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37results about How to "Good fiber shape" patented technology

Biocompatible nano-conductive fiber and preparation method thereof

InactiveCN101805938AReasonable formReasonable morphology is better, the distribution of carbon nanotubes in the fiberElectroconductive/antistatic filament manufactureFilament/thread formingCarbon nanotubeBiocompatibility Testing
The invention discloses a biocompatible nano-conductive fiber and a preparation method thereof. The biocompatible nano-conductive fiber comprises the following three components in part by mass: 100 parts of polylactic acid, 5 to 10 parts of carbon nano tubes and 1 part of sodium dodecyl sulfate. The three components are prepared into spinning solution by utilizing compound solvents, i.e. chloroform and dimethyl sulfoxide, and an electrostatic spinning device is used to spray to prepare the biocompatible nano-conductive fiber, wherein the fiber diameter is between 200 and 500nm; the carbon nano tubes are coated uniformly with the polylactic acid and are orderly arrayed in the fiber; the surfaces of the carbon nano tubes are subjected to hydroxylation; the mass percentage of hydroxy is 3.06 weight percent; the diameter of the carbon nano tubes is between 10 and 20nm; the length of the carbon nano tubes is 30mum; the purity of the carbon nano tubes is over 95 weight percent; and the specific surface area of the carbon nano tubes is over 200m<2>/g. The invention has advanced and simple process and reasonable formula. The prepared nano-conductive fiber has good biocompatibility and has wide application prospect.
Owner:YANGZHOU UNIV

Chemical warfare agent self-disinfection MOF (metal organic framework) fiber filtering membrane and preparation method thereof

The invention provides a chemical warfare agent self-disinfection MOF (metal organic framework) fiber filtering membrane and a preparation method thereof. The preparation method comprises the following steps of performing electrostatic spinning calcining to prepare a zirconium oxide fiber film; mixing with a corresponding organic ligand and an activated acid solution, and performing hydrothermal reaction, so as to obtain the self-disinfection MOF fiber filtering membrane. The prepared self-disinfection MOF fiber filtering membrane has the advantages that the additional support material is notneeded, the self ultra-large specific surface area of MOFs is maintained, and the adsorption capacity and catalytic property are excellent; by adopting the micro-nano multi-stage structure, the reaction matter is favorably transmitted, the catalytic sites are exposed, and the agglomeration of the catalyst is avoided; the excellent self-disinfection property is realized; the degrading conversion rate of a simulating matter of a chemical warfare agent is high, the half-life period is short, and the stability in cyclic use is good; by adopting the thin film form, the self-disinfection MOF fiber filtering membrane can be directly applied into the actual filtering protection device.
Owner:SHANDONG UNIV

Polylactic acid-polyethylene glycol coated florfenicol nanofiber and preparation method thereof

The invention relates to polylactic acid-polyethylene glycol coated florfenicol nanofiber and a preparation method thereof, belonging to the technical fields of veterinary drugs and preparation thereof. The polylactic acid-polyethylene glycol is segmented copolymer D, L-polylactic acid-polyethylene glycol-D, L-polylactic acid; and florfenicol is filled in a reticular structure of polylactic acid-polyethylene glycol, and mass ratio of the florfenicol to the polylactic acid-polyethylene glycol is 1: (3.5-10). The preparation method comprises the steps of adding the polylactic acid-polyethylene glycol and the florfenicol into an organic solvent, stirring and dissolving to obtain a spinning solution; and then carrying out electrostatic spinning to obtain a polylactic acid-polyethylene glycol coated florfenicol nanofiber membrane. The preparation method provided by the invention realizes drug loading while carrying out electrostatic spinning on the polylactic acid-polyethylene glycol, and solves the problems such as sudden release of drugs, short action time and poor water solubility; and the adopted raw materials cannot cause the problem of environmental protection after degradation, the cost is low, the preparation process is simple and quick, and the polylactic acid-polyethylene glycol coated florfenicol nanofiber and the preparation method are applicable to mass production.
Owner:JILIN UNIV

