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58results about How to "Many sites" patented technology

Preparation method and application of metal-organic framework compound electrocatalyst

The invention discloses a preparation method and an application of a metal-organic framework compound electrocatalyst. The preparation method comprises the following steps: respectively dissolving tartaric acid, FeCl3. 6H2O and Ni(NO3)2. 6H2O in methanol; mixing above two obtained solutions, and transferring the obtained mixture into a reaction kettle; vertically putting foamed nickel into the reaction kettle, heating the reaction kettle to react, and naturally cooling the reaction kettle; and taking out the foamed nickel, washing the foamed nickel with ethanol, and carrying out vacuum drying.In a three-electrode system, the metal-organic framework compound electrocatalyst is directly placed in an electrolyte as a working electrode to carry out an electrocatalytic water decomposition oxygen evolution reaction. The three-position nanoflower-tartaric acid-iron and nickel bimetal-organic framework compound is formed through one-step wet chemical self-assembling by using the strong coordination capability of tartaric acid and taking the foamed nickel as a substrate, and the has ean xcellent electrocatalytic oxygen evolution activity and a very excellent cycling stability under a highcurrent density.
Owner:SHANGHAI UNIVERSITY OF ELECTRIC POWER

Composite bactericide for controlling fruit and vegetable oomycetes diseases

The invention relates to pesticides, in particular to composite bactericide for controlling fruit and vegetable oomycetes diseases. The composite bactericide consists of active elements, fillers and/or auxiliary agents, which is characterized in that the active elements consist of carboxylic acid amide bactericides and metiram, the weight ratio of the carboxylic acid amide bactericides to the metiram is (1-10):(10-100). The product form of the composite bactericide for controlling the fruit and vegetable oomycetes disease can be wettable powder or water dispersible granules. The composite bactericide for controlling the fruit and vegetable oomycetes diseases is suitable for controlling various oomycetes diseases of the fruits and vegetables, in particular controlling the potato late blight, the cucumber downy mildew, the grape downy mildew, the tomato late blight, the capsicum blight and the Chinese cabbage downy mildew; the composite bactericide has remarkable synergism and more action mechanisms and sites, and can effectively delay the generation and spread of oomycetes pesticide resistance; in addition, the invention has the advantages of wide disease controlling spectrum, high biologic safety, simple preparation method, low cost and remarkable economic benefit.
Owner:INST OF PLANT PROTECTION HEBEI ACAD OF AGRI & FORESTRY SCI

Preparation method and application of boron nitride loaded Ni-MoOx nano catalyst

The invention discloses a preparation method and application of a boron nitride loaded Ni-MoOx nano catalyst. The preparation method comprises the following steps: preparing an aqueous solution of hexagonal boron nitride BN, and ultrasonically treating to obtain a uniformly dispersed hexagonal boron nitride BN aqueous solution; adding a NiCl2 aqueous solution into the BN aqueous solution in step I, and continuously stirring to obtain a mixed solution A; adding a Na2MoO4 aqueous solution into the mixed solution A, and continuously stirring to obtain a mixed solution B; adding 20-60 mg of sodiumborohydride NaBH4 into the mixed solution B, stirring for 5-15 minutes to perform reduction reaction, thereby obtaining the boron nitride loaded Ni-MoOx nano catalyst. The preparation method adopts aone-step quick reduction method to synthesize the boron nitride loaded Ni-MoOx nano catalyst, can be completed at room temperature and has the advantages of being short in synthetic time, simple andconvenience in operation and the like; the synthesized Ni-MoOx/BN catalyst can be used for catalyzing decomposition of hydrazine borane water solution 323K to produce hydrogen and the catalyst still has a 100% conversion rate in case of not adding any additive, 100% hydrogen gas selectivity, relatively good circulating stability and extremely high catalytic activity.
Owner:JILIN UNIV

A kind of graphite phase nitrogen carbide nanosheet/cobalt trioxide nanosheet fish scale structure composite nanomaterial and its preparation method and application

The invention aims at providing a method for synthesizing a scale-shaped graphite-phase nitrogen carbide nanosheet / cobaltosic oxide nanosheet composite material and belongs to the technical field of material preparation and catalysis. The composite material is prepared from the raw materials of functionalized graphite-phase nitrogen carbide and cobalt salt through a hydrothermal method at high temperature. The prepared scale-shaped two-dimensional nitrogen carbide nanosheet / cobaltosic oxide nanosheet composite material is in morphology that a scale-shaped cobaltosic oxide nanosheet nanocomposite material evenly grows on the surface of a two-dimensional nitrogen carbide nanosheet. Compared with a traditional pure two-dimensional nitrogen carbide nanomaterial, the specific surface area of the material and the screening capacity of the material to a catalytic substrate are effectively improved, and the material has more efficient photocatalytic performance. The preparation method has the advantages of simple technology, low cost and high catalytic efficiency; the prepared material has efficient carbon dioxide reducing capacity, and thus has good application prospect in the photocatalysis field of environmental modification, greenhouse gas elimination and the like.
Owner:FUJIAN MEDICAL UNIV

