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162results about How to "Short firing time" patented technology

Lithium-titanium oxide type lithium ion sieve absorbent and method for preparing precursor thereof

The invention discloses a lithium-titanium oxide type lithium ion sieve absorbent and a method for preparing a precursor thereof, and relates to a method for preparing an inorganic absorbent for absorbing enriched lithium from salt lake brine, seawater and other liquid lithium resources. The method is characterized in that: titanium dioxide and lithium salt are taken as raw materials, ground by a ball grinder and dried so as to prepare a precursor Li2TiO3 of an ion sieve through a high-temperature solid-phase roasting method; and the lithium is eluted from the precursor Li2TiO3 by inorganic acid to prepare an ion sieve H2TiO3. The method has the advantage of simple technology, and the obtained ion sieve has the advantages of low solution loss and high adsorption capacity.
Owner:CENT SOUTH UNIV

Integrated utilization method of low grade magnesite

The invention belongs to the fields of integrated utilization technology of magnesite and environmental protection, and relates to an integrated utilization method of low grade magnesite. The method comprises steps of: magnesite fragmentation; ore grinding; ore dressing; ore dressing product calcining; conversion of calcined useful components into magnesium salt to prepare high purity magnesium oxide or direct electrolysis of the calcined useful components into magnesium metal or preparation of refractory material; and recovery utilization of gas generated by calcination. The invention comprehensively utilizes useful ingredients in the magnesite, realizes zero discharge of magnesite mine tailing, increases utilization rate of low grade magnesite and efficiently utilizes ore resource; and especially, fluidized roasting by a horizontal fluidized bed saves energy consumption and maximize economic benefit.
Owner:UNIV OF SCI & TECH BEIJING

Ceramic permeable bricks and method for producing the same

The invention provides a ceramic water permeable brick and a method for manufacturing the same. The ceramic water permeable brick comprises the following components in weight percentage: 75 to 85 percent of waste ceramic powder, 2 to 5 percent of waste glass powder, 10 to 20 percent of low-temperature clay, 2 to 5 percent of limestone, 2 to 5 percent of dextrin, 0 to 6 percent of albite and 2 to 5 percent of water. The preparation process comprises the following steps: (1) the waste ceramics, the waste glass, the low-temperature clay and the limestone are crushed and sieved; (2) material mixing; (3) the dextrin is added to water and heated; (4) waste ceramic grains are mixed with dextrin water; (5) other powder materials are added and stirred; (6) the mixing pulp is added into a die and subjected to press forming by a pressing machine; (7) drying; (8) the mixing pulp after drying is burned at a temperature of between 1,100 and 1,200 DEG C for 5 to 6 hours; and (9) checking. The application of the water permeable brick has the advantages of having short burning time, simple process method, lower production cost, good water permeable performance, high strength and high utilization rate of waste, and solving the problem of utilizing waste ceramics, protecting the environment and saving natural resources, and so on; and the ceramic water permeable brick can be widely used to pave roads in public places such as squares, parks, sidewalks, parking lots.
Owner:邱陶辉

Sagger for mullite-cordierite lithium battery cathode material and preparation method thereof

The invention relates to a sagger for a mullite-cordierite lithium battery cathode material and a preparation method thereof. According to the technical scheme, by weight, 30-35 of mullite particles, 20-25% of mullite fine powder, 30-35% of cordierite particles, 4-7% of dextrin and 5-7% of Guangxi white mud are mixed and stirred to obtain a mixture A; by weight, 30-35% of mullite fine powder, 30-35% of magnesium aluminate spinel fine powder and 35-36% of andalusite fine powder are stirred, dried and ground to obtain a mixture B; then, the mixture A is placed into a mold, the mixture B is uniformly sprayed on the surface of a pressure head, mechanical pressing is performed in the mode that a bowl opening faces downwards, drying is performed under the temperature of 1,300-1,400 DEG C, and the temperature is kept constant for 5-6 h to obtain the sagger for the mullite-cordierite lithium battery cathode material. The sagger is low in cost, simple in technology and high in yield; the prepared sagger for the mullite-cordierite lithium battery cathode material is high in volume density, high in compression strength, good in thermal shock resistance and good in corrosion resistance.
Owner:WUHAN UNIV OF SCI & TECH +1

