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42results about How to "Not easy to crust" patented technology

High-covering-power styrene-acrylate emulsion, synthesis method thereof and use thereof in aqueous printing ink

The invention relates to the field of printing ink and discloses high-covering-power styrene-acrylate emulsion, a synthesis method thereof and use thereof in aqueous printing ink. The preparation method comprises: mixing deionized water, an initiator, a lacquer and a composite emulsifier to obtain solution A; regulating the pH value; introducing nitrogen to remove oxygen; mixing a monomer with a molecular weight regulator to obtain solution B; dripping solution B into solution A to perform a chemical reaction; regulating the pH value of shell emulsion and heating to prepare shell emulsion; adding a composite emulsifier and an initiator into the synthesized shell emulsion; dripping a vinyl monomer to synthesize core-shell emulsion; and cooling, regulating the pH value and filtering to obtain the styrene-acrylate emulsion. The invention also provides aqueous printing ink using the high-covering-power styrene-acrylate emulsion. The preparation process is very simple, the reaction processis simple and easy to control, the operability is high, and the method is suitable for large-scale production. The aqueous printing ink disclosed by the invention is high in resolubility, is insusceptible to crusting and blocking printing plate and has high printing adaptability.
Owner:广东天龙油墨有限公司

Preparation method for pelletizing and producing yellow phosphorus by phosphorus ore concentrate

The invention provides a preparation method for pelletizing and producing yellow phosphorus by a phosphorus ore concentrate which comprises the following components in terms of producing 1000 Kg of yellow phosphorus: 7100-8500 Kg of phosphorus ore concentrate powder, 1800-2000 Kg of coke dust, 1800-3300 Kg of silica powder, 130 Kg of humic acid and 65 Kg of sodium hydroxide. The preparation method is as follows: grinding formula components by a ball mill; adding a binder composed of the humic acid and the sodium hydroxide, and evenly stirring; processing into a compound pellet by a ball pressing and forming machine; dying by a chain plate dryer; and sending into a yellow phosphorus electric furnace to prepare into a yellow phosphorus finished product. The invention fully utilizes powder phosphate ores and low-grade phosphate ores; the phosphorus ore concentrate powder obtained by mineral separation is produced into a pellet by the binder, and then the pellet is prepared into yellow phosphorus by the electric furnace. Compared with the existing phosphorus preparation by a phosphorus ore concentrate, the invention lowers cost by one time, reduces CO emission by about 35%, reduces electricity consumption by about 40%, improves capacity by 2 times and reduces materials by about 40%. Thus, the invention is an excellent method for solving the problems of high energy consumption, high emission and high pollution for yellow phosphorus production in China.
Owner:瓮安烨烨磷化工实业有限公司

Starting method of magnesium electrolytic cell

The invention relates to a starting method of a magnesium electrolytic cell. Specifically, the bottom of an electrolysis chamber (1) in a multipolar magnesium electrolytic cell and the central section of a magnesium collection chamber (2) are respectively provided with a set of AC (alternating current) electrodes (4), and the two sets of electrodes are separately controlled. When the electrolytic cell is started, electrolyte prepared in advance is added to submerge the AC electrodes (4) located at the bottom of the electrolysis chamber (1), so that alternating current of the electrodes is to be delivered. The electrolyte is added continuously until reaching a position of 50mm-60mm below a cathode (3) bottom, and is heated to a temperature of 680-700DEG C and maintained at a constant temperature for more than 4 hours. Then, the electrolyte is added to a standard liquid level (5), and when the AC electrodes (4) located at the central section of a magnesium collection chamber (2) are submerged by the electrolyte, alternating current of the electrodes is delivered. After the electrolyte is heated to a temperature of 700DEG C and maintained at a constant temperature for 48 hours, direct current is sent to start the electrolytic cell. For an electrolytic cell started with the method of the invention, the bottom of the electrolytic cell is free of incrustation, and the generated magnesium can gather well. Distribution of cathode current is uniform and distribution of anode current is also measured to be uniform. Thus, the adoption of the method provided in the invention can have a good effect.
Owner:遵宝钛业有限公司

CVI process method for batch quick preparation of carbon/carbon composite crucible enclosure

