85results about How to "Reduce the amount of acid and alkali" patented technology

The invention discloses a manufacturing technique of yeast gluglucosan to decompose yeast cellar wall conjugase under high temperature, which compriss the following steps: adopting yeast cell wall as raw material; adding water with weight rate at 1:3-1:8 to make suspension; heating to 105-150 deg.c for 1-6h; cooling; diluting; centrifuging; washing for 2-3 times; removing sediment; adding water with rate at 1;15-1:25; heating to 30-40 deg.c; adjusting pH value to 9-11; stirring; adding proteinase; enzymolyzing 2-6h; neutralizing; centrifuging; washing; disposing through excessive ketone; filtering; washing residual for three times through ketone; freezing sediment at -70 deg.c for 22h; freezing sediment at -60 deg.c for 6-10h; obtaining the product.

The technical scheme for xylose preparation with enzyme comprises: using CGMCC1476 as a Aspergillus niger strain to ferment and prepare excision xylanase that has high activity and needs mild reaction condition; enzymolyzing specially corn core and zylan in straw materail; refining to prepare single-xylose with purity more than 90%. This invention has no pollution to environment and conversion more than 80%.

The invention discloses an extraction method of deep-sea fish skin gelatin, and the method comprises the following steps of putting cleaned fish skin in conditioning fluid which is prepared from compound organic acid and stirring, cleaning the conditioned fish skin by water at room temperature, putting the cleaned fish skin in weakly acidic water solution at 30-60 DEG C for extraction, combining the extracting solution, filtering the extracting solution by 100-mesh filter cloth, and carrying out concentration and drying to obtain the gelatin. The method provided by the invention is gentler, and the prepared product is high in yield and purity, large in molecular weight, narrow in molecular weight distribution, shallow in color and light in fishy smell.

The invention provides a system and a method for treating sewage. The system comprises a thick grid, a water collecting tank, a fine grid, a rotational flow sand settling tank, a regulating tank, an emergency tank, a coagulation sedimentation tank, gas flotation equipment, an intermediate water tank, ultra-filtration equipment, a concentrated water regulating tank, a multistage coagulation sediment, an A2O biochemical tank, an inclined-tube sedimentation tank, a fiber turntable filter tank, a sludge concentrated water tank, a sludge dewatering room, a disinfection tank and a water recycling tank. The system and the method have the advantages that diversified processes for treating the sewage are combined with one another to form the complete system for treating the sewage, accordingly, different stages of sewage can be assuredly effectively treated, and treatment effects can be improved; outlet water treated by the aid of the system is high in quality, requirements of national emission indexes can be met, the outlet water can be applied to life again, and accordingly water resources can be reused.

The invention discloses an extracting agent, an extraction system and an application. The extracting agent comprises 2-ethylhexyl phosphonic acid mono-ethylhexyl ester and di-(2-ethylhexyl) phosphinic acid. The extraction system comprises an organic phase and a water phase, wherein the organic phase comprises a diluent and the extracting agent; the water phase comprises rear-earth ions; and the pH value of the water phase is 1.0-3.0. The extraction system disclosed by the invention can effectively improve extraction and reverse extraction performances of a P507 extraction system, is good in separating capacity on heavy rear-earth elements, capable of carrying out extraction and reverse extraction under relatively low acidity and reducing dosage of acid and alkali, more green and environmentally-friendly, low in cost, high in saturation capacity, free of an emulsion phenomenon and more suitable for practical industrial production.

The invention relates to a chemical process, which is a new extraction process of L-proline, and provides the new extraction technology of the L-proline. The new extraction technology of the L-proline comprises the step of filtering a fermentation liquor through a ceramic membrane to obtain filter clogging liquid, and is characterized by decoloring the filter clogging liquid, and obtaining a finished product through ion exchange for less than or equal to two times. The new extraction technology of the L-proline has the beneficial effects that the acid-base dosage and the water discharge are reduced, energy conservation, consumption reduction and emission reduction are realized, the cost is greatly reduced, the finished product yield is high, and the quality is good.

