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98results about How to "Process parameters are reasonable" patented technology

A kind of preparation method of porous foamed iron-chromium-aluminum alloy material

The invention is a preparation method of porous foamed iron-chromium-aluminum alloy material, which is characterized in that: the steps include: select porous material, soak water-based polymer adhesive at normal temperature; mix chromium powder and high-activity aluminum The powder is evenly sprayed on the surface of the porous material impregnated with the water-based polymer adhesive; drying; the excess chromium powder and aluminum powder are separated from the porous material matrix; the chrome-aluminum porous material is dip-coated with conductive adhesive; Electrodeposition of iron after warm curing treatment; redox treatment; secondary diffusion treatment of chromium and aluminum to obtain porous foamed iron-chromium-aluminum alloy material. Its preparation method is scientific, the selected process parameters are reasonable, the quality is easy to control, the cost is low, and it can be prepared with light weight, large specific surface area, ultra-thickness, thickness is 5-100mm, high porosity 96-99.9%, high temperature resistance and corrosion resistance. Excellent, able to meet the requirements of high temperature resistance, corrosion resistance and other harsh working conditions. It is especially suitable as high-temperature filtration, chemical catalysis, carrier, burner gas distribution and high-temperature flame-retardant materials.
Owner:JILIN ZHUOER TECH

Process for heat treatment of tube body of drill rod

The invention discloses a process for heat treatment of the tube body of a drill rod, which comprises quenching and tempering heat treatment. The process comprises the following steps with the following process parameters: (1) quenching: a, conveying the tube body of the drill rod to a stepping quenching furnace with the temperature rising to be 880-930 DEG C, and keeping the temperature for 40-60 minutes; b, taking the tube body of the drill rod out of the furnace and placing the tube body of the drill rod into quenching solution with the temperature being 10-30 DEG C within 15 seconds, wherein the quenching time is no less than 30 seconds; and (2) tempering: conveying the tube body of the drill rod to a stepping tempering furnace with the temperature rising to be 560-590 DEG C, keeping the temperature for 60-85 minutes, taking the tube body of the drill rod out of the furnace, and naturally cooling the tube body of the drill rod to the room temperature. When the invention is applied, the impact performance of the drill rod is good and is 30 percent above the V150 steel grade standard; the strength, elongation rate and other mechanical indicators of the tube body of the drill rod after heat treatment meet the V150 steel grade requirements, and the qualification rate is higher than 98 percent; and the operating steps and process parameters of the heat treatment of the invention are reasonable.
Owner:CNPC BOHAI EQUIP MFG +1

Preparation method of acrylic ester type processing aid with multilayer gradient core-shell structure

ActiveCN103467663AProcess parameters are reasonableReduce material and process costsEmulsionSolubility
The invention relates to a preparation method of an acrylic ester type processing aid with a multilayer gradient core-shell structure, belonging to the field of modification of functional macromolecular materials. The preparation method comprises the following process steps: (1) under the condition of stirring at 30 DEG C, adding deionized water, an initiator A, an emulsifier, a co-emulsifier, a dispersant, a soft monomer and a crosslinking agent into a reaction kettle, and performing pre-emulsification to obtain a pre-emulsion; (2) heating the pre-emulsion to a temperature less than or equal to 90 DEG C, and performing a thermal reaction to obtain a soft monomer core layer emulsion; and (3) adding an initiator B, alpha olefin and a monomer which has a solubility parameter similar to that of PVC (polyvinyl chloride) into the soft monomer core layer emulsion, and sequentially polymerizing 1-5 layers of rigid polymer shells with a solubility parameter similar to that of polyvinyl chloride to obtain the acrylic ester type processing aid. The obtained PVC processing aid has the advantages of low price, good effect of promoting plasticization, excellent weathering resistance, capability of improving impact properties of a product and the like, and can be widely applied to the fields of PVC building door and window profiles, pipes, wires, cables, small-scale household appliances and the like.
Owner:乌鲁木齐市华泰隆化学助剂有限公司