Preparation method of modified nano cellulose bentonite composite material for treatment of printing and dyeing wastewater

The invention discloses a preparation method of modified nano cellulose bentonite composite material for treatment of printing and dyeing wastewater. The preparation method comprises the steps of: firstly extracting cellulose of sunflower seed hull by using an acid-extraction alkali-extraction process, and modifying bentonite by using polyacrylamide, so as to enable a part of polyacrylamide intercalated structure to be embedded into sheet layers of bentonite, and further to provide more sites and surface pores, improve the adsorption performance and later progress of a grafting reaction. According to the invention, cellulose is dispersed in urea, then modification of ammonium persulfate and polyacrylamide-modified bentonite is carried out, thus reaction of cellulose chains is initiated bythe ammonium persulfate, hydroxyl on the cellulose chains after reaction initiation is grafted to polyacrylamide, and after grafting polymerization for a certain period of time, amide groups are successfully introduced, so that the composite material with dual effects of adsorption and flocculation is obtained. For treatment of printing and dyeing wastewater, the composite material still maintainsexcellent flocculation performance while has improved decoloring performance, has excellent effect on actual comprehensive treatment of printing and dyeing wastewater, and is worthy of promotion.
Owner:WUHU PENGLEI NEW MATERIAL

c-KIT somatic mutation gene detecting kit and detecting method thereof

The invention relates to a c-KIT somatic mutation gene detecting kit and a detecting method thereof. The kit comprises primers and probes for detecting c-KIT somatic cell gene mutation. The primers and the probes are specifically the primer and the probe for detecting a No. 11 exon of a c-KIT gene, wherein a primer sequence is as shown in SEQ ID NO: 1-6, and a probe sequence is as shown in SEQ IDNO: 7-8; the primer and the probe are used for detecting a No. 9 exon of the c-KIT gene, wherein the primer sequence is as shown in SEQ ID NO: 9-10, and the probe sequence is as shown in SEQ ID NO: 11; the primer and the probe are used for detecting a No. 13 exon of the c-KIT gene, wherein the primer sequence is as shown in SEQ ID NO: 12-14, and the probe sequence is as shown in SEQ ID NO: 15; andthe primer and the probe are used for detecting a No. 17 exon of the c-KIT gene, wherein the primer sequence is as shown in SEQ ID NO: 16-19, and the probe sequence is as shown in SEQ ID NO: 20. Thedetecting kit and the detecting method are far more than similar products in detecting site number, complete in site, high in detecting sensitivity, strong in specificity, high in accuracy, low in cost, and capable of meeting clinical GIST targeted administration c-KIT mutation detection.
Owner:PRIMBIO GENES BIOTECH WUHAN CO LTD

Aqueous zinc-bromine battery

The invention discloses an aqueous zinc-bromine battery, and the battery comprises a positive electrode, wherein the positive electrode is a carbon, metal or nonmetal matrix material modified by a carbon material with a high specific surface area and is used for carrying out an oxidation-reduction reaction of zero-valent bromine and negative monovalent bromine, and the electrode can provide more sites for an active substance, so the improvement of the reversibility of electrode reaction is facilitated, and high loading capacity can be realized; a negative electrode which adopts a metal material capable of being alloyed with zinc or a zinc-loving carbon material and is used for carrying out redox reaction of positive divalent zinc and zero-valent zinc, wherein the electrode material can reduce a nucleation energy barrier of zinc and homogenize a surface electric field, so the reversibility of the reaction is improved and formation of zinc dendrites is avoided; an aqueous electrolyte which is an aqueous solution containing a zinc salt, a bromine salt, a complexing agent and a zinc dendritic crystal inhibitor, wherein the complexing agent and the bromine elementary substance are combined at the positive electrode and exist in a solid form, so that pollution to the negative electrode can be avoided, the battery stability is improved, and the zinc dendritic crystal inhibitor can avoid formation of zinc dendritic crystals of the negative electrode, so the cycle stability of the battery is improved.
Owner:UNIV OF SCI & TECH OF CHINA
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