The invention discloses a production process of glutamic acid and monosodium glutamate, which comprises the following steps: firstly, evaporating and concentrating fermentation liquid; after concentrated sulfuric acid is added for isoelectric operation, cooling to 5-15 DEG C; obtaining an alpha-crystalline glutamic acid crystal suspension after primary separation, primary crystal washing, secondary separation and secondary crystal washing; regulating the pH value to be 4.0-5.0 at 80-90 DEG C, cooling to 35 DEG C, and obtaining a beta-crystalline glutamic acid crystal through filtration and separation, wherein the beta-crystalline glutamic acid crystal can be dried by air flow to obtain glutamic acid products, and the beta-crystalline glutamic acid crystal can be continuously neutralized and refined to obtain monosodium glutamate products; carrying out cyclone precipitation on primary mother liquid after primary separation, removing protein in supernatant liquid by flocculation air flotation process, and drying the protein to obtain bacterial protein powder; and carrying out ion exchange on the deproteinized clear liquid to prepare compound fertilizer. The extraction method of the glutamic acid provided by the invention fundamentally reduces the generation of waste water, improves the extraction yield and the product quality, reduces the amount of water for exchanging ions and washing columns to the minimum, and has higher production efficiency and lower production cost.

The invention discloses a method for producing xylo-oligosaccharide by utilizing cotton seed hulls, which adopts the cotton seed hulls as raw materials and comprises the steps: the cotton seed hulls are dipped in a dilute sulphuric acid solution according to a solid-to-liquid ratio of 1 to 10, pretreated at room temperature for 20-24 hours, treated in high pressure steam at temperature of 180-190 DEG C for 7-15 minutes, cooled down by water to 50 DEG C and then added with 1.0-2.5% xylanase for enzymolysis for 24-36 hours in slow stirring or vibration manner, after being boiled for 10 minutes to remove enzyme, enzymatic hydrolyzate is filtered and concentrated in a vacuum manner till sugar concentration is more than 75 percent to obtain the xylo-oligosaccharide syrup. The method is characterized in that the cotton seed hulls with more xylose content of xylan is adopted as raw materials; pretreatment is conducted to effectively remove coloring matters; high pressure processing can greatly shorten time; the technological process of xylo-oligosaccharide production is simple and practical, with relatively low production cost; and the production technique and method of xylo-oligosaccharide have good industrialized application prospect.

The invention discloses an iron-carbon micro-electrolysis process for introducing ozone and treating waste water. The iron-carbon micro-electrolysis process comprises the following steps: S1, adjusting the pH of the waste water to 2 to 9 by utilizing an acid solution/alkali solution; S2, filtering the waste water with the pH of 2 to 9 in S1, outputting the waste water into an iron-carbon micro-electrolysis reactor, introducing ozone into the iron-carbon micro-electrolysis reactor, reacting for 1h to 3h, and discharging the waste water out of the iron-carbon micro-electrolysis reactor; and S3,transporting the waste water outputted from the iron-carbon micro-electrolysis reactor into a neutralizing precipitating pond to be precipitated. Compared with the prior art, the iron-carbon micro-electrolysis process has the beneficial effects that the treatment capacity for organic matters in the waste water can be improved, the color reversion phenomenon can be well overcome, the pH range of the waste water entering the iron-carbon micro-electrolysis reactor can be enlarged, the consumption of acid and alkali can be reduced, the generation amount of the neutralized precipitated sludge is reduced, and the comprehensive treatment cost of the waste water can be reduced.