Electrolyzer circumfluence calcination method

ActiveCN101550563AUniform firing temperatureEvenly distributedElectrolysisEngineering
The present invention provides electrolyzer circumfluence calcination method, when installing the electrolyzer, between the anode seam, center seam and inside edge cavity are provided with no materials, installing the electrolyzer in full cavity mode, then using the medium generated heat to calcine cathode lining of the electrolyzer in multiple heat transferring modes of radiation, convection and heat transmission etc, smoke generated by pressure difference during calcination circumfluence in the electrolyzer to make sure calcination temperature of all the sections is uniform, and avoids problem of heat stress centralization and sodium enriching in part effectively; a high-temperature insulation thermal insulating layer is lay in anode seam cavity, center seam cavity and top of edge cavity in the electrolyzer for reducing heat loss effectively, improving warming speed, shorting calcination time, saving energy sources and helpful for earlier regular production of the electrolyzer, meanwhile can reduce calcination energy consumption effectively and improve affect of radiation on operation environment; and the most important is that, using full electrolytes powder to instead of cryolite can reduce calcination startup cost greatly.
Owner:YUNNAN RUNXIN ALUMINUM

Al4SiC4 material synthetic method

The invention relates to an Al4SiC4 material synthetic method. An employed technical scheme comprises the following steps by weight percentage: taking 45-65% of Al powder, 20-35% of SiC powder, 15-30% of powdered carbon and uniformly mixing with absolute alcohol while planetary ball milling, drying under the temperature of 80-120 DEG C, shaping, then imbedding a sample in a graphite crucible equipped with metal aluminum powder, placing the graphite crucible in a furnace, under the imbed carbon condition, heating and insulating for 2-7 hours under the temperature of 1500-1700 DEG C, cooling and removing the sample from the graphite crucible and then removing an impurity layer on the surface to obtain the Al4SiC4 material. According to the invention, the material can be synthesized without protection atmosphere of vacuum or inert gas and the like, the technology is simple, the synthesis temperature is low, the obtained product possesses high yield and purity, and is adapted to large scale production. The product can be used for ceramic matrix components, and can be used as an additive to be introduced to a carbonaceous refractory material for increasing its antioxidation performance.
Owner:SHANDONG UNIV OF SCI & TECH

Pretreatment method for refractory gold ore with antimony and arsenic

The invention relates to the technical field of metallurgy, in particular to a pretreatment method for refractory gold ore with antimony and arsenic. The method comprises the steps that 1, the refractory gold ore with antimony and arsenic is broke and subjected to ball milling to form powder; 2, the powder obtained in the step 1 is added into a hermetic vertical pipe type heating furnace, neutral protective gas is introduced in, roasted ore is obtained after roasting and cooling are carried out, produced tail gas enters a tail gas collection device, collected smoke dust is leached through a mixed solution of Na2S with the concentration of 50-200 g / L and NaOH with the concentration of 20-100 g / L, solid-liquid separation is carried out, a filter residue with arsenic and a leaching solution with antimony are obtained, and the leaching solution is electrodeposited to produce metal antimony, wherein leaching time is 30-180 min, and leaching temperature is 20-95 DEG C. The pretreatment method has the advantages that the technological process is simple, operation is flexible, roasting time is short, energy consumption is low, antimony and arsenic can be synchronously removed, smoke gas is low in toxicity and small in amount, and economic and social benefits are good.
Owner:BEIJING MINING & METALLURGICAL TECH GRP CO LTD