The invention discloses a CVI process method for batch quick preparation of a carbon / carbon composite crucible enclosure. By sleeving of crucible enclosure prefabs in different sizes, gas flowing arealimiting is realized; by reasonable setting of a fluid flowing route, the gas flows in a limited narrow area, and detention time of the gas in narrow slits is controlled. Narrow slit flowing has theadvantage that in a pyrolytic carbon deposition process, the prefab surface is less prone to crusting, and accordingly crucible enclosure prefabs can be deposited in high density in one time. When hydrocarbon gas flows through a first crucible enclosure prefab layer from top to bottom, splitting and pyrolytic carbon deposition reaction occurs in a high-temperature environment; when the gas reachesa second crucible enclosure prefab layer, precursors in a gas source are partially consumed, and the consumed precursors are offset by means of gas replenishing. By combination of sleeving and gas replenishing, efficiency in preparation of the carbon / carbon composite crucible enclosure can be greatly improved.
Owner:上海康碳复合材料科技有限公司 +1

Defoaming agent for paint and ink and preparation method thereof

The invention discloses a defoaming agent for paint and ink and a preparation method of the defoaming agent. The defoaming agent for the paint and the ink is prepared from the following raw materialsin parts by mass: 42-48 parts of silicone oil, 14 -20 parts of hydrophobic silicon dioxide, 14-18 parts of silicon paste, 10-20 parts of higher alcohol, 1-3 parts of glycerin fatty acid ester, 3-5 parts of sodium hexametaphosphate, 1-2 parts of sodium secondary alkyl sulfonate, 4-10 parts of magnesium hydroxide, 5-11 parts of dimer linoleic acid, 5-7 parts of white carbon black, 4-8 parts of whitemineral oil, 8-14 parts of a surfactant, 20-30 parts of polyethylene wax, 10-12 parts of lecithin, 7-18 parts of a thickener, 4-14 parts of a co-emulsifier, 16-20 parts of distearoyl diethylamine and90-110 parts of deionized water. The defoaming agent of the invention has the beneficial effects of good dispersibility, strong affinity, strong foam inhibition capability, fast foam inhibition speed, lasting action time, capacity of realizing difficult generation of fine pinhole foams in the paint, strong high temperature resistance and stability and good compatibility with the paint and enablesthe surface of the paint to not prone to skinning and to have gloss, and a mixed solution of the defoaming agent with the paint has no layering phenomenon .
Owner:安徽銮威化工科技开发有限公司

High-covering-power styrene-acrylate emulsion, synthesis method thereof and use thereof in aqueous printing ink

The invention relates to the field of printing ink and discloses high-covering-power styrene-acrylate emulsion, a synthesis method thereof and use thereof in aqueous printing ink. The preparation method comprises: mixing deionized water, an initiator, a lacquer and a composite emulsifier to obtain solution A; regulating the pH value; introducing nitrogen to remove oxygen; mixing a monomer with a molecular weight regulator to obtain solution B; dripping solution B into solution A to perform a chemical reaction; regulating the pH value of shell emulsion and heating to prepare shell emulsion; adding a composite emulsifier and an initiator into the synthesized shell emulsion; dripping a vinyl monomer to synthesize core-shell emulsion; and cooling, regulating the pH value and filtering to obtain the styrene-acrylate emulsion. The invention also provides aqueous printing ink using the high-covering-power styrene-acrylate emulsion. The preparation process is very simple, the reaction processis simple and easy to control, the operability is high, and the method is suitable for large-scale production. The aqueous printing ink disclosed by the invention is high in resolubility, is insusceptible to crusting and blocking printing plate and has high printing adaptability.
Owner:广东天龙油墨有限公司

High-solid low-viscosity large-particle-size polyvinyl acetate emulsion and preparation method thereof

The invention discloses a high-solid low-viscosity large-particle-size polyvinyl acetate emulsion and a preparation method thereof, and the emulsion is applied to the technical field of adhesive compounding. The emulsion comprises, in parts by weight, vinyl acetate, vinyl versatate, methacrylic acid, a crosslinking monomer hydroxyethyl methylacrylate (HEMA), deionized water, an emulsifier, polyvinyl alcohol, ammonium persulfate as an initiator, a reducing agent as an initiator, a plasticizer, urea, a defoaming agent and a preservative. According to the invention, a core-shell copolymerization process is adopted, and polymerization is carried out in a manner of early-stage high-bottoming monomers and staged gradual acceleration of rotation speed, so that the emulsion is narrower in particle size distribution, larger in average particle size and lower in viscosity in a later stage; and the defects of small particle size, high viscosity, low compression shear strength, poor freeze-thaw stability, easy surface skinning, aldehyde existence and the like of a traditional high-solid-content polyvinyl acetate emulsion are overcome, and the polyvinyl acetate emulsion has good glue performance and storage stability.
Owner:顶立新材料科技股份有限公司 +1