Water-based stearic acid amide emulsion and preparation method thereof

The invention provides a water-based stearic acid amide emulsion. The water-based stearic acid amide emulsion comprises, by weight, 60-70 parts of deionized water, 30-40 parts of stearic acid amide, 3-7 parts of a wetting dispersant, 1-3 parts of an emulsifier, 0.5-1.5 parts of a crosslinking agent, 1-3 parts of a water-based defoaming agent, 0.6-1 part of a suspending agent and 1-1.4 parts of a bactericide. A preparation method of the water-based stearic acid amide emulsion comprises the steps of adding the deionized water in a dispersion pot; heating and stirring; adding the wetting dispersant, the emulsifier, the crosslinking agent, the bactericide and the suspending agent; dispersing and emulsifying the above materials; adding the water-based defoaming agent; adding stearic acid amide; grinding into particles with the particle size of 0.5-1 micrometer after stearic acid amide is completely emulsified; and discharging and packaging the materials. The method provided by the invention is simple in process, reasonable in process parameters and low in preparation cost, and realizes micro-particulation of stearic acid amide. The solid content of stearic acid amide particles in the emulsion is high. The emulsion is low in viscosity and uniform, has ideal enhancing and lubricating effects, can be stored for a long time without changing quality, does not appear phenomena of flocculation stratification, has no foam during the production, and is ideal in product quality.
Owner:杨福敬

Preparation method of flame-retardant, impact-resistant and high-fluidity chloroethylene-based special resin

The invention relates to a preparation method of flame-retardant, impact-resistant and high-fluidity chloroethylene-based special resin, and belongs to the field of modification of functional polymer materials. The preparation method comprises the following process steps of (1) adding deionized water, an initiator A, an emulsifier, a co-emulsifier, a dispersing agent, a soft monomer and a crosslinking agent into a reaction kettle at 30 DEG C while stirring, pre-emulsifying the resulting solution to obtain a pre-emulsified solution; (2) increasing the temperature of the pre-emulsified solution to be not greater than 90 DEG C, and carrying out reaction while keeping the temperature to obtain a soft monomer kernel emulsion; and (3) adding a chloroethylene-based monomer, styrene, the soft monomer kernel emulsion, an initiator B, the deionized water, and the dispersing agent into the reaction kettle and carrying out reaction while keeping the temperature at 30-70 DEG C to obtain the special resin. Compared with acrylonitrile-butadiene-styrene copolymer (ABS), the chloroethylene-based special resin has the advantages of low price, self flame retardance, high toughness and the like, and can be used for completely replacing ABS and the flame-retardant ABS to be widely applied to the fields of airplanes, cars, ships, household appliances, building materials and the like.
Owner:SUZHOU HONGDING WATER

Boron-free high-performance glass fiber taking pulverized fuel ash and desalted river sand as raw materials, as well as preparation method thereof

The invention discloses a boron-free high-performance glass fiber taking pulverized fuel ash and desalted river sand as raw materials, as well as a preparation method thereof, belonging to the technical field of materials. The boron-free high-performance glass fiber is prepared from the following raw materials in percentage by weight: 30-55% of pulverized fuel ash, 0-15% of blast-furnace slag, 40-50% of desalted river sand, 0-12%of magnesium oxide, and 0-6% of calcium oxide. The high-performance glass fiber can be prepared in a common refractory material liner smelting furnace by pretreating the pulverized fuel ash and adding a less amount of blast furnace slag, magnesium oxide and calcium oxide through taking pulverized fuel ash and desalted river sand as raw materials, the strength and elastic modulus are obviously higher than those of the common E glass and ECR, Advantex boron-free glass and the like, the preparation processes are simple, the smelting temperature is at 1400-1420DEG C, a difference between the fiber forming temperature and liquid phase temperature is more than 70DEG C which is far higher than the lowest standard of the glass fiber industrial production being 50DEG C, the production cost is low, and the glass fiber industrial production standard can be met. The component glass has higher chemical corrosion resistance and high-temperature resistance properties compared with the traditional E glass.
Owner:UNIV OF JINAN

Heat treatment process of welded type weighted drill rod joint

The invention discloses a heat treatment process of a welded type weighted drill rod joint. The heat treatment process comprises the following steps of: sequentially placing workpieces into a box type quenching furnace, vertically placing in a large-space mode, heating the furnace to 860 to 890 DEG C, preserving heat for at least 60 minutes, and stirring quenching oil before discharging the workpieces out of the furnace, wherein the oil temperature is controlled to be 80+/-1 DEG C; taking the workpieces out of the furnace, throwing the workpieces into the quenching oil at once, quenching, and cooling the workpieces in the quenching oil for at least 10 minutes; performing tempering treatment on the workpieces within 3.5 hours after the workpieces are quenched, heating a tempering furnace to 600 to 630 DEG C, preserving heat for at least 120 minutes, taking the workpieces out of the tempering furnace, throwing the workpieces into a water channel at once, and cooling to normal temperature. By adopting the heat treatment process, the quenching quality is improved mainly by taking a series of technology measures of reducing the quenching upper limit temperature, increasing the heat-preserving time and the like, so that the cracking phenomenon is avoided.
Owner:JIANGSU SHUGUANG OIL DRILLING EQUIP CO LTD