Method for preparing puddling iron concentrate by high-alumina iron ore

ActiveCN101037722ATo achieve the effect of dealuminationReduce energy consumptionProcess efficiency improvementGranularityLower grade
The invention disclosed a method for manufacturing the iron ore concentrate for ironmaking by the high aluminium iron ore, wherein after iron ore is broken to the granularity of less than 1.0mm which is in 40%-60%, it is mixed with Na2CO3 based on the proportion of 10-40 weight percent, and is braked for 10-30 minutes at the temperature of 900-1050 DEG C, then placed in the reactor to be extracted by 100-150 g / l solution at the temperature of 80-150 DEG C based on the liquid-solid quality rate of 3 / 1 -6 / 1 for 5-30 minutes, the filtrate can be extracted by the dilute sulphuric acid of 1.0-15 mass concentration percent at the temperature of 80-120 DEG C after solid-liquid separation for 10-30 minutes, and the solid is the iron ore concentrate after solid-liquid separation. The content of Al2O3 and Na2O in ore concentrate satisfies the requirement of blast furnace ironmaking materials using the invention. The invention can sufficiently and reasonably use existing rich high aluminium low-grade iron ore with good dealuminzation and low cost for reusing the extractive alkali liquor. The invention is suitable for the dealuminzation of each aluminiferous iron ore, in particular, high aluminium iron ore for reducing the close symbiosis and interdigitating of aluminium-containing minerals and iron-containing minerals, the manufactured iron ore concentrate can be used as the blast furnace ironmaking materials.
Owner:CENT SOUTH UNIV

Method and device for preparing aluminum-smelting carbon material, and used raw material

The invention discloses a method and a device for preparing aluminum-smelting carbon material, and a used raw material, wherein the method comprises the steps of artificially selecting and crushing electrolytic aluminum wastes; obtaining carbon powder by magnetic selection and floatation process; kneading the carbon powder, asphalt and tar, obtaining roasting material; putting the roasting material to a medium frequency induction roasting furnace, stacking the roasting material on four sides of the graphite heating ring; finally, and roasting the material by heating of the graphite heating ring. The method and the device of the invention directly take the carbon powder in the carbon-containing waste slag as raw material of the aluminum-smelting carbon material, so that the recovery value and processing capability of the waste material of an aluminum manufacturer are improved. Meanwhile, the used medium frequency induction roasting furnace has short roasting time and high temperature, so that the production energy consumption is reduced and the production time is shortened.
Owner:周俊和 +1

Antique matte cracked glaze and preparation technology thereof

The invention discloses antique matte cracked glaze and a preparation technology thereof. The cracked glaze comprises the following raw materials in parts by weight: 25-30 parts of feldspar, 40-45 parts of limestone, 5-10 parts of kaolin, 5-10 parts of calcined kaolin, and 9-15 parts of quartz. The preparation technology of the antique matte cracked glaze comprises the following steps that: the raw materials are uniformly mixed to obtain a mixture; water is added into the mixture with the weight ratio of the mixture to the water being equal to 1:0.80, and ball-milling and sieving are performed on the mixture and the water to obtain a glaze material of the cracked glaze; and a red clay porcelain body coated with the glaze material is sintered, and then the sintered red clay porcelain body is colored, thus obtaining the finished product of the antique matte cracked glaze. The glazed effect of the antique matte cracked glaze is stable; the glaze color of the antique matte cracked glaze is slightly dim, so that the antique matte cracked glaze is more of an antique beauty; in addition, as the sintering time for a single batch of the antique matte cracked glaze can be 12 hours, the quick sintering adaptability of the antique matte cracked glaze is high, so that the antique matte cracked glaze is applicable to volume production; and as the sintering time is short, the efficient production is realized, the aims of energy conservation and environmental friendliness are achieved, the production cost of the antique matte cracked glaze is reduced, and the market competitiveness of theantique matte cracked glaze is improved, so that the antique matte cracked glaze has very high social and economic benefits.
Owner:FUJIAN JIAMEI GRP +1

Sludge treatment apparatus for water conservancy project

The invention relates to a sludge treatment apparatus for a water conservancy project. The sludge treatment apparatus comprises a transport apparatus, a stirring chamber, a transport pipeline part, a sludge filter chamber, a sludge mixing and drying part, a mixing and granulating chamber and a ceramsite heating chamber. By arranging various parts, the sludge treatment, the ceramsite preparation from sludge and the ceramsite forming can be continuously carried out, so that not only can the sludge containing heavy metal be removed and the secondary pollution of the sludge to a water body be avoided, but also heavy metal elements are secondarily utilized for the ceramsite, and the harmful sludge can be actually turned into benefit.
Owner:畅庆环保科技(太仓)有限公司

