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52results about How to "Increase the amount of introduction" patented technology

Preparation method of quaternary ammonium type positive ion polyurethane base polyether block hydrophilic silicone softener ultra-micro emulsion and product thereof

ActiveCN103497307AImprove soft feelGood application performanceGrip property fibresVegetal fibresPrepolymerIon
The invention relates to a preparation method of quaternary ammonium type positive ion polyurethane base polyether block hydrophilic silicone softener ultra-micro emulsion and a product thereof. The preparation method comprises the steps that raw materials comprising polymerization monomers, a modifier, an adjuvant and distilled water are prepared; dehydration pre-treatment is conducted on polyether ether glycol; the pre-polymerized reaction is conducted on the dehydrated polyether ether glycol, an end hydroxyl polysiloxane linear body and diisocyanate under the catalyst function of a polymerization catalyst, and a prepolymer is prepared; the chain extension reaction is conducted on the prepolymer, a tertiary amine chain extender agent and an aminosilane coupling agent and an intermediate is prepared; a polymerization stropping agent is added and the reaction is stopped, and a quaternization reagent is added for conducting a quanternization reaction; a product is prepared through emulsification. The preparation method of quaternary ammonium type positive ion polyurethane base polyether block hydrophilic silicone softener ultra-micro emulsion can give unique soft waxy style for various fabric weaving products, is used for improving the soft feel of various kinds of fabric products, does not affect the hydrophilia of natural fiber fabrics, and has good application performance and wide application prospects.
Owner:中山市天信助剂实业有限公司

Method for preparing silicone acrylic emulsion with high solid content and high silicon content

The invention relates to a method for preparing a silicone acrylic emulsion with high solid content (of over 50 percent), high organic silicon content (of over 15 percent) and low emulsifier consumption (of less than 2.5 percent), in particular a silicone acrylic emulsion for preparing high-grade exterior wall coating materials. The method comprises steps of preparing a vinyl polysiloxane emulsion by using octamethylcyclotetrasiloxane, tetravinyl tetramethylcyelo tetrasiloxane, dodecylbenzene sulfonic acid, sodium dodecyl benzene sulfonate, a non-ionic emulsifier NP-40 and deionized water through acid catalyzed ring opening, and performing silicone acrylic emulsion copolymerization of the vinyl polysiloxane emulsion and acrylic monomers in the presence of a thermal initiator to prepare the stable silicone acrylic emulsion with high solid content, high organic silicon content and low emulsifier consumption. By the method, problems that the silicon content cannot be improved substantially, the solid content is low and the emulsifier consumption is high in the preparation of the silicone acrylic emulsion are effectively solved. The silicone acrylic emulsion has excellent weather resistance, stain resistance, water resistance and the like, and has high cost performance; and the application range of the silicone acrylic emulsion is greatly widened.
Owner:武汉强力荷新材料有限公司

Steel fiber reinforced internal curing high-strength silicate ceramsite and preparation method thereof

The invention discloses steel fiber reinforced internal curing high-strength silicate ceramsite and a preparation method thereof. Raw materials of the ceramsite are composed of dried material powder and steel fibers, wherein the doping amount of the steel fibers accounts for 0.5-3.0% of the volume of the dried material powder; the dried material powder comprises the following components in percentage by mass: 12-40% of fly ash, 25-28% of quick lime, 20-50% of diatomite and 10-15% of yellow sand. The preparation method comprises the following steps: performing wet balling, naturally curing, andperforming hydrothermal synthesis, thereby obtaining the steel fiber reinforced internal curing high-strength silicate ceramsite. The prepared ceramsite has cylinder compressive strength of 12-28MPa,a water absorption rate of 15-30% within an hour and obviously improved elasticity modulus, and can be used for preparing light concrete of an LC45-80 structure. The steel fiber reinforced internal curing high-strength silicate ceramsite disclosed by the invention has the advantages of simplifying the process and saving the equipment, energy and raw materials, the internal curing effect of lightweight aggregate on concrete can be effectively improved, and the problems that the conventional lightweight aggregate is low in cylinder compressive strength and high-grade lightweight aggregate concrete is difficultly prepared are well solved.
Owner:NANJING UNIV OF SCI & TECH

