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45results about How to "The steps are simple and controllable" patented technology

Preparation and surface modification methods of ferrous titanate/iron trioxide composite photoelectrode

ActiveCN106119882AEasy to prepareHigh photoelectrocatalytic water splitting performanceElectrodesInorganic saltsDecomposition
The invention provides preparation and surface modification methods of a ferrous titanate/iron trioxide composite photoelectrode and relates to the field of materials. The preparation method of the composite photoelectrode includes the steps that FTO conducting glass is washed; the FTO conducting glass is placed in an inorganic salt water solution of titanium in the manner that the conducting face is downward, and the FTO conducting glass is soaked for 10-60 min at the temperature of 60-80 DEG C; the washed FTO conducting glass is heated for 10-30 min at the temperature of 150-200 DEG C; the heated FTO conducting glass is placed in a reaction still containing inorganic salt of iron and a mineralizer water solution, and the reaction still is heated for 2-5 h at the temperature of 60-100 DEG C; and the FTO conducting glass obtained after the reaction in the reaction still is taken out and washed, the washed FTO conducting glass is annealed for 1-3 h at the temperature of 500-600 DEG C and then annealed for 10-30 min at the temperature of 700-800 DEG C, and the nano ferrous titanate/iron trioxide composite photoelectrode is prepared. The preparation method of the composite photoelectrode is simple, experimental conditions are easy to control, and the prepared composite photoelectrode has high photoelectrocatalysis water decomposition performance.
Owner:SUZHOU UNIV

High dielectric microwave ceramic dielectric material and preparation method thereof

The invention discloses a high dielectric microwave ceramic dielectric material and a preparation method thereof. The material has the following formula: (1-x) (Sm0.5Li0.5) TiO3-xCaTiO3, wherein x uses the mole fraction and satisfies the relation of 0.15<=x<=0.20; and the material is prepared from the main raw materials of CaCO3, Li2CO3, TiO2 and Sm2O3. The preparation method of the high dielectric microwave ceramic dielectric material is as below: adding the raw materials to a mill pot, conducting wet milling for 14-18 h, baking, sieving, calcining at 1090-1110 DEG C for 2-3 h, and carrying out a solid state reaction to synthesize a principal crystalline phase powder; cooling the principal crystalline phase powder, adding the principal crystalline phase powder into the mill pot, conducting wet milling again for 14-18 h, drying, sieving, and conducting compression molding at pressure of0.4 to 0.5 tons to obtain a cylindrical base substrate; placing the base substrate in a alumina square porcelain boat with a platinum foil pad, burning with cover at 1290-1300 DEG C for 2-3 h into a porcelain, so as to obtain the final product. The invention provides a high dielectric microwave ceramic dielectric material, which has high microwave dielectric constant epsilon r while ensuring a low resonant frequency temperature coefficient tau f.
Owner:JIANGSU UNIV OF SCI & TECH

Fishy smell removing agent for yellow croakers and preparation and use method thereof

The present invention discloses a fishy smell removing agent for yellow croakers. The fishy smell removing agent is composed of the following raw materials in weight percentages: 22-50% of a yeast extract, 1-22% of a heartleaf houttuynia herb extract, 11-22% of a fresh ginger extract and 17-22% of edible salt. The fishy smell removing agent for the yellow croakers is prepare from the yeast extract, heartleaf houttuynia herb extract, fresh ginger extract and edible salt as the raw materials. These raw materials are natural and safe, free of chemical additives and combined in a specific ratio, enable the fishy smell removing agent for the yellow croakers to have a good fishy smell removing effect, can remove fishy smell of the yellow croakers and at the same time maintain the aroma of the yellow croakers and increase delicious taste and mellow feeling of fish fleshes. The fishy smell removing agent for the yellow croakers is mild in use conditions and can conduct the fishy smell removingtreatment at room temperature; fishy smell removing liquid and minced yellow croakers cannot be separated after the fishy smell removing treatment. Steps are simple and controllable, do not cause thenutrient loss in the minced yellow croakers, and can retain the delicious taste of the yellow croakers to the utmost extent.
Owner:NINGBO LANYANG AQUATIC FOOD

Method for preparing composite membrane through interfacial polymerization and reaction device

The invention belongs to the field of membrane preparation, and particularly relates to a method for preparing a composite membrane through interfacial polymerization. Themethod comprises the steps ofvertically fixing a support body in a reaction container with a liquid cavity, dividing the accommodating cavity of the reaction container into two parts by the support body, respectively adding a water phase and an organic phase into the two parts of the accommodating cavity, and standing; and after the two phases react and a polymer membrane layer is formed on the surface of the support body, ending the reaction to obtain the support body attached with the polymer membrane layer, namely the composite membrane; and solvents of the water phase and the organic phase being immiscible, and solutes in the water phase and the organic phase reacting with each other to form a polymer layer. The invention further relates to a reaction device adopting the method for preparing the composite membrane through interfacial polymerization. The reaction device comprises a container and a clamping mechanism, the clamping mechanism vertically fixes the supporting body in the container and divides the accommodating cavity of the container into a left part and a right part, and the two parts of accommodating cavity are respectively provided with a feeding port.
Owner:HEFEI UNIV