The invention relates to chitin extraction, in particular to a method for cleaning comprehensive utilization of shrimp and crab shell waste. The method includes the steps of steam explosion, wherein shrimp shells and / or crab shells are soaked in water, placed in steam explosion equipment, treated at 1.4MPa-2.4MPa for 60-600s, dried and crushed; decalcification, wherein shrimp shell and / or crabshell powder is treated with a decalcifying agent at 20-80 DEG C for 60-300min, filtering is conducted, a filtrate A is obtained, a solid material is washed with water, and drying is conducted; deproteinization, wherein the shrimp shell and / or crab shell powder is treated with a lye at 60-100 DEG C for 90-300min, filtering is conducted to obtain a filtrate B, the solid material is washed with water, and drying is conducted; the shrimp shells and / or the crab shells are treated according to the sequence of the steam explosion, the decalcification and the deproteinization or the steam explosion, the deproteinization and the decalcification to obtain the chitin. The method improves the separation efficiency of the chitin and reduces the amount of acid and alkali and waste discharge.

A post-extraction method for fermentation-process epsilon-polylysine production is provided, belonging to the technical field of extraction and separation. The method mainly includes extracting epsilon-polylysine in a fermentation solution by utilizing an electrodialysis technique and a membrane separation technique. The method specifically includes: subjecting the fermentation solution to solid liquid separation through ceramic membrane filtration after the fermentation solution is subjected to thermal flocculation; then removing soluble macromolecule substances through filtration with an ultrafiltration membrane; performing decoloration with activated carbon; performing filtration to obtain a decolorized solution; subjecting the decolorized solution to electrodialysis treatment; pumpinga dialysis liquid product to a nanofiltration membrane device and performing cyclic concentration; subjecting the concentrate to spray drying or vacuum freeze drying to obtain an epsilon-polylysine product. Compared with traditional ion exchange extraction methods, the method when being used for epsilon-polylysine extraction enables a product recovery rate of 80% or above, and product purity of 98% or above; and the method can save water by 60% and reduce the environment protection cost by 50% for products per ton after the electrodialysis technique is adopted to replace a traditional ion exchange technique. The method has advantages of capability of reducing wastewater generation, a high degree of automation, a high extraction and recovery rate and high purity of extract products, and issuitable for industrial production.

The invention discloses a glutamic acid extraction process, which comprises heating glutamic acid fermenting liquor, ultra-filtering, and filtering with a nano-filter system, heating the fermenting liquid, adjusting the pH value to 3.0-4.0 with sulfuric acid, concentrating by evaporation in a crystallizer pan; and discharging to a crystallization promoting tank when 50%-80% of water is evaporated off, slowly cooling to a temperature below 60 DEC C, and centrifugally separating glutamic acid. The glutamic acid extraction process has small usage amount of acid and alkali, less waste water amount, and higher extraction efficiency of the glutamic acid. The obtained glutamic acid is ensured that the product quality reaches the national standard.

The invention discloses an extraction system, an extraction method and a reextraction method. The extraction system disclosed in the invention comprises an organic phase and an aqueous phase, wherein the organic phase comprises a diluent and an extraction agent shown as a formula I; the aqueous phase comprises rare earth ions; the pH value in the aqueous phase is 2.5-4.5; M is hydrogen, alkali metal ions or positive ammonium ions. The extraction method disclosed in the invention comprises the following steps: oscillating and balancing the extraction system. The reextraction method disclosed in the invention comprises the following steps: (1) saponifying the organic phase of the extraction system, mixing with the aqueous phase containing the rare earth ions, and obtaining an organic phase loaded with the rare earth ions; and (2) mixing the organic phase loaded with the rare earth ions with an aqueous solution of acid. According to the extraction system, the rare earth ions can be efficiently separated under low acidity, the extraction system is high in saturation capacity and difficult in emulsification, realizes reextraction of the rare earth ions under low acidity and is suitable for actual production.