Preparation method of high-thermal-conductivity CNTs directed modification ceramic-based composite material

The invention relates to a preparation method of a high-thermal-conductivity CNTs directed modification ceramic-based composite material. A prefab is subjected to interface layer and matrix preparation in a high-temperature furnace so that the relative density of the prefab can reach 30%-70%; ultra-short pulse lasers are adopted to prepare ceramic-based composite material thickness-direction directed holes; ultrasonic dispersion is adopted to prepare a CNTs solution, and in combination with a vacuum soaking method, filling and sealing are conducted to form CNTs directed columns; a CVI method is adopted to further compact the prefab, and the high-thermal-conductivity CNTs directed modification ceramic-based composite material is finally obtained. The technology has the advantages that through the high-thermal-conductivity CNTs directed columns, the heat conductivity of the composite material in the thickness direction is greatly improved; a CNTs interlayer dispersion structure and the CNTs directed columns form a strong heat conduction network, and the overall heat conductivity of the composite material is improved; the directed holes have designability, the size, interval and distribution of the directed holes can be designed according to engineering requirements, and operation is simple.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Preparation method of nuclear shell structure high-silicon silicone acrylic emulsion used for building exterior wall

The invention discloses a preparation method of nuclear shell structure high-silicon silicone acrylic emulsion used for building exterior walls. Firstly, the invention uses octavinyl cyclotetrasiloxane, octamethylcyclotetra siloxane, dodecylbenzene sulfonic acid, sodium dodecyl benzene sulfonate, emulsifier 0P-10 and deionized water to prepare unsaturated organo-siloxane low polymer emulsion; theorgano-siloxane low polymer emulsion, acrylate monomer mixture, initiator A, emulsifier, pH value regulator, molecular weight regulator and deionized water are adopted to polymerize nuclear emulsion;and finally, silicon acrylic nuclear emulsion, deionized water, anion / non-ion emulsifier, acrylate monomer mixture, VTES coupling agent and initiator B are adopted to polymerize nuclear emulsion to prepare high-silicon silicone acrylic emulsion. The method of the invention effectively inhibits organosilicon self-polymerization, so that the silicone acrylic emulsion of the invention has high silicon content and stable storage, has the properties of favorable weather resistance, smudge resistance, water resistance and the like, has high gloss and beautiful degree and can satisfy the requirements of high-grade buildings on exterior wall paint.
Owner:TIANJIN URBAN CONSTR COLLEGE

Remediation method of saline-alkali land soil

The invention discloses a remediation method of saline-alkali land soil. The remediation method specifically comprises the following steps of 1, selecting a certain day of the first ten days of May with sunny and rainless weather, laying a degradable waterproof thin film on the bottom after the soil is deeply dug, then laying a layer of a super-water-absorption sponge on the thin film, and then conducting backfilling of a little soil; 3, after the backfill soil is leveled, laying a layer of a salinity anion adsorption thin film on the surface of the soil, then continuing to conduct backfillingof a little soil, then laying a layer of a salinity anion adsorption thin film, then continuing to conduct backfilling of a little soil, laying a layer of a super-water-absorption sponge, and repeating the step until soil backfilling is finished; 3, after soil backfilling is completely finished, conducting exposure on the soil in the sun for 40-60 days, then ploughing the soil under to great depth, and taking away the salinity anion adsorption thin film in the soil and soil of 1-2 cm in thickness on the surface of the thin film to complete soil remediation. By means of the remediation method,by adsorbing and removing salinity cations contained in the soil, the salinity content in the soil is reduced accordingly, and the purpose of improving soil quality is improved.
Owner:孙天民