Processing method of ready-to-eat tuna slice

The invention provides a processing method of a ready-to-eat tuna slice. The method comprises the following steps: preprocessing raw materials; slicing; seasoning, namely adding 490 to 510g of tuna, 15 to 20g of white granulated sugar, 6 to 8g of table salt, and 10 to 15g of bean flour, then adding 5 to 8g of cinnamon, clove, ginger powder and aginomoto, finally adding 2 to 3g of a water activity water-retaining agent, and seasoning for 3 to 5 hours; uniformly spreading the seasoned slices; drying through an oven for 6 to 8 hours at the temperature of 40 to 45 DEG C until the water content reaches 20 to 25wt%; moving out the slices; baking through an infrared baking machine for 5 to 8 minutes at the temperature of 160 to 180 DEG C until the centers of the slices reach the temperature of 85 to 95 DEG C; drying, namely, drying to dewater the slices by hot air until the water content ranges from 15 to 17wt%; cooling the dried slices to reach room temperature; and introducing nitrogen and packing to obtain the finished product. The processing method is reasonable in preparation process and easy to operate; the processed ready-to-eat tuna slices are uniform in color, fresh and delicious in taste, and unique in flavor, and meets the demands of modern people on convenient, ready-to-eat, healthy and nutritional aquatic products; in addition, the expiration date of the product can be prolonged, and therefore, the commercial value of the tuna slice can be increased.
Owner:ZHEJIANG OCEAN UNIV

A kind of preparation method of porous foamed iron-nickel-chromium alloy material

The present invention is a preparation method of a porous foamed iron-nickel-chromium alloy material, which is characterized in that: the steps include: selecting a porous material, immersing a water-based polymer adhesive at normal temperature; spraying nano-chromium powder evenly on the Immersion on the surface of porous material with water-based polymer adhesive; drying; separating excess chromium powder from porous material matrix; dip-coating conductive adhesive on chromium porous material; electrodepositing iron-nickel alloy after heating and curing treatment on chromium porous material ; Oxidation-reduction treatment; Carrying out secondary diffusion treatment of chromium to obtain porous foamed iron-nickel-chromium alloy material. Its preparation method is scientific, the selected process parameters are reasonable, the quality is easy to control, the cost is low, and it can be produced with light weight, large specific surface area, super thickness, thickness of 5-100mm, high porosity of 96-99.9%, high temperature resistance and corrosion resistance. Excellent, able to meet the requirements of high temperature resistance, corrosion resistance and other harsh working conditions. It is especially suitable as high-temperature filtration, chemical catalysis, carrier, burner gas distribution and high-temperature flame-retardant materials.
Owner:JILIN ZHUOER TECH

Determination method of normal anisotropy coefficient of pipe in any direction

ActiveCN110763568AAccurately reflect plastic propertiesFully reflect the plastic flow characteristicsMaterial strength using tensile/compressive forcesExperimental methodsElement analysis
The invention discloses a determination method of a normal anisotropy coefficient of a pipe in any direction, and belongs to the field of pipe performance testing. The method comprises the steps of firstly establishing a relational expression between the normal anisotropy in any direction and a yield function, determining an undetermined coefficient of the yield function through a pipe bidirectional loading experimental method, and then determining the normal anisotropy coefficient of the pipe in any direction by substituting the established relational expression. The method ensures the accuracy and reliability of the normal anisotropy coefficient from three aspects, 1) blanks of related experiments are original tube blanks, the shape of the tube cannot be damaged, pre-deformation cannot be introduced, and the obtained experiment result can accurately reflect the plasticity of the tube; 2) an advanced yield function can be selected, and experimental data under different loading paths can be introduced simultaneously, so that the plastic flow characteristic of the pipe can be reflected more comprehensively; and 3) characteristic experiments for obtaining the same deformation in different directions are designed, and the accuracy and reliability of the coefficients of the shearing components can be ensured by repeatedly iterating the finite element analysis and the characteristicexperiments, thereby establishing an accurate and reliable yield function.
Owner:DALIAN UNIV OF TECH