Light heat-preserving brick and fabrication method thereof

The invention discloses a light heat-preserving brick and a fabrication method thereof. The light heat-preserving brick comprises a green body layer and can also comprises a glaze layer which can totally or partly cover the green body layer, wherein the green body layer includes the following compositions, by weight: 60.0-70.0 pyrophyllite, 3.0-8.0 clay, 20.0-25.0 white talc, 3.5-5.0 feldspar, 0.5-1.4 glass and 0.3-0.8 carbonate. The method includes the steps of fabricating the green body layer, fabricating the ground glaze and fabricating the spot glaze. The light heat-preserving brick has the advantages of light weight, heat preservation property, big strength and attractive appearance.
Owner:厦门三荣陶瓷开发有限公司

Raney nickel catalyst used for low-pressure hydrogenation of dinitrotoluenem, preparation method and application thereof

A Raney nickel catalyst used for low-pressure hydrogenation of dinitrotoluenem. The catalyst is characterized by comprising, by mass, 80-90 wt% of nickel, 5-10 wt% of aluminium and 1.65-10 wt% of an auxiliary agent metal, wherein the nickel is in the form of a simple substance, the aluminium is in the form of the simple substance of an oxide and the auxiliary agent metal is in the form of the oxide. The catalyst is low in price and has an excellent performance of catalytic hydrogenation of the dinitrotoluenem (DNT) without an additional solvent and under a low-pressure condition of 1Mpa.
Owner:TAIYUAN UNIV OF TECH +1

Ultra-light fully-closed-cell foamed ceramic with compact surface and low-temperature firing method of ultra-light fully-closed-cell foamed ceramic

The invention discloses ultralight fully-closed-cell foamed ceramic with a compact surface. According to the invention, quartz sand is taken as a main material, calcium carbonate is taken as a foaming agent, borax is taken as a fluxing agent and zinc oxide, albite, potassium feldspar and spodumene are taken as conditioning agents; and a sintering temperature is 740 to 800 DEG C. The invention further discloses a low-temperature firing method of the ultralight fully-closed-cell foamed ceramic. The preparation technology disclosed by the invention has the remarkable advantages of simple process, low sintering temperature, short sintering time and the like, so the manufacturing cost of the method is far lower than the manufacturing cost of existing preparation technology. Besides, different from foamed ceramic prepared in the prior art, the interior of the ultralight fully-closed-cell foamed ceramic with the compact surface is of a porous structure, pores are independent from one another and do not communicate with each other, the surface is continuous and compact and free of pores, the heat preservation and sound insulation effects of the foamed ceramic can be remarkably improved, the foamed ceramic has excellent waterproof and moisture-proof performance, and the reliability of a product is obviously improved.
Owner:YANTAI UNIV

A compound roasting additive for extracting vanadium pentoxide from vanadium-containing stone coal and its application

The invention relates to a composite roasting additive used in the roasting process of vanadium-containing stone coal and application of composite roasting additive. The composite roasting additive comprises the following components in percentage by mass: 35 to 45 percent of sodium fluoaluminate, 40 to 50 percent of calcium fluoride, and 15 to 25 percent of hyperoxide of alkali metal, wherein the hyperoxide of the alkali metal is sodium hyperoxide or potassium hyperoxide or calcium hyperoxide. When the composite roasting additive is used, the adding amount of the composite roasting additive for extracting vanadium pentoxide from the vanadium-containing stone coal is 1 to 6 percent of the mass of the vanadium-containing stone coal, the composite roasting additive and the vanadium-containing stone coal are fully mixed uniformly, the roasting temperature is 700 to 900 DEG C, and the roasting time is 1 to 4 hours. Compared with the prior art, the composite roasting additive has the advantages of (1) low adding amount, (2) low roasting temperature and short roasting time, (3) no smoke pollution, (4) high leaching rate, (5) wide additive component source, and (6) good adaptability.
Owner:WUHAN INSTITUTE OF TECHNOLOGY

