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103results about How to "High degree of sphericity" patented technology

Method for preparing fracturing propping agent special for shale gas from fly ash

The invention relates to a method for preparing a fracturing propping agent special for shale gas from fly ash. The method comprises the following steps of: performing wet grinding on the fly ash, kaolinite, a high-activity compound sintering aid and a small amount of industrial coke to form mixed slurry in a ball mill; performing primary granulation on the mixed slurry in a fluidized bed spray granulator; performing secondary granulation by using powdered coal slurry formed by wet grinding of coke as coating liquid; putting balled granules into a crucible; and putting the crucible into an electric furnace for ultralow temperature self-propagating sintering, cooling naturally and then taking the crucible out of the electric furnace to obtain the fracturing propping agent special for shale gas. By adopting the method, the raw material has a wide source, the temperature of the self-propagating sintering is low, the sintering period is short, energy resources are saved, a low-carbon environmental protection effect is achieved, and the comprehensive performance of the product is improved; a shaping method adopted in the method is low in energy consumption, the production process is simple and easy to control, and the product quality is stable; and the prepared propping agent is low in density and high in strength, has excellent characteristics of high-temperature resistance and corrosion resistance, and can provide a fracturing material with better performance for medium and deep layer shale gas fields.
Owner:SHAANXI UNIV OF SCI & TECH

Plasma-etching-resistant granulated yttrium oxide for hot spraying and preparation method thereof

The invention belongs to the technical field of hot spraying, and particularly relates to plasma-etching-resistant granulated yttrium oxide for hot spraying and a preparation method thereof. The preparation method of the plasma-etching-resistant granulated yttrium oxide for hot spraying comprises the following steps: preparing nano or ultrafine yttrium oxide powder and deionized water or an organic solution into a paste, performing depolymerization and reduction, adding surface activity activator into the paste for preparation, and performing hot expansion balling and high-temperature densification treatment to obtain the granulated yttrium oxide for hot spraying. According to the invention, the surface activity activator is added into the paste before hot expansion balling, so that the prepared granulated yttrium oxide for hot spraying is favorable in spherical degree, and the high-spherical-degree favorable-flowability high-density granulated yttrium oxide for hot spraying can be obtained without later spheroidization, thereby achieving favorable flowability during hot spraying, ensuring that the supply of the granulated yttrium oxide for hot spraying is more stable, and providing a guarantee for obtaining a hot spray coating having a uniform thickness.
Owner:CHANGZHOU GEOQUIN NANO NEW MATERIALS

Method for preparing Na4Fe3 (PO4) 2 (P2O7) by homogeneous phase method and application

The invention discloses a method for preparing Na4Fe3 (PO4) 2 (P2O7) by a homogeneous method and an application, and the preparation method comprises the following steps: mixing a carbon source, an iron source, a sodium source and a phosphorus source according to a certain stoichiometric ratio, adding an organic solvent, and sanding to form a homogeneous dispersion system; and carrying out spray drying to obtain a precursor, and sintering the precursor in an inert atmosphere to obtain Na4Fe3 (PO4)2(P2O7) powder. According to the method, the agglomeration phenomenon of the Na4Fe3 (PO4) 2 (P2O7) micro-nano powder can be remarkably improved, the morphology and the electrical performance of the powder are improved, the used organic solvent can be recycled through a cooling system for secondary utilization, the latent heat of vaporization of the organic solvent is far lower than that of water, and the heating power consumption is reduced. Compared with the existing transition metal oxide, Prussian blue and vanadium-based polyanionic compound positive electrode materials, the Na4Fe3 (PO4) 2 (P2O7) positive electrode material prepared by the invention is lower in cost, better in cycling stability, green and pollution-free, and can provide an ideal positive electrode for a commercial sodium ion battery.
Owner:HUBEI WANRUN NEW ENERGY TECH DEV

Microwave ablation antenna

The invention provides a microwave ablation antenna. The antenna is provided with an antenna body, the antenna body comprises an inner conductor, and the outer side of the inner conductor is sequentially covered with a dielectric, an outer conductor and a shell; the antenna body extends in the axial direction, one end of the antenna body is used for being connected with a coaxial cable, the otherend of the antenna body is an antenna tail end, and the portions, at the antenna tail end, of the outer conductor and the inner conductor protrude out of the dielectric and are welded to each other; three gaps are girdled in the portion, close to the antenna tail end, of the outer conductor; the dielectric in the middle of the antenna body is axially and sequentially provided with a dielectric hollowed-out section and a thickened outer conductor extending inwards from the outer conductor. According to the microwave ablation antenna, the large ablation long diameter and ablation sphericity areobtained through a three gap joint, the ablation radius is increased through the cooperation with a pi matching joint, the comet tail effect can be well eliminated under the condition of not increasing the diameter of the antenna, the ablation sphericity is increased, the sphericity of an ablation area cannot be significantly reduced even if the microwave power is increased, and the large-range high-sphericity ablation area can be formed.
Owner:EAST CHINA UNIV OF SCI & TECH

Preparation method of novel fracturing propping agent-polymer sand

The invention provides a preparation technology of novel fracturing propping agent-polymer sand. The preparation method comprises the following steps: 1) adding styrene, divinyl benzene, a latent active monomer and an initiator into water filled with an organic/inorganic dispersant, stirring the components, heating the mixture to 70-100 DEG C, carrying out suspension polymerization reaction for 4-12 hours, and filtering, washing and drying a reaction product to obtain an intermediate product polymer microsphere; and 2) carrying out a thermal cross-linking reaction for 10-120 min at a temperature of 180-230 DEG C. The organic proppant polymer sand has the characteristics that 1) the organic proppant polymer sand is high in compressive strength at high temperature, good in temperature resistance and not easy to break; 2) a flexible latent active monomer is introduced into a molecular chain to improve the toughness and crosslinking degree of the product and reduce the dosage of a crosslinking agent, and 3) the product not only has the advantages of simple preparation and use of an organic proppant, but also has the characteristics of high temperature resistance and high strength of aninorganic proppant, and obviously improves the flow conductivity of fracturing exploitation of oil and gas fields.
Owner:BEIJING UNIV OF CHEM TECH
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