6 results about "Methyl t-butyl ether" patented technology

The utility model discloses a methyl tert -butyl ether sampling detection device relates to methyl tert -butyl ether technical field, including the extraction pipe, the surface fixedly connected with the pivot of extraction pipe, the surface of extraction pipe is opened with the square hole, the fixedly connected with the discharge gate of extraction pipe surface square hole department, the outside of pivot is inserted with the connecting shaft, the outside rotation is connected with the collection box of connecting shaft, the surface fixedly connected with the baffle of collection box. The utility model through baffle divides the inside of collection box into several cabins, through with the specified cabin corresponding mark rotates to the display hole department, then will sample liquid extraction to the inside of extraction pipe, then will device upset, then to the one side rotation limit rod of fixed plate arc shape, through the spring's elasticity, will piston rod push back, and stop moving at the front side of spacing septum, and the sample of extraction flows into the specified cabin inside due to the action of gravity, then rotates the knob to the next mark department again, thereby realizes the sample of multiple extraction and separates storage.

This invention discloses a solvate of rememega-2 and its preparation method. The rememega-2 solvate (compound II) provided by this invention has a purity of up to 99.15% compared with the existing rememega-2 methyl tert-butyl ether solvate. The preparation method includes the following steps: adding crude rememega-2 to a binary solvent, heating to 45℃~75℃, adding an antisolvent, stirring, crystallizing, cooling and filtering, and drying under reduced pressure to obtain rememega-2 solvate (compound II). Then, placing rememega-2 solvate (compound II) in ethanol and stirring to obtain rememega-2 (compound I). This route is simple to operate, the process is stable, and it is easy to scale up. Moreover, the rememega-2 (compound I) prepared by this solvate (compound II) has a purity of up to 99.66%, which is higher than that of rememega-2 (compound I) prepared by the existing rememega-2 methyl tert-butyl ether solvate. It also has better fluidity, does not caking, is easy to transfer, and is convenient for later production.

This invention relates to the fields of environmental and bioanalytical technology, and particularly to a method for simultaneous pretreatment and detection of bisphenol S and bisphenol AF in biological tissues. The technical solution includes a framework process for simultaneous pretreatment and detection of bisphenol S and bisphenol AF in biological tissues. This invention establishes a dual-solvent secondary extraction system composed of n-hexane and methyl tert-butyl ether, achieving differentiated adaptation to different tissue matrices. By combining the advantages of non-polar and moderately polar solvents, it can simultaneously handle the relatively highly polar bisphenol S and the relatively non-polar bisphenol AF in a single extraction process. Furthermore, this method sets key physical parameters during the extraction process according to the histological characteristics of each organ. For heart and lung tissues, specific ultrasonic power is used to ensure thorough cell disruption; while for liver and spleen with high lipid content, different power and time are used to ensure the full release of lipid-bound target substances.

The utility model relates to the methyl tert -butyl ether recovery field especially relates to a recovery unit for methyl tert -butyl ether, including recovery box, rectangular frame no.

The application belongs to the technical field of environmental monitoring and analytical chemistry, and discloses a detection method for the content of methyl tert-butyl ether in soil. The method uses surface functionalized mesoporous silica adsorbent for solid phase extraction, combines ultrasonic assisted extraction with gas chromatography-mass spectrometry analysis, the adsorbent has a pore size of 2.5-4.0 nm, and a surface grafted with bifunctional ligands containing tertiary amine groups and short chain alkyl groups, and has high selectivity and adsorption capacity for methyl tert-butyl ether; the mass spectrometry detection adopts double ion confirmation and intensity ratio criterion, effectively eliminating the interference of structural analogues. Through the design of special adsorption materials, the optimization of the pretreatment process and the construction of the mass spectrometry confirmation logic, the application realizes high sensitivity, high selectivity and high reproducibility detection of trace methyl tert-butyl ether, and can be widely applied to industrial pollution site investigation, farmland soil safety evaluation, groundwater pollution tracing and emergency monitoring of environmental incidents.

This invention discloses a catalytic synthesis process for methyl tert-butyl ether, belonging to the field of etherification catalytic synthesis technology. The main raw materials are methanol and pre-ether C4. By introducing mesoporous silica in situ into a strongly acidic cation exchange resin and loading sulfonic acid imidazole trifluoromethanesulfonate ionic liquid into the ion exchange resin, a composite catalyst with a multi-level pore structure is formed, thereby significantly improving the utilization rate of acidic sites inside the catalyst. The resulting modified catalyst can be used in the etherification reaction of methyl tert-butyl ether and subsequent catalytic distillation process, so that the reaction equilibrium continuously shifts towards the product, thereby improving the overall conversion rate of the etherification reaction. This process also improves the raw material conversion rate and product purity through the synergistic effect of reaction and separation, and realizes the recycling of raw materials by combining a methanol recovery system. This process has high reaction efficiency, good catalyst stability, and is suitable for large-scale industrial continuous production.