The invention relates to a sucralose wastewater advanced treatment and desalination method. The method is characterized by comprising the following steps of: (1) adding ammonia water into wastewater to adjust the pH value to 6-7; (2) adding 10% of a composite settling agent, controlling the volume ratio of the settling agent to the wastewater at 1:18-23, and performing depositing for 1.5-2.5h to obtain a supernatant; (3) carrying out wet oxidation treatment on the wastewater at a temperature of 200DEG C-250DEG C under a pressure of 2.0-3.0Mpa, and remaining the state for 4-5h; (4) feeding thewastewater into MVR for evaporation and concentration, wherein the concentration ratio is 70-75%; (5) pumping a mother liquor into an evaporation kettle, performing evaporating and concentrating to obtain mother liquor, adding butanol or octanol, controlling the volume ratio of the mother liquor to the butanol or octanol at 1:1-4, and carrying out aerobic biochemical treatment on the supernatant;(6) cooling and crystallizing the mother liquor, and performing filtering to obtain a salt and alcohol; and (7) rectifying the alcohol to obtain a pure product. The method has the advantages that theuse amount of acid and alkali is greatly reduced; a relatively pure ammonium chloride salt is obtained; the mother liquor amount after alcohol extraction is reduced by 40 times compared with that of raw water, and the environmental protection pressure is greatly reduced.

The invention discloses a method for preparing gallic acid with tara powder. The method comprises the following steps that the tara powder is extracted with water, and water extract is collected; water extract concentration is conducted; concentrated solution hydrolysis is conducted; gallic acid is refined. According to the method, by changing the original technology, the acid and alkali dosage islowered, and meanwhile tara powder residues discarded before can be used for preparing organic fertilizer, and the comprehensive utilization efficiency of resources is improved.

The invention discloses application of graded lignin in preparation of phenolic foam thermal-insulation materials. Compared with the prior art, the phenolic foam thermal-insulation materials are prepared by directly blending the graded lignin with foamable phenolic resin through control of the molecular weight of the graded lignin, so that tedious modification steps in a process for preparing phenolic resin from lignin are avoided, using amount of acids and alkalis is saved, and energy consumption in a modification process is reduced, and at the same time, the lignin content in the final phenolic foam thermal-insulation material products can be greatly improved, and the products are economical and more environmentally friendly. The phenolic foam thermal-insulation materials filled with thegraded lignin have better mechanical properties, thermal stability, anti-ultraviolet aging properties and better fineness, and the product quality meets national standards, and can meet a market demand.

The invention belongs to the field of food processing and in particular relates to a pH regulation method in a high fructose corn syrup production process. The pH regulation method in the high fructose corn syrup production process is characterized by comprising the following steps: conveying a material of which the pH value is to be adjusted to a pH regulation front tank, pumping the material into an ion exchange column I and an ion exchange column II which are connected in parallel, and allowing the material to be subjected to ion exchange in the two ion exchange columns, wherein sampling valves are respectively arranged on the lower parts of the two ion exchange columns, and a pH value is monitored through the valves; continuously conveying the material of which the pH value is adjusted to a required pH value to a regulation rear tank after the material reaches the pH value required to be adjusted through a regulation column, sampling and detecting through the sampling valves at fixed time intervals, and determining that the regulation column is ineffective after the pH value is unqualified; converting the material to a standby ion exchange column for continuous feeding.

The invention discloses a titanium dioxide aluminum coating technology with the cost advantage. The technology comprises the following steps: 1) adjusting the pH value of a titanium dioxide slurry to8-11 by using a metaaluminate solution; 2) adding the metaaluminate solution and an acidic aluminum salt solution to the titanium dioxide slurry in a cocurrent flow manner to control the pH value of the slurry to 8-11; 3) adding an acid solution and a metaaluminate solution to the slurry obtained in the step 2) in a cocurrent flow manner to control the pH value of the slurry to 8-11; and 4) adjusting the pH value of the slurry obtained in step 3) to 6-8 by using the acid solution. The aluminum coating technology of titanium dioxide is improved, the use amount of acids and alkalis for adjustingthe pH value is reduced, the cost is saved, and obtained coated titanium dioxide still can keep excellent glossiness and product compactness.