Production method for quickly firing aventurine glaze for stoneware

The invention relates to a production method for quickly firing aventurine glaze for stoneware, comprising the following raw materials: clinker 1#, clinker 2#, potassium feldspar powder, talcum powder, quartz, Guizhou soil, spodumene and calcined iron oxide red, wherein the formula of clinker 1# includes borax, quartz, soda ash and potassium feldspar, and the formula of clinker 2# includes borax,glass, quartz, potassium feldspar, calcite and potassium nitrate; wet ball milling is adopted; the proportion of selected material to ball to water is 1 : 2 : 0.46; the smashed material of the clinkers and the rest materials are put into a ball mill to be subjected to ball milling until reaching 250 meshes, and the rest material is less than 0.3 percent, and then a slurry with the concentration of 45 baume degree is prepared; a glaze dipping manner is adopted to glaze a stoneware green body, the thickness of the glaze layer is controlled to be 0.6-0.8mm, and then the aventurine glaze is produced by sintering in a fast tunnel furnace at the temperature of 1180-1196 DEG C. The aventurine glaze is simple to produce, can be quickly sintered in the tunnel furnace, and has short sintering time and bright glazing color, and the aventurine glaze surface is bright and flickers under the irradiation of light, thus giving people a luxury and elegant impression.
Owner:湖南陶润会文化传播有限公司

Method for roasting and preheating aluminum electrolysis cell using direct currents

InactiveCN102912377AImprove roasting effectRealize low-carbon roastingCell cavityRadiative heating
The invention relates to a method for roasting and preheating an aluminum electrolysis cell using direct currents and is characterized in that radiation heating tubes are used for replacing scorched particles to serve as heating media, and currents of an electrolytic cell series are connected, so that heat produced by the radiation heating tubes in a electrolysis cell cavity is transferred to the surrounding to heat, warm and roast linings and anodes in an electrolysis cell cathode continuously in radiation, convection and heat conduction modes, a heating device is detached after the temperature reaches or approaches a roasting start temperature of the electrolysis cell, and electrolyte is infused to start the heating device. Compared with traditional roasting methods, the method for roasting and preheating the aluminum electrolysis cell using direct currents has the advantages that the roasting effect is good, the energy consumption is low, the environment benefit is good, the labor intensity is low and the like.
Owner:YUNNAN RUNXIN ALUMINUM

Method for preparing ceramsite by using Xianfeng diatomite

The invention discloses a method for preparing ceramsite by using Xianfeng diatomite. The method comprises steps of: crushing a naturally dried raw material Xianfeng diatomite; mixing the raw material with water in a ratio of 100:60-70 and stirring uniformly; air-drying the mixture to a water content of 40-50%; moulding; air-drying naturally; and finally sintering to obtain high strength diatomite ceramsite. The method of the invention is simply operated, has good effect; and the ceramsite prepared by the method has good strength, reduced water absorption, strong durability and wide application scope.
Owner:KUNMING UNIV OF SCI & TECH

Novel tunnel-type folded-rail continuous sintering furnace and sintering method thereof

InactiveCN102620559ARigorous and simple structureSmall footprintFurnace typesSlagTemperature difference
The invention relates to a novel tunnel-type folded-rail continuous sintering furnace and a sintering method thereof. The novel tunnel-type folded-rail continuous sintering furnace comprises a furnace body, wherein one end of the furnace is open while the other end of the furnace is closed; an upper layer of roll-type or push-plate-type conveying devices (3) and a lower layer of roll-type or push-plate-type conveying devices (2) which are folded and move in opposite directs are arranged in the inner cavity of the furnace; a slag falling-preventing baffle plate (6) and a carrying mechanism (10) capable of doing an up-and-down reciprocating movement are arranged between the two layers; and a heating device (9) and a fuel gas curtain separating nozzle (8) are arranged in the inner cavity of the lower layer of the furnace. By virtue of a super-fast single-sided heating sintering mechanism, and by the adoption of a pair of opposite conveying devices with an extremely high heat exchanging rate and an extremely high afterheat utilizing rate, the temperature difference between the upper layer and the lower layer can remain about 150-300 DEG C at the same section, thus achieving the most economical ceramic continuous sintering state; therefore, the novel tunnel-type folded-rail continuous sintering furnace is a novel continuous sintering furnace with a super-high sintering speed, an extremely high heat exchanging rate and a super-short length.
Owner:JIANGXI KOAON IND

