to be higher than the isoelectric point of the metal oxide or hydroxide, the acting force between the metal and the carrier can be weakened, the dispersity of the metal is improved, and finally the arsenic removal efficiency of the catalyst is improved.
Owner:PETROCHINA CO LTD

Electrically conductive organic polymer coated phenolic resin-based porous carbon composite material

The invention relates to an electrically conductive organic polymer coated phenolic resin-based porous carbon composite material. A preparation method for the material comprises the following steps: (1) water-soluble phenolic resin and curing agent are orderly added in an anhydrous alcohol solution to obtain a mixture; after stirring and curing operation, a cured phenolic resin is obtained; (2) phenolic resin microspheres obtained in step (1) are carbonized and calcined in an inert gas atmosphere at a temperature of 850 to 950 DEG C to obtain phenolic resin-based porous carbon; (3) the phenolic resin-based porous carbon obtained in step (2) is added to a 30-60 ml acetone solution, and then a surfactant is added to obtain a mixed solution after ultrasonic dispersion. Electrically conductivepolymer monomers are ultrasonically dispersed in an acetone solution to obtain an electrically conductive polymer monomer acetone solution. The electrically conductive polymer monomer acetone solution is added dropwise to the mixed solution, microwave hydrothermal reaction was performed, and the electrically conductive organic polymer coated phenolic resin-based porous carbon composite material with high specific capacity, specific energy density, and good cycle stability is obtained.
Owner:ENERGY RESOURCES INST HEBEI ACADEMY OF SCI

A kind of highly conductive lithium iron phosphate powder and preparation method thereof

ActiveCN107403902BReduce agglomeration defectsReduce reunionElectrode thermal treatmentIron sulfateLithium oxide
The invention discloses high-conductivity lithium iron phosphate powder and a preparation method thereof. The preparation method comprises the steps as follows: 1) formation of precursor of high-conductivity lithium iron phosphate: a lithium hydroxide solution is stirred and mixed with phosphoric acid; a graphene oxide dispersion liquid is added and stirred; iron sulfate heptahydrate is added and stirred, and a uniform mixture is obtained; the mixture is filtered, washed and dried, and black powder, namely, the precursor of the high-conductivity lithium iron phosphate, is obtained; 2) formation of high-conductivity lithium iron phosphate powder: the precursor, obtained in the step 1), of high-conductivity lithium iron phosphate and lithium carbonate are subjected to ball milling and uniformly mixed, the mixture is calcined in the atmosphere of inert gas, and the high-conductivity lithium iron phosphate powder is obtained. The lithium iron phosphate powder prepared with the method has high conductivity, large specific surface area and higher compaction density, has the particle size of 0.5-1 mu m, has 1-5 layers of graphene and has the iron-phosphorous ratio of 0.95-1.05, and a produced pole piece has the surface resistance of 60 omega and has wide application prospects in the lithium ion battery field.
Owner:THE SIXTH ELEMENT CHANGZHOU MATERIALS TECH

High-conductivity flexible touch graphene composite material and preparation method thereof

InactiveCN108795042AAvoid reunion situationsOptimize the conductive network structureCarbon nanotubePotassium
The invention relates to a high-conductivity flexible touch graphene composite material and a preparation method thereof. The high-conductivity flexible touch graphene composite material comprises thefollowing components: 20 to 25 parts of graphene hydrosol, 5 to 8 parts of aluminum powder, 1 to 10 parts of carbon nanotube, 0.3 to 0.4 part of potassium carboxymethylcellulose, 10 to 14 parts of polyimide, 6 to 8 parts of polydimethylsiloxane, and 0.2 to 0.45 part of zirconium dioxide powder. The preparation method comprises the following step: mixing all the components, so as to form the high-conductivity flexible touch graphene composite material. The method is simple in technology, effectively avoids the situation of agglomeration caused by large specific surface area of graphene powderthrough the added the graphene hydrosol, optimizes a conductive network structure in the composite material through the added zirconium dioxide powder and a potassium carboxymethylcellulose dispersingagent, further improves the electrical conductivity of the composite material while enhancing the ductility of the composite material through the added aluminum powder, and meets the application requirements on flexible touch materials by current electronic devices.
Owner:TIANJIN BAOXINGWEI TECH

Tin selenide nanosheet array/carbon cloth composite negative electrode material structure for sodium ion battery

The invention provides a tin selenide nanosheet array / carbon cloth composite negative electrode material structure for a sodium ion battery, and belongs to the technical field of nano materials and batteries. The negative electrode material structure is prepared by adopting a simple vacuum thermal evaporation technology, and tin selenide powder is heated to a certain temperature in a vacuum environment to sublimate and deposit on carbon cloth to form a tin selenide nanosheet array, so that the composite negative electrode material structure is formed. The tin selenide nanosheet array uniformly covers the surface of the carbon cloth, so that each nanosheet can contribute effective capacity, the agglomeration phenomenon of a powder material can be effectively avoided, and the specific capacity and the cycling stability of the material are improved. And the composite negative electrode structure has the flexibility of the carbon cloth, and the conductivity of the composite negative electrode structure is improved by the carbon cloth. Compared with a traditional battery negative electrode material, the structure does not need to use a binder and a conductive agent, can be directly used as a sodium ion battery negative electrode, has high specific capacity and has a good application prospect.
Owner:GUANGDONG UNIV OF TECH

Multifunctional thin film for energy storage device and preparation method thereof

The invention relates to a multifunctional thin film for an energy storage device and a preparation method. The preparation method comprises the following steps: firstly, dispersing a graphene-based material, a metal-organic framework material or a precursor of the metal-organic framework material into a solvent respectively; obtaining a graphene-based material dispersion liquid, a metal-organic framework material dispersion liquid or a precursor dispersion liquid of the metal-organic framework material respectively; mixing the graphene-based material dispersion liquid with the metal-organic framework material dispersion liquid or the precursor dispersion liquid of the metal-organic framework material to obtain a mixed system; transferring the mixed system to a planar substrate; and removing the solvent to obtain the multifunctional film for the energy storage device. On the premise of ensuring good wettability, the prepared thin film also has good multiplying power and cycle performance, has good tensile strength and puncture resistance, is suitable for new energy storage devices, and overcomes the defects that a traditional thin film is poor in mechanical performance, poor in electrolyte wettability, complex in preparation process and the like.
Owner:LUOYANG NORMAL UNIV
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