High-efficiency zinc alloy sacrificial anode for high-temperature crude oil deposition water environment

InactiveCN110106509AIncrease working potentialLower grain boundary potentialSeawaterWater environment
The invention provides a high-efficiency zinc alloy sacrificial anode suitable for a high-temperature crude oil deposition water environment. The high-efficiency zinc alloy sacrificial anode is prepared from the compositions in percentage by weight: 0.10-0.25% of Al, 0.05-0.15% of Mg, 0.005-0.009% of Sn, the impurity content including less than or equal to 0.006% of Pb, less than or equal to 0.001% of Cd, less than or equal to 0.001% of Cu, less than or equal to 0.002% of Fe, and the balance of Zn. The high-efficiency zinc alloy sacrificial anode is processed and manufactured through conventional fusion casting, zinc ingots are held through a dedicated graphite crucible, and melted in a heating furnace, Al and an Al-Mg alloy are added into a molten zinc solution in proportion, the productis stirred through a graphite rod, slag is removed, and the product is casted after being removed from the furnace; and the heating furnace selects a coke-fired furnace, an electric furnace, an oil furnace, a gas furnace and the like. According to the high-efficiency zinc alloy sacrificial anode for the high-temperature crude oil deposition water environment, compared with the prior art, the preparation technology and method are mature, operation is easy and convenient, the proportion is reasonable, the service life is long, the protective effect is good, and the high-efficiency zinc alloy sacrificial anode can be widely applied to cathode protection under the high temperature conditions in the fields of seawater and offshore oil.
Owner:SUNRUI MARINE ENVIRONMENT ENG

Method for preparing metal beryllium by electrolyzing beryllium oxide through fluoride molten salt

The invention discloses a method for preparing metal beryllium by electrolyzing beryllium oxide through fluoride molten salt, which comprises the following steps: (1) constructing a BeF2-MFn molten salt system, where MFn is one or more of alkali metal fluoride or alkaline earth metal fluoride except beryllium fluoride; (2) adding beryllium oxide into a BeF2-MFn molten salt system in a molten state; and (3) electrolysis is conducted, and solid-state metal beryllium is separated out on the cathode. According to the method, beryllium smelting intermediate product beryllium oxide is adopted as a raw material and dissolved in fused salt, beryllium ions and oxygen ions are dissociated, due to positive and negative phase attraction, the oxygen ions with negative electricity move to an anode and lose electrons, oxygen or carbon-containing gas is obtained, the beryllium ions with positive electricity move to a cathode, and the electrons are reduced into beryllium atoms to be deposited on the surface of the cathode; according to the method, the technological process is greatly shortened, and the direct recovery rate of beryllium is increased; and beryllium oxide is used as a raw material, carbon dioxide and oxygen are generated on the anode, and the method is more environment-friendly.
Owner:ZHENGZHOU UNIV

Feeding device of biogas pool

The invention relates to a feeding device of a biogas pool. The feeding device comprises a feeding box, a discharge valve, a driving unit, a stirring mechanism, a pressure sensor and a controller. A top cover is arranged at the top of the feeding box, a discharging hole is arranged in the bottom of the feeding box and is communicated with a discharging pipe, and a discharging pipe is arranged in the discharge pipe; the driving unit is mounted on the top cover, the stirring mechanism is located in the feeding box and comprises a stirring shaft and two stirring pieces, the stirring shaft is connected with the outlet shaft of the driving unit, the stirring pieces are respectively arranged on two sides of the stirring shaft, and a plurality of stabs used for crushing are arranged on outer walls of the stirring pieces; the pressure sensor is arranged in the biogas pool and is connected with the input end of the controller, the controller is mounted on the top cover with the output end being in communication connected with the discharging valve and capable of controlling opening of the discharging valve. By the arrangement, materials in the biogas pool are less prone to crusting, the materials can be automatically fed into the biogas pool according to biogas yield in the biogas pool, and the materials are favorably sufficiently utilized.
Owner:NANAN CITY GREEN BIOGAS TECH DEV & RES INST