Crackle glaze and manufacturing process

The invention discloses crackle glaze and a manufacturing process. The crackle glaze is composed of a transparent glaze material and a high-expansion glaze material according to a mass percentage. The transparent glaze material and the high-expansion glaze material are composed of silicon dioxide, aluminum oxide, potassium feldspar, albite, calcium carbonate, borax and barium carbonate of different mass percents. The raw materials are evenly mixed in proportion, the mixture and water are mixed in proportion, a crackle glaze material is obtained after ball milling and sieving, the surface of a ceramic green body is coated with the crackle glaze material and then the ceramic green body is sent into a heating-up furnace to be fired, a semi-finished product with a crackle cracked glaze effect is obtained after drawing and cooling, and cracks on the outer surface of the semi-finished product are colored. The crackle glaze is simple in composition and rational in formula, the glaze effect of the manufactured crackle glaze is stable, the crack effect is good, and the crackle glaze is more uniform and attractive. The firing time in the manufacturing process is short, the firing temperature is low, so that the energy consumption is reduced, the crackle glaze saves energy and is environmentally friendly, and the production cost is reduced.
Owner:MYINGFA CERAMIC CO LTD DEHUA FUJIAN

Roasting method for extracting vanadium from vanadium-containing shale

The invention relates to a roasting method for extracting vanadium from vanadium-containing shale. According to the technical scheme of the invention, the method comprises the following steps of: uniformly mixing vanadium-containing shale raw ore with a vanadium-containing shale extraction roasting additive in a ratio of 1:(0.06 to 0.1), feeding the mixture to a roasting furnace, heating to 850 to 1000 DEG C at a temperature rise rate of 400 to 500 DEG C / h, maintaining the temperature for 1 to 2 hours, then adding the roasted product to dilute sulfuric acid with volume fraction of 4 to 10% in a solid-liquid mass ratio of 1:2, and leaching at 90 to 100 DEG C for 0.5 to 1 hour under the condition of stirring. The preparation method of the vanadium-containing shale extraction roasting additive comprises the steps of: preparing Mg compounds, namely NaClO3, Na2CO3 and CaCO3 and mixing uniformly, wherein the mass ratio of NaClO3:Na2CO3:CaCO3 is 1:1:(4 to 8):(6 to 10); and grinding until the particle size is not more than 0.15 mm. The method provided by the invention increases the leaching rate up to 86% to 87% and has the characteristics of high recovery rate, short roasting period, high leaching speed and little roasting pollution.
Owner:WUHAN UNIV OF SCI & TECH

Ion-aluminum separation technique of high-alumina brown iron ore

InactiveCN101037721ARaise the gradeFacilitate the dissolution reactionProcess efficiency improvementRational useMaterials science
The invention discloses a process for separating iron and aluminium from high aluminium brown iron ore, wherein brown iron ore is broken to the granularity of less than 1.0mm, and is actived and braked for 10-20 minutes at the temperature of 400-500 DEG C, then placed in the reactor to have a stripping dealuminzation by 100-150 g / l NaOH solution at the temperature of 120-150 DEG C based on the quality liquid-solid rate of 3 / 1 -6 / 1, the time of stripping is 20-45 minutes, the filtrate can be causticized and be back to reuse after solid-liquid separation, and the filter cake is reacted with lime solution at the temperature of 100- 140 DEG C for 30-50 minutes and then solid-liquid separation, accordingly Al2O3 content can be reduced to 3.0%, and Na2O content can be less than 0.25% in the iron ore concentrate, while iron ore concentrate grade can be greatly improved. The invention is usable for the iron and aluminium separation of brown iron ore with higher-content aluminium oxide in the form of gibbsite of aluminium mineral with good dealuminzation and low process cost, the content of Al2O3 and Na2O in ore concentrate satisfies the requirement of blast furnace ironmaking materials, provided a powerful technical support for the rational use of existing rich high aluminium brown iron ore.
Owner:CENT SOUTH UNIV

Method for performing flash reducing and roasting on zinc calcine

The invention discloses a method for performing flash reducing and roasting on zinc calcine. The method comprises the following steps: adding the zinc calcine and material conveying gas into a flash roasting furnace in a jet mode; and dropping the zinc calcine in the flash roasting furnace in a suspended state, and roasting. According to the method, the energy consumption is low, zinc ferrite in the zinc calcine can be rapidly and completely decomposed and reduced, and according to the method, economic value is high, and industrialized production can be realized.
Owner:CENT SOUTH UNIV

