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45results about How to "Good stability at room temperature" patented technology

Detecting method and detecting kit for immunosuppressive agents in dried blood spots

InactiveCN109030673AApplicable common detectionEfficient detectionComponent separationEverolimusLinear regression
The invention discloses a detecting method for immunosuppressive agents in dried blood spots, and further discloses a detecting kit for the immunosuppressive agents in the dried blood spots. The detecting method comprises the steps that the standard curve dried blood spots and the to-be-detected dried blood spots are mixed with an extracting solution and an internal standard solution correspondingly and then extracted, centrifuging is conducted, and supernate is taken; the supernate is blown dry and then redissolved through a redissolving solution, and detecting is conducted through a tandem mass spectrum method; according to the peak exceeding area specific value of standard samples to an internal standard object and the concentration of the standard samples, linear regression is conducted to obtain a standard curve equation of the immunosuppressive agents; the peak exceeding area specific value of to-be-detected samples to the internal standard object is substituted into the standardcurve equation, and the content of the immunosuppressive agents in the to-be-detected samples is calculated; the extracting solution is a water solution of methyl alcohol and/or acetonitrile; and theimmunosuppressive agents are one or more of cyclosporine A, tacrolimus, sirolimus and everolimus. The detecting method can effectively detect the four types of immunosuppressive agents simultaneously, and thus the detecting efficiency is improved.
Owner:易达精准(杭州)科技有限公司

Method for improving stability of copper ion ink and conductivity of copper film

InactiveCN106833130AEasy to store and transportTaking into account room temperature stabilityInksIonSolvent
The invention discloses a method for improving the stability of copper ion ink and the conductivity of a copper film. The method comprises the following steps: dissolving a mixed ligand of anhydrous organic acid copper salt, alkylamine and hydramine in an anhydrous alcohol solvent, adding an alcohol-soluble binding agent to obtain a uniform and stable ink stock solution, adding a certain proportion of water prior to ink jet printing to prepare ink, printing the ink on a substrate in a ink jet printing manner, and performing heating and reduction in nitrogen to obtain the conductive copper film. The method adopts anhydrous organic acid copper salt and the anhydrous solvent and adjusts proportions of alkylamine and hydramine, so that the ink stock solution with good room temperature stability can be prepared, has no deterioration for at least three months, and is convenient to transport and store; an appropriate amount of water is added prior to the printing to prepare the ink to be printed into a pattern; the copper film with high conductivity can be obtained by the heating and the reduction in the nitrogen after drying; and the resistivity of the copper film obtained by the reduction at below 250 DEG C is only 3-10 times of that of bulk copper. The method is easy and simple to operate, and gives consideration to the room temperature stability of the ink and the high conductivity of the copper film.
Owner:TSINGHUA UNIV

Aerogel flame-retardant microsphere for high nickel ternary lithium battery electrolyte and preparation method

InactiveCN108461754AGood stability at room temperatureGood high temperature sustainable flame retardancyCell electrodesMicrosphereInternal resistance
The invention belongs to the field of lithium batteries, and provides an aerogel flame-retardant microsphere for a high nickel ternary lithium battery electrolyte and a preparation method. The methodcomprises the steps that an aerogel flame-retardant microsphere inner layer material, namely, graphene oxide aerogel loaded nanometer magnesium hydroxide for the high nickel ternary lithium battery electrolyte is prepared; graphene oxide aqueous dispersion is atomized into a graphene oxide droplet microsphere through electrostatic spraying, distribution of graphene oxide in the microsphere body ofthe graphene oxide droplet microsphere formed through electrostatic spraying is extremely uniform, collection is conducted in an organic mixture, and a good sphere is obtained. By means of an ordinary spraying or fluidized bed, an aluminum hydroxide colloid is stuck to the surface of the microsphere and dried, and the aerogel flame-retardant microsphere for the high nickel ternary lithium batteryelectrolyte is obtained. The microsphere has the good normal temperature stability and high temperature sustainable flame retardance. In addition, at high temperature or in the burning process, graphene oxide aerogel makes contact with the electrolyte to form a circuit, the electrode internal resistance is increased, and the electrode voltage is lowered.
Owner:CHENDU NEW KELI CHEM SCI CO LTD

Preparation method, product and application of lead-free halogen microcrystal

The invention relates to a preparation method of a lead-free halogen micron crystal as well as a product and application of the lead-free halogen micron crystal, and belongs to the technical field of preparation of the lead-free halogen micron crystal. The invention discloses a preparation method of a lead-free halogen micron crystal, which comprises the following steps: dissolving silver chloride (AgCl) and rubidium chloride (RbCl) in dimethyl sulfoxide, and extracting by an anti-solvent method to obtain the Rb2AgCl3 lead-free halogen micron crystal. The Rb2AgCl3 lead-free halogen microcrystal is prepared by using a normal temperature method and has the advantages of simple experimental steps and easiness in operation, compared with lead-containing halide, the prepared Rb2AgCl3 lead-free halogen microcrystal solves the problem of toxicity of lead, and particularly compared with cesium-lead-bromine, the luminous quantity of the Rb2AgCl3 lead-free halogen microcrystal prepared by the method is higher than that of cesium-lead-bromine under X rays when the Rb2AgCl3 lead-free halogen microcrystal is used as a scintillator material, and the service life of the Rb2AgCl3 lead-free halogen microcrystal is prolonged. And the process for preparing the micron crystal powder into the film is simple, and after the film is prepared, materials in the film are uniformly distributed, so that the imaging effect is better.
Owner:CHONGQING UNIV
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