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58results about How to "Increase the reaction interface" patented technology

Stannic selenide/graphene oxide negative pole composite material for sodium ion battery and preparation method thereof

The invention discloses a stannic selenide / graphene oxide negative pole composite material for a sodium ion battery and a preparation method thereof. The negative pole composite material is formed by uniformly growing nanometer stannic selenide on the surface of graphene oxide. The preparation method comprises the following steps of: ultrasonically dispersing graphene oxide powder into a mixed solution of water and ethylene glycol to obtain a dispersion solution; adding tin salt and selenite to the dispersion solution, then carrying out hydrothermal reaction, and placing a hydrothermal reaction product into an inert gas protective tube furnace for heat treatment so as to obtain a negative pole composite material which has nanometer sheet-like morphology and is formed by uniformly growing nanometer stannic selenide on the surface of graphene oxide. The composite material disclosed by the invention can be used for preparing the sodium ion battery which has the characteristics of high discharging specific capacity, excellent magnification property, long cycle life and the like. The preparation method disclosed by the invention has the advantages of simplicity, reliability, good process repeatability, high operability, low cost and suitability for industrialized production.
Owner:CENT SOUTH UNIV

Concrete sealing curing agent

ActiveCN106699006ABack alkali reductionPrevent back alkalinityLithiumEpoxy
The invention provides a concrete sealing curing agent. The concrete sealing curing agent is prepared from a component A and a component B, which are packaged independently, wherein the component A is prepared from the following components in percentage by weight: 20 weight percent to 25 weight percent of sodium silicate, 5 weight percent to 15 weight percent of poly-lithium silicate, 5 weight percent to 15 weight percent of silica sol, 3 weight percent to 7 weight percent of a photocatalyst, 0.5 weight percent to 1 weight percent of a penetrating agent, 0.5 weight percent to 1 weight percent of a surfactant, 0.4 weight percent to 0.6 weight percent of a surface modifier, 0.4 weight percent to 0.6 weight percent of a de-foaming agent and the balance of de-ionized water; the component B is prepared from the following components in percentage by weight: 0.2 weight percent to 0.6 weight percent of graphene, 25 weight percent to 45 weight percent of organic silicon modified water-based epoxy resin, 5 weight percent to 15 weight percent of silica sol, 0.1 weight percent to 2 weight percent of a catalyst, 0.1 weight percent to 3 weight percent of a stabilizer and the balance of de-ionized water. The concrete sealing curing agent provided by the invention has the advantages of reasonable design, high rigidity, high permeability, good wearing resistance and good waterproof performance, and also has a protection effect on concrete.
Owner:湖北省路桥集团有限公司

Method for continuously preparing polyester polyol and device used in method

The invention discloses a method for continuously synthesizing polyester polyol and a device used in the method. A solid raw material, namely acid or acid anhydride, and liquid polyol are used for synthesizing the polyester polyol in the presence of a catalyst. The method comprises the following steps of: preheating to melt the solid raw material for synthesizing the polyester polyol or slurryingin an alcoholic solution to obtain slurry, adding the catalyst, injecting the slurry into a slurry tank, metering by using a first metering pump, adding into a reaction kettle into which part of polyol is put in advance, starting a circulating pump to ensure that reaction liquid in the reaction kettle is circulated and fully reacted, and reacting according to the conventional steps under the conventional reaction conditions; and when an acid value is less than 1mgKOH / g, starting a second metering pump, continuously adding the polyol for reaction into the reaction kettle, continuously adding the slurry in the slurry tank into the reaction kettle, opening a discharge port at the upper end, and continuously discharging. The raw material is fluidized in advance, so that a high specific surface area and pipeline liquidity are achieved, and continuous feeding is facilitated.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY

Process for preparing benzoic ether plasticizer by using slurry method

The invention relates to a process for preparing a benzoic ether plasticizer by using a slurry method. In the process, benzoic acid and alcohol react in the presence of a catalyst to produce a benzoic ether plasticizer. The process is characterized by comprising the following steps of: slurrying solid granular, powdery or blocky raw material benzoic acid in alcohol; after the slurrying is finished, adjusting the mole ratio of the alcohol to the benzoic acid to be (1-4):1; then mixing with a conventional catalyst which accounts for 0.1-0.2% of the mass of the raw material benzoic acid, raisingthe temperature to 210-240 DEG C gradually while stirring in a reactor with an oil-water separator, reacting for 1-4h under heat insulation and ending the reaction till the acid value is lower than 1; and then performing conventional dealcoholization and purification treatment to obtain the benzoic ether plasticizer. The invention has the advantages that the original solid benzoic acid raw material is slurried under the condition that original equipment is not necessary to change completely, therefore, the reaction contact area of two phases is increased, the reaction speed is increased greatly, the efficiency is increased and the energy is saved.
Owner:JIANGSU QIANGLIN BIO ENERGY +1