Method for preparation of silicon nitride bonded silicon carbide refractory material by using silicon cutting waste mortar

The invention discloses a method for preparation of silicon nitride bonded silicon carbide refractory material by using silicon cutting waste mortar, and the method comprises the following steps: (1), preparing raw materials, wherein the raw materials including, by weight, 5%-20% of the silicon cutting waste mortar, 50%-80% of silicon carbide, 2%-20% of silicon nitride and 1%-10% of alumina; (2), adding the raw materials into absolute ethanol for wet ball milling; (3), drying the raw materials treated by the wet ball milling; (4), adding PVA (polyvinyl acetate) to the dried raw materials for granulation to prepare blank, wherein the mass of the added PVA being 3%-8% of the mass of the raw materials; and (5), sintering the blank in air atmosphere into the silicon nitride bonded silicon carbide refractory material. The method can realize full utilization of the silicon cutting waste mortar, has no secondary pollution, also does not need the protection of nitrogen, and only needs an electric furnace for heating in the air atmosphere to prepare the low-volume-density and high-flexure-strength silicon nitride bonded silicon carbide refractory material, and can reduce environment pressure, turn waste into treasure, reduce the production cost and realize industrialized production.
Owner:CHANGZHOU GUICHENG BUILDING MATERIALS CO LTD

Method for preparing corundum abrasive by microwave sintering

The invention discloses a method for preparing corundum abrasive by microwave sintering, and belongs to the technical field of abrasive preparation. The corundum abrasive comprises the following raw materials in percentage by weight: 95-98% of Al2O3, 0.5-2.5% of SiO2, 0.5-1% of MgO, 0.2-1% of TiO2, 0.2-1% of MnO2, and 0.1-1% of CuO. The method comprises the following steps: mixing the raw materials; molding; crushing; sieving; grading; performing rubber removing; transferring the rubber-removed blank particles into an SiC crucible; increasing the temperature to reach 1300-1500 DEG C at the rate of 10-20 DEG C per minute; then maintaining the temperature for 5-30min, and performing microwave sintering to obtain the corundum abrasive. With the adoption of the method, energy consumption of the corundum abrasive production can be greatly decreased; in addition, the blank particles are in contact with each other, so that the clearances among the particles are small, the temperature gradient of a sintered body can be reduced, the sintering time is greatly decreased, and as a result, the corundum abrasive sintering quality can be improved.
Owner:河南建筑材料研究设计院有限责任公司

Regeneration method of inactivated titanium silicon molecular sieve

The invention discloses a regeneration method of an inactivated titanium silicon molecular sieve, specifically comprising the following steps of: mixing organic acid with an inactivated silicon molecular sieve and putting in a sealed reaction kettle, treating for 1 hour under the temperature of 40-150DEG C, continuously treating for three times, washing products by deionized water under normal temperature and normal pressure, drying, and roasting, so that the regenerated titanium silicon molecular sieve can obtained, wherein the lowest place in the reaction kettle contains the water quantity forming into saturated steam under a reaction condition, and the molar ratio of the inactivated titanium silicon molecular sieve, the organic acid to the water is 1.04: (0.002-0.5): (0.5-20). The regeneration method is low in energy consumption, and less in three-waste discharge, and the regenerated titanium silicon molecular sieve can be basically recovered to the activity level of the fresh catalyst.
Owner:CHINA TIANCHEN ENG +1

Method of manufacturing object with low reflection film

InactiveCN103842098AShort drying or firing timeShort coating timeCoatingsSpecial surfacesManufactured ObjectLow volume
Provided is a method of manufacturing an object with a low reflection film, with which it is possible to form a low reflection film with which it is possible to handle a wide substrate, have a comparatively rapid speed of conveyance of the substrate, a comparatively low volume of required coating compound, a comparatively short time for drying, firing, and / or application, and a uniform thickness, as well as have superior thickness controllability whereby a low reflection film having thickness which is arbitrarily optically designable is easily formed. When forming, upon a substrate (2) which is conveyed in a prescribed direction, a low reflection film by applying a coating compound (20) by a coating roll (14) of a reverse roll coater (10), the rotation speed of the coating roll (14) is made slower than the conveyance speed of the substrate (2), and the coating compound (20) includes a dispersal medium (a), fine particles (b) which are dispersed in the dispersal medium (a), and a binder (c) which is either dissolved or dispersed in the dispersal medium (a), wherein the viscosity is 1-10mPa.s.
Owner:ASAHI GLASS CO LTD