Preparation method of acrylic board surface lining protective body paper

The invention discloses a preparation method of acrylic board surface lining protective body paper. The preparation method comprises following steps: by weight, 3 to 10 parts of cellulase, 1 to 8 parts of pectase, 3 to 10 parts of xylanase, 0.1 to 0.8 part of an alkylolamide, 0.1 to 0.6 part of Span-60, and 75.7 to 88.8 parts of water are combined to prepare a composite bio-enzyme preparation; byweight, 1 to 5 parts of a mixed pulpboard is introduced into a pulper, 95 to 99 parts of water is added, the composite bio-enzyme preparation is added, and defibering is carried out for 5 to 30min soas to obtain a mixed slurry, wherein the adding amount of the composite bio-enzyme preparation accounts for 100 to 300ppm of the weight amount of absolutely dry paper pulp; the mixed slurry is introduced into a pulping machine for pulp refining, pulping concentration ranges from 1 to 4%, and pulp refining is carried out until beating degree is 20 to 45 DEG SR; obtained paper pulp is subjected to dilution, screen moulding, squeezing, drying, and curling processing so as to obtain a finished product. According to the preparation method, the composite bio-enzyme preparation at an optimal ratio isadded in body paper pulp refining process, so that paper pulp beating degree is increased, pulp refining time is shortened, energy consumption is reduced, pollution is reduced, the ratio of fiber morphological substances in paper pulp is improved, and body paper object amount index is increased obviously.
Owner:浙江蓝宇新材料有限公司

Nanofiber coated with polylactic acid-polyethylene glycol and preparation method thereof

The invention relates to polylactic acid-polyethylene glycol coated florfenicol nanofiber and a preparation method thereof, belonging to the technical fields of veterinary drugs and preparation thereof. The polylactic acid-polyethylene glycol is segmented copolymer D, L-polylactic acid-polyethylene glycol-D, L-polylactic acid; and florfenicol is filled in a reticular structure of polylactic acid-polyethylene glycol, and mass ratio of the florfenicol to the polylactic acid-polyethylene glycol is 1: (3.5-10). The preparation method comprises the steps of adding the polylactic acid-polyethylene glycol and the florfenicol into an organic solvent, stirring and dissolving to obtain a spinning solution; and then carrying out electrostatic spinning to obtain a polylactic acid-polyethylene glycol coated florfenicol nanofiber membrane. The preparation method provided by the invention realizes drug loading while carrying out electrostatic spinning on the polylactic acid-polyethylene glycol, and solves the problems such as sudden release of drugs, short action time and poor water solubility; and the adopted raw materials cannot cause the problem of environmental protection after degradation, the cost is low, the preparation process is simple and quick, and the polylactic acid-polyethylene glycol coated florfenicol nanofiber and the preparation method are applicable to mass production.
Owner:JILIN UNIV

Method for preparing polyvinyl alcohol BiVO4 composite fiber by electrostatic spinning method

The invention provides a method for preparing polyvinyl alcohol BiVO4 composite fiber by an electrostatic spinning method. The method comprises the following steps of: firstly adding Bi(NO3)3.5H2O and citric acid monohydrate in deionized water and stirring evenly, and then adding ethanolamine and continuously stirring to be clear so as to obtain a solution A; then adding ammonium metavanadate and the citric acid monohydrate in the deionized water to obtain orange mixed liquid, stirring at the constant temperature of 70 DEG C to enable the color of the mixed liquid to turn into dark blue without precipitation, and obtaining a solution B; mixing the solution B and the solution A, and stirring to obtain a precursor solution; then evenly mixing the precursor solution and a polyvinyl alcohol solution binding agent to prepare an electrostatic spinning solution; and finally putting the electrostatic spinning solution into a syringe to start spinning, and collecting the prepared polyvinyl alcohol BiVO4 composite fiber by a receiver. The preparation method provided by the invention is simple and convenient, low in energy consumption and cost, and environmentally-friendly, the prepared polyvinyl alcohol BiVO4 composite fiber has good dispersibility, and nanofiber with good appearance can be obtained in a high-voltage electric field.
Owner:SHAANXI UNIV OF SCI & TECH