Solar cell electrode, preparation method therefor, and solar cell

InactiveCN105702472ASolve a series of contradictions that cannot be balancedRealize a series of contradictions that cannot be balancedLight-sensitive devicesPhotovoltaic energy generationMicro nanoElectronic transmission
The invention relates to the technical field of solar energy capturing and conversion, and discloses a solar cell electrode, a preparation method therefor, and a solar cell comprising the electrode. The solar cell electrode has a double-layer titanium oxide micro-nano structure, wherein the lower layer is a one-dimensional nanowire array which vertically grows on a transparent conductive glass substrate, and the upper layer is a three-dimensional dendritic micro-nano ball structure stacked on the one-dimensional nanowire array. The design of the novel electrode successfully avoids a series of contradiction which cannot be considered by a conventional electrode. Compared with a conventional photoelectrode, the electrode has a large electronic transmission free path, is high in visible light absorption efficiency, has a large photoelectric conversion reaction interface, can achieve one-step integration, has an electron flow and high-reaction interface for the preparation of the solar cell with the high photoelectric conversion ratio, meets the requirements for strong scattering and absorption of visible light, greatly improves the overall performance of the solar cell, and speeds up the industrial transformation of this type of new energy devices and the final large-scale industrialized application.
Owner:PEKING UNIV SHENZHEN GRADUATE SCHOOL

Fuel oil preparation technique utilizing waste plastics

The invention discloses a fuel oil preparation technique utilizing waste plastics. The preparation technique comprises the following steps: the waste plastics are chopped, the chopped waste plastics are added into a cracking kettle, a catalyst and quartz sand are added, and the materials are heated at a heating rate of 5 to 10 DEG C per minute after uniform stirring and mixing; the materials are heated within different temperature ranges through temperature control to achieve a slow reaction, and condensates within the different temperature ranges are respectively collected; after the mixed cracking reaction is completed, the collected liquid fuel oils are respectively sent to a rectifying tower for rectification, and fraction products within the different temperature ranges are respectively collected; the fractions captured from the rectifying tower respectively undergo extraction separation through a complexation extraction solvent. The technique provided by the invention has the advantages that the quartz sand is added into the reaction kettle, so as to achieve uniform heating of the reaction materials, enlarge the reaction contact surface, and reduce the phenomena of wall sticking and coking of the materials under a high temperature; the fuel oil yield is high, and the fuel oil quality is stable; the technique is simple to operate, so as to facilitate scale production.
Owner:云浮市力道新能源科技有限公司

Preparation method of lithium-ion battery

The invention discloses a preparation method of a lithium-ion battery. The method comprises a preparation process of positive paste and negative paste, wherein the positive paste and the negative paste are prepared through the process of mixing, soaking, dispersion and flocculation of a positive raw material and a negative raw material; the positive paste contains, by weight, 80-90 parts of a nickel-cobalt-manganese ternary material, 1-5 parts of a binder and 5-20 parts of a conductive agent; and the negative paste contains polytetrafluoroethylene which is added according to the proportion of60% of negative raw material paste, wherein the 60% of polytetrafluoroethylene contains 2 parts of carboxymethylcellulose. According to the method, the nickel-cobalt-manganese ternary material is adopted as the positive raw material of the lithium-ion battery first, the positive raw material is made into appropriate paste through pretreatment of the positive material and the paste making process of mixing, soaking and flocculation, and the positive paste is spread on an aluminum thin film to form the intact lithium-ion battery in cooperation with the functions of the negative material, an electrolytic solution and a membrane. The battery has the advantages that discharge voltage is high, safety is good, and repeated discharge can be performed multiple times cyclically.
Owner:泰顺永庆电力技术有限公司

Zero-discharge system for desulfurization wastewater

The invention discloses a zero-discharge system for desulfurization wastewater. The zero-discharge system comprises a boiler, a dust remover and a desulfurization tower, which are arranged in sequence; a drying tower is arranged between the boiler and the dust remover; and a rotary atomizer is arranged on the tower top of the drying tower. The rotary atomizer rotates at a high speed and wastewatergenerated by the desulfurization tower is sprayed into the drying tower by the rotary atomizer; and an air flow diversion device is arranged in the drying tower, exhaust gas generated by the boiler enters the drying tower through an exhaust gas inlet and forms a downwards rotating air flow under the diversion of the air flow diversion device, and the rotating direction of the air flow is oppositeto the rotating direction of the rotary atomizer. The zero-discharge system for the desulfurization wastewater provided by the invention is used for wastewater treatment, in which the desulfurizationwastewater is directly atomized by the rotary atomizer and instantaneously evaporated by the hot exhaust gas in the drying tower, therefore no sludge is produced and no heating is needed in the process, so that the construction cost and the running cost of the zero-discharge system for the desulfurization wastewater are greatly reduced.
Owner:江苏海澜正和环境科技有限公司