Ultra-thin evenly mixed straw biogas material distribution mode

The invention relates to an ultra-thin evenly mixed straw biogas material distribution mode. By adopting the mode, an anaerobe is promoted to be dispersed in all fermentation liquor, biogas fermentation is facilitated, and the gas efficiency is greatly improved in comparison with the traditional mixing mode. The upper layer of the fermentation liquor is not easily crusted, and is easy to vent, and meanwhile, the ultra-thin evenly mixed straw biogas material distribution mode is simple, convenient and fast to discharge. The ultra-thin evenly mixed straw biogas material distribution mode has the characteristics that the cost is saved, and an energy source is saved.
Owner:TIANJIN BEIFANG LANDSCAPE ECOLOGY INST OF SCI & TECH

Dispersion liquid film type absorption tower used for organochlorosilane concentrated acid hydrolysis

The invention relates to a dispersion liquid film type absorption tower used for organochlorosilane concentrated acid hydrolysis. The absorption tower comprises a casing, wherein a liquid distribution plate is fixedly mounted between an upper seal head and an outer barrel body of the absorption tower; a splash-proof screen mesh is arranged on the liquid distribution plate; 3-10 layers of neatly arrayed film forming plates are arranged below the liquid distribution plate and are supported horizontally; an included angle between every film forming plate and the water level ranges from 15 degrees to 75 degrees; and film forming plates are arrayed in a staggered manner between adjacent layers. According to the absorption tower, appropriate reacting pressure (0.1 MPa to 0.5 MPa of gauge pressure) enables HCl gas generated by hydrolysis to have sufficient pressure; the dispersion liquid film type absorption tower enables an organic phase and an aqueous phase to be contacted in a film manner, so that the hydrolysis reaction is sufficient without emulsion; and a phase separator is used to separate hydrolysates and concentrated hydrochloric acid rapidly, the hydrolysates are prevented from polymerizing under the acid catalysis, and the qualities of the hydrolysates are improved.
Owner:QINGDAO UNIV OF SCI & TECH

Movable-cover-free cyclic feeding and discharging type methane-generating pit

The invention discloses a movable-cover-free cyclic feeding and discharging type methane-generating pit. The methane-generating pit is composed of a feeding hole, a feeding pipe, a pit body of the methane-generating pit, a prefabricated top sealing cover, a gas guide pipe, a water pressure chamber and a discharging hole, wherein the feeding pipe is mounted above the bottom of the pit body of the methane-generating pit and the other end of the feeding pipe is upward introduced out to be communicated with the feeding hole; a channel is arranged at the bottom of the pit body of the methane-generating pit and is communicated with the bottom of the water pressure chamber; the discharging hole is formed in the upper end of the water pressure chamber; the prefabricated top sealing cover is mounted at the upper part of the pit body of the methane-generating pit and is in sealed connection with the pit body of the methane-generating pit; the gas guide pipe is mounted on the prefabricated top sealing cover. The methane-generating pit disclosed by the invention is simple in construction, convenient to use, good in sealing performance and long in service life; material liquid is not easily crusted. By combining a sunlight greenhouse, the problem that gas is not generated in winter is solved; the movable-cover-free cyclic feeding and discharging type methane-generating pit has the characteristic that the gas is normally generated in a whole year.
Owner:CHINA AGRI UNIV

Concentrated acid hydrolysis system used for organochlorosilane concentrated acid hydrolysis

The invention relates to a concentrated acid hydrolysis system used for organochlorosilane concentrated acid hydrolysis, which utilizes a dispersion liquid film type absorption tower serving as a core and comprises accessory equipment such as a static mixer, an oil-water phase separator and a falling-film evaporator. The absorption tower comprises a casing, wherein a liquid distribution plate is fixedly mounted between an upper seal head and an outer barrel body of the absorption tower; a splash-proof screen mesh is arranged on the liquid distribution plate; 3-10 layers of neatly arrayed film forming plates are arranged below the liquid distribution plate and are supported horizontally; an included angle between every film forming plate and the water level ranges from 15 degrees to 75 degrees; and film forming plates are arrayed in a staggered manner between adjacent layers. According to the absorption tower, appropriate reacting pressure (0.1 MPa to 0.5 MPa of gauge pressure) enables HCl gas generated by hydrolysis to have sufficient pressure; the dispersion liquid film type absorption tower enables an organic phase and an aqueous phase to be contacted in a film manner, so that the hydrolysis reaction is sufficient without emulsion; and a phase separator is used to separate hydrolysates and concentrated hydrochloric acid rapidly, the hydrolysates are prevented from polymerizing under the acid catalysis, and the qualities of the hydrolysates are improved.
Owner:QINGDAO UNIV OF SCI & TECH
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