A Fabrication Method of Flexible and Stretchable Devices Based on Ordered Arrangement and Twisted Structures

InactiveCN104153128BAccurate realization of pre-strain controlAchieve pre-strain controlNew-spun product collectionFilament/thread formingPre strainElectrospinning
The invention belongs to the technical field of flexible device manufacturing, and relates to a method for manufacturing a flexible stretchable device based on an ordered arrangement torsion structure. The method includes the steps that firstly, a flexible macromolecule substrate is pre-stretched to be fixed to a glass sheet, and electrodes are manufactured at the four edges of the pre-stretched flexible macromolecule substrate; secondly, the flexible macromolecule substrate is placed on an annular metal collector connected with the negative electrode of a power source to serve as a collecting substrate, and a machined hollow stainless steel needle serves as a spinning spraying head; a spinning solution is injected into a spinning solution container for electrospinning; the flexible macromolecule substrate is horizontally rotated by 90 degrees for continuous electrospinning and then taken down from the glass sheet, and the flexible stretchable device based on an ordered arrangement torsion structure is obtained. The method is simple in manufacturing process and convenient to operate; the manufactured flexible stretchable device can be stressed and tensioned in one or two of the two-dimensional directions respectively, pre-strain control over materials in the two directions can be accurately achieved, and the application range is wide.
Owner:QINGDAO UNIV

Graphene/polysiloxane spun fiber membrane and preparation method thereof

The invention provides a graphene / polysiloxane spun fiber membrane and a preparation method thereof. The preparation method comprises the following steps of dispersing graphene in a silane dilute solution, and performing a stirring reaction to obtain a graphene suspension; uniformly mixing graphene turbid liquid with a multifunctional silane monomer, adding a catalyst, performing a hydrolysis pre-polycondensation reaction, and removing small molecules under reduced pressure to prepare a prepolymer; dissolving the prepolymer in an organic solvent to prepare a polymer spinning solution; and carrying out electrostatic spinning. According to the preparation method, the polycondensation degree, the crosslinking degree and the structure of the polysiloxane prepolymer for spinning are regulated and controlled, a polysiloxane sol-gel chemical process in a short time of electrostatic spinning is accurately controlled, and graphene is supplemented for supporting and enhancing the fiber performance, so that the graphene / polysiloxane spun fiber membrane is prepared, and the technical difficulty of curing forming of polysiloxane spun fiber is overcome. The prepared fiber membrane has important application prospects in the fields of electrochemistry, catalysis, sensors, adsorption and separation, flexible electronic elements and medical engineering.
Owner:SHANDONG UNIV

Lasting mutually promoting and win-win developing implementation scheme for wood plastic production, resource exploitation and environment protection

The invention relates to a lasting mutually promoting and win-win developing implementation scheme for wood plastic production, resource exploitation and environment protection. The scheme is characterized in that: osier is planted in low-lying areas which are easy to be flooded, and sword iris is planted in saline-alkali lands; osier powder and sword iris fiber are used for replacing wood powder, such that the lasting mutually promotion and win-win development of wood plastic production, low-lying flooded area treatment, saline-alkali land treatment and ecological environment protection can be realized. With the scheme, wood plastic production is changed from a dependant industry into a leading industry; the dependence of wood plastic base material on wood is solved; a problem of insufficient biomass base material is solved; a history that wood products are dependant on deforestation is ended; the performance of wood plastic material is improved; wood plastic composite material with light weight and high toughness is produced; and ecological environment is obviously improved. With the scheme, an integral production system of osier powder, sword iris fiber and wood plastic composite material is established; and problems in each link can be coordinated and solved scientifically and quickly. Therefore, a lasting mutually promotion and win-win development of wood plastic production, resource exploitation and environment protection can be ensured.
Owner:翟云升
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