Process for preparing benzoic ether plasticizer by using slurry method

The invention relates to a process for preparing a benzoic ether plasticizer by using a slurry method. In the process, benzoic acid and alcohol react in the presence of a catalyst to produce a benzoic ether plasticizer. The process is characterized by comprising the following steps of: slurrying solid granular, powdery or blocky raw material benzoic acid in alcohol; after the slurrying is finished, adjusting the mole ratio of the alcohol to the benzoic acid to be (1-4):1; then mixing with a conventional catalyst which accounts for 0.1-0.2% of the mass of the raw material benzoic acid, raisingthe temperature to 210-240 DEG C gradually while stirring in a reactor with an oil-water separator, reacting for 1-4h under heat insulation and ending the reaction till the acid value is lower than 1; and then performing conventional dealcoholization and purification treatment to obtain the benzoic ether plasticizer. The invention has the advantages that the original solid benzoic acid raw material is slurried under the condition that original equipment is not necessary to change completely, therefore, the reaction contact area of two phases is increased, the reaction speed is increased greatly, the efficiency is increased and the energy is saved.
Owner:JIANGSU QIANGLIN BIO ENERGY +1

Silicon-carbon negative electrode material and preparation method thereof

The invention provides a silicon-carbon negative electrode material and a preparation method thereof, belonging to the technical field of material preparation. The method specifically comprises the following steps: step 1, putting a nanoscale graphite substrate into a chamber of a settling device, and conducting sufficient heating to remove moisture under the protection of nitrogen gas; step 2, introducing a gas mixture of inert gas containing a silicon source and hydrogen at a high temperature, and uniformly settling nanoscale elemental silicon generated by a reaction in the graphite base mentioned in the step 1 under high-temperature catalysis; and step 3, introducing a gas carbon source into a silicon-carbon composite negative electrode material prepared in the step 2 under the protection of inert gas, and performing sintering treatment with a temperature controlled to be 400-600 DEG C, thereby finally obtaining the carbon-coated silicon-carbon negative electrode material. The novelpreparation method provided by the invention is simple, and the whole preparation process is completed in one step; and a prepared sample does not need to be transferred and prepared multiple times,and the whole preparation process is short in time and can be completed within 24 hours.
Owner:南京同宁新材料研究院有限公司

Low-concentration flue gas desulfurization method for hydroelectric silicon smelting

The invention discloses a low-concentration flue gas desulfurization method for hydroelectric silicon smelting. The method comprises the following steps: 1) preparing absorption slurry, namely fully uniformly mixing a desulfurization adsorbent ground to the granularity of 325-400 meshes and water so as to obtain the absorption slurry; 2) absorbing acid gas, namely enabling the absorption slurry and flue gas to be fully contacted in a desulfurizing tower when flue gas during hydroelectric silicon smelting enters a desulfurization system, so that acid gas and particles in the flue gas are absorbed by the absorption slurry; and 3) discharging the flue gas, namely detecting the emission concentration of SO2 at the outlet, discharging the SO2 while meeting requirements, if not, returning to thedesulfurization system to treat, filtering the absorption slurry after absorption, and returning the filtrate to the step (2) to serve as absorption liquid, and taking the filter residues as by-products for sales, thereby obtaining the product. According to the method disclosed by the invention, limestone and other desulfurization adsorbents are mixed with water to prepare the absorption slurry,the flue gas enters the desulfurization system to be fully contacted with the slurry, and the acid gas and particles are removed, so that the emission concentration of sulfur dioxide in the flue gas is reduced to 80mg/Nm3, and green and environmental-friendly production is effectively realized.
Owner:云南永昌硅业股份有限公司

Method for continuously preparing polyester polyol and device used in method

The invention discloses a method for continuously synthesizing polyester polyol and a device used in the method. A solid raw material, namely acid or acid anhydride, and liquid polyol are used for synthesizing the polyester polyol in the presence of a catalyst. The method comprises the following steps of: preheating to melt the solid raw material for synthesizing the polyester polyol or slurrying in an alcoholic solution to obtain slurry, adding the catalyst, injecting the slurry into a slurry tank, metering by using a first metering pump, adding into a reaction kettle into which part of polyol is put in advance, starting a circulating pump to ensure that reaction liquid in the reaction kettle is circulated and fully reacted, and reacting according to the conventional steps under the conventional reaction conditions; and when an acid value is less than 1mgKOH / g, starting a second metering pump, continuously adding the polyol for reaction into the reaction kettle, continuously adding the slurry in the slurry tank into the reaction kettle, opening a discharge port at the upper end, and continuously discharging. The raw material is fluidized in advance, so that a high specific surface area and pipeline liquidity are achieved, and continuous feeding is facilitated.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY
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