Preparation method of novel amino silicone oil modified acrylate anti-doodling emulsion

The invention discloses a preparation method of a novel amino silicone oil modified acrylate anti-doodling emulsion, which comprises the following steps: reacting an epoxy group with an amino group, adding glycidyl methacrylate during emulsion polymerization, introducing the epoxy group to the molecular chain of the emulsion, and reacting with amino-terminated silicone oil to prepare the novel amino silicone oil modified acrylate anti-doodling emulsion. According to the novel amino silicone oil modified acrylate anti-doodling emulsion disclosed by the invention, silicone oil is introduced through a cross-linking reaction, so that the problems that an organic silicon monomer is difficult to polymerize, silane active groups are easy to generate self-crosslinking, the introduction amount of organic silicon is relatively low, volatile organic compounds are polluted and the like caused by a conventional process are solved. The emulsion prepared by the invention not only has the characteristics of extremely strong adhesive force, better ethanol resistance, scrubbing resistance, mechanical shearing resistance and the like, but also has excellent high temperature resistance, weather resistance and chemical resistance, and can be widely applied to the fields of coatings, printing ink, adhesives and the like.
Owner:ANHUI XOANONS CHEM +1

Air volume multiplier fresh air duct suitable for integrated air-conditioning window

The invention provides an air volume multiplier fresh air duct suitable for an integrated air-conditioning window. The air volume multiplier fresh air duct suitable for the integrated air-conditioningwindow comprises an air suction opening, a motor, a turbofan, an air guiding cavity and an air duct. Coarse, medium and high efficiency air filter screens are arranged on the air suction opening in sequence to be connected with the external environment. The air guiding cavity is a long-strip-shaped wing type cavity, the inside of the air guiding cavity and outside of the air guiding cavity are smooth walls, and the tip of the air guiding cavity is in a thin-seam-opening shape. Sound absorbing materials are evenly arranged in the air guiding cavity and the air duct. According to the air volumemultiplier fresh air duct suitable for the integrated air-conditioning window, fresh air volume introduced by the integrated air conditioning window is greatly increased by the coanda effect, the effect of air multiplier is achieved, the indoor air exchange efficiency is effectively improved, the requirement of indoor fresh air volume is reached, and at the same time the fresh air can be subjected to purification and noise reduction treatment. The air volume multiplier fresh air duct suitable for the integrated air-conditioning window provides a new solving way to solve the problem of difficultly introducing the fresh air into a general residence, the performance of the air-conditioning is improved, and the improvement of indoor air quality is facilitated.
Owner:SICHUAN UNIV

Mullite fiber reinforced metal-based composite ceramic sheet and preparation method thereof

The invention provides a mullite fiber reinforced metal matrix composite ceramic sheet and a preparation method thereof.The preparation method comprises the steps that calcined aluminum oxide, magnesian soil, nanoscale fused quartz, monazite, bentonite, pyrophyllite, black talc, potassium albite, aluminum powder and sodium tripolyphosphate are mixed and then subjected to ball milling treatment, and mixed powder is obtained; performing pulping and spray granulation to obtain green body powder; the preparation method comprises the following steps: preparing a ceramic thin plate blank, pressing the blank powder into a ceramic plate-shaped blank, sintering the ceramic plate-shaped blank to obtain a ceramic thin plate blank, glazing the ceramic thin plate blank, grinding the surface, and polishing to obtain the mullite fiber reinforced metal-based composite ceramic thin plate. The invention has the advantages of simple preparation process and low raw material cost, and can be applied to the commercial fields of architectural decoration ceramics, protective materials and the like. By optimizing the solid-phase reaction sintering schedule and regulating and controlling the internal mullite crystal phase precipitation rate and precipitation amount, the prepared large-size ceramic sheet is excellent in mechanical property and wide in potential commercial market.
Owner:SHAANXI UNIV OF SCI & TECH
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