Heat treatment technology for engine shield

The invention discloses a heat treatment technology for an engine shield. The heat treatment technology comprises the steps of 1) carrying out normalizing, specifically, carrying out secondary normalizing treatment on the cast-formed engine shield; 2) carrying out high-temperature tempering, specifically, carrying out heat preservation on the normalized shield in a furnace at 340-380 DEG C for 6-8 hours, carrying out high-temperature tempering to increase the temperature to 670-730 DEG C, carrying out heat preservation for 8-10 hours, gradually cooling the shield until the temperature is lower than 120 DEG C, and discharging the shield from the furnace; 3) carrying out quenching, specifically, raising the temperature of the shield to 680-720 DEG C, carrying out heat preservation for 2-3 hours, increasing the temperature to the quenching temperature of 820-880 DEG C, carrying out heat preservation for 4-5 hours, and then carrying out water cooling to the room temperature; and 4) carrying out annealing, specifically, the shield is finally heated to 380-420 DEG c, carrying out heat preservation for 8-10 hours, increasing the temperature to the annealing temperature of 660-720 DEG C, carrying out heat preservation for 10-12 hours, and carrying out air cooling to the room temperature. According to the heat treatment technology, the heating temperature is properly increased and the heat preservation time is prolonged, and therefore the structure of alloy steel of the engine shield can be fully converted, the mechanical property and the impact toughness of the engine shield can be effectively improved, and the good comprehensive mechanical property requirements of the automobile engine shield can be met.
Owner:SHANDONG ZHONGTUO NEW ENERGY CO LTD

A device for simulating the initial solidification of molten steel in a mold

The invention discloses a device for simulating initial solidification of liquid steel in a crystallizer. The inner surface of a heating electric furnace is covered with a fireproofing layer. A liquid steel cavity is formed in the fireproofing layer. A fireproofing baffle is arranged at the bottom of the liquid steel cavity. A first lifting rod penetrates the bottom of the heating electric furnace and is fixedly connected with the fireproofing baffle. The water-cooling crystallizer is located on the heating electric furnace, and the water-cooling crystallizer and the heating electric furnace are in sealing connection through a sealing ring. A second lifting rod is vertically arranged on the water-cooling crystallizer. The lower end of the second lifting rod is connected with a thermocouple. The device has the capability of directly obtaining an initial solidification blank shell in the crystallizer, simulates the solidification behavior of the initial solidification blank shell in the crystallizer by extruding liquid steel to move reversely and can guarantee the stability of the liquid steel face, and the steel liquid face coincides with the actual site continuous casting liquid steel face better. By means of the obtained continuous casting blank initial solidification blank shell and combination of macroscopic heat transferring solidification and microstructure, more reasonable technical parameters can be designed, and then quality defects of the continuous casting blank are reduced.
Owner:NORTHEASTERN UNIV LIAONING

Device for simulating initial solidification of liquid steel in crystallizer

The invention discloses a device for simulating initial solidification of liquid steel in a crystallizer. The inner surface of a heating electric furnace is covered with a fireproofing layer. A liquid steel cavity is formed in the fireproofing layer. A fireproofing baffle is arranged at the bottom of the liquid steel cavity. A first lifting rod penetrates the bottom of the heating electric furnace and is fixedly connected with the fireproofing baffle. The water-cooling crystallizer is located on the heating electric furnace, and the water-cooling crystallizer and the heating electric furnace are in sealing connection through a sealing ring. A second lifting rod is vertically arranged on the water-cooling crystallizer. The lower end of the second lifting rod is connected with a thermocouple. The device has the capability of directly obtaining an initial solidification blank shell in the crystallizer, simulates the solidification behavior of the initial solidification blank shell in the crystallizer by extruding liquid steel to move reversely and can guarantee the stability of the liquid steel face, and the steel liquid face coincides with the actual site continuous casting liquid steel face better. By means of the obtained continuous casting blank initial solidification blank shell and combination of macroscopic heat transferring solidification and microstructure, more reasonable technical parameters can be designed, and then quality defects of the continuous casting blank are reduced.
Owner:NORTHEASTERN UNIV
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