Matte glaze and production process thereof

InactiveCN109896745AHas color protectionImprove bindingTemperature controlCalcium biphosphate
The invention provides matte glaze and a production process thereof. The matte glaze comprises 25-30 parts of kaolin, 10-16 parts of clay, 8-12 parts of borax, 15-18 parts of matte frit, 5-8 parts ofbentonite, 3-5 parts of aluminum-magnesium hydrotalcite, 2-5 parts of kojic dipalmitate, 3-6 parts of calcium phosphate, 3-5 parts of calcium oxide and 9-12 parts of stannous chloride. The productionprocess includes: grinding, regulating glaze concentration, applying the glaze and performing oxidation firing to obtain a ceramic product with the matte glaze on the surface. The matte glaze producedaccording to the material proportion has the advantages that the glaze can be stably combined with a green body and be solidified into a polycrystalline structure during ceramic firing to achieve a matte effect, and the glaze is moderate in surface tension, smooth and mellow in surface and fine and smooth in texture. The production process is easy in temperature control, short in firing time andlow in production cost.
Owner:福建省德化县哈维陶瓷有限公司

Low-temperature semiwhite porcelain and manufacturing method thereof

The invention discloses a low-temperature semiwhite porcelain and a manufacturing method thereof, belonging to the technical field of ceramics. The blank of the low-temperature semiwhite porcelain comprises the following raw materials in parts by mass: 30-40 parts of Longyan clay, 25-35 parts of Gangxi kaolin raw ore, 20-28 parts of flint, 7-12 parts of feldspar, 2-9 parts of talcum and 5-10 parts of dolomite. The low-temperature semiwhite porcelain can be quickly fired at the low temperature of 1000 DEG C, and can be discharged out of the kiln only by 7-8 hours from firing to cooling. The linear shrinkage is low and can be kept at 12% or below. The low-temperature semiwhite porcelain has high hardness and excellent whiteness (85% or above), and has comparable whiteness with light-weight porcelain. The low-temperature semiwhite porcelain has low water absorptivity (which can be kept at 3% or below and can reach the porcelain industry standard), has the advantages of high strength excellent high temperature resistance and excellent microwave resistance, can be subjected to 180-DEG C drying oven testing more than twice, and can pass the microwave oven and dishwasher performance test. The low-temperature semiwhite porcelain has wide applicability, and can be widely used for producing medium / high-grade domestic ceramics.
Owner:FUJIAN DEHUA HUAMAO CERAMICS CO LTD

Cracked glaze and making process thereof

The invention discloses a cracked glaze and a making process thereof. The cracked glaze is composed of albite, kaolin, quartz, zinc oxide, barium carbonate and frits, wherein the frits are composed of quartz, red lead, feldspar, dolomite and barium carbonate, and the feldspar is composed of potassium feldspar and albite according to the mass ratio. The making process comprises the steps of smashing quartz, red lead, potassium feldspar, albite, dolomite and barium carbonate, uniformly mixing, and smelting to prepare the frits; and respectively smashing all the raw materials and the frits, uniformly mixing according to a certain ratio, then, adding water to stir, sieving by using a mesh screen after ball milling, coating the prepared glaze on the surface of a ceramic blank, firing in a roasting kiln, and cooling after taking the glaze out of the kiln. The cracked glaze disclosed by the invention is simple in component and reasonable in formula, the glaze surface effect of the prepared cracked glaze is stable, glaze surfaces with different effects can be made through changing the contents of the components, and the crack is good in effect and more uniform and attractive; and the making process is short in firing time and low in firing temperature, so that the energy consumption is reduced, the energy is saved, the environment is protected, and the production cost is reduced.
Owner:DEHUA HENGHAN ARTS
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