Method for preparing nanometer silver halide colloids

The invention discloses a method for preparing nanometer silver halide colloids. The method comprises the following steps: placing solid paraffin into de-ionized water with temperature of 70-100 DEG C for stirring to obtain paraffin / water microemulsion; adding metal halide salts with the molar concentration of 0.01-0.1 mol / L and AgNO3 aqueous solution to the paraffin / water microemulsion by using a double-dipping method, keeping the temperature and stirring to obtain uniformly dispersed mixed microemulsion; standing and naturally cooling to the room temperature, taking out a paraffin mass condensed on a water surface after oil-water separation occurs in the mixed microemulsion , adding a small amount of dispersing agent to the remaining microemulsion, and continuously stirring to obtain a silver halide colloid with stable dispersion. In the invention, the whole reaction process by using the solidification and melting of paraffin, is simple and easy to control, green and environmental friendly, and the paraffin can be recycled, thereby the invention is particularly suitable for industrial production. The microcosmic shape and appearance of nano particle in the prepared product has the characteristics of uniform size, excellent dispersing stability and non-decomposition when exposing to light.
Owner:JIANGSU NADN SCI TECH CO LTD

Cell model and constructing method thereof, and applications of cell model in screening active substances targeting serotonin receptor

The invention discloses a cell model for stably expressing a 5-HT1B (serotonin) gene, and a constructing method thereof, and applications of the cell model in screening of active substances targeting5-HT1BR (serotonin receptor), particularly in screening of anti-depression drugs and anti-migraine drugs, wherein the cell model is mammalian cells capable of carrying and stably expressing the 5-HT1Bgene. The constructing method comprises: linking a 5-HT1B gene to an expression vector to construct recombinant plasmid, introducing the recombinant plasmid into mammalian cells, and carrying out screening culture to obtain the cell line capable of stably expressing the 5-HT1B gene, wherein the cell line can be used for screening the active substance targeting 5-HT1BR. According to the present invention, whether the to-be-screened substance is screened is judged by determining the yield or the activation degree of the response element after the to-be-screened substance is added to the cell model culture medium, such that the high-throughput, low-cost and accurate screening of the active substance targeting 5-HT1BR can be achieved, and the good stability and the good reliability can be achieved.
Owner:EZHOU INST OF IND TECH HUAZHONG UNIV OF SCI & TECH

Preparation method of loquat vinegar drink

The present invention discloses a preparation method of loquat vinegar drink and relates to the technical field of drink processing. The loquat vinegar drink is prepared from loquat leaves, licorice, crystal sugar powder and pure water. The loquat leaves and licorice are boiled into solution, the solution, crystal sugar powder and pure water are poured into a porcelain jar, the temperature of the porcelain jar is heated to 85 DEG C until the crystal sugar powder is melt, the melt crystal sugar is cooled, acetic acid bacterium strains are inoculated into the cooled melt crystal sugar with a weight of 0.5%-2% of the total weight of the raw materials, the mixture is stirred evenly, and the stirred mixture is subjected to a sealed fermentation; after the completion of the fermentation, the obtained fermentation liquid is subjected to an acid regulation at an environment temperature of 20-28 DEG C and the total acid content of the fermentation liquid is controlled; and the acid regulated fermentation liquid is sterilized, the sterilized fermentation liquid is subjected to filling, and the fermentation liquid after being subjected to filling is put into a storage to be stored at 2-6 DEG C. The processes are simple, the steps are easy to control, and the prepared loquat vinegar drink is good in tastes, excellent in quality, soft in mouthfeel, refreshing and good in stability. Due to the addition of the licorice and loquat leaves, and at the same time, the loquat vinegar drink can prevent and cure symptoms of cough, excessive phlegm, etc., also has nutrients of the acetic acids, and is moderate in acidity and suitable for people at all ages.
Owner:吴林媛

A kind of metal fiber electric brush and preparation method thereof

The invention discloses a metal fiber brush and a preparation method thereof. The brush comprises conductive metal fibers and filling metal fibers. The length of the filling metal fibers is shorter than the length of the conductive metal fibers, one end of each filling metal fiber is flush with one end of each conductive metal fiber, the conductive metal fibers and the filling metal fibers are uniformly arranged along a length direction, and after compacting molding, the filling metal fibers and the conductive metal fibers are integrally wrapped by a metal wrapping sleeve. The preparation method comprises: winding the conductive metal fibers and the filling metal fibers together on a wire reel to form a metal fiber ring; and cutting the metal fiber ring, after the compacting molding, immersing one end of the metal fiber ring in an acid solution or aqueous alkali, and dissolving the filling metal fibers to obtain the metal fiber brush. The metal fiber brush is compact and reasonable in structure, high in fiber bonding strength, simple in preparation process, large in current carrying capability, small in contact resistance, long in service life, fast in sliding speed, small in heat productivity and small in debris amount, is suitable for industrial production, can replace a conventional carbon brush or a conventional metal fiber brush, and can satisfy the application demand for a large-power high-precision conductive slip ring.
Owner:CENT SOUTH UNIV

A preparation method of thermosensitive liposome with whitening effect

The invention relates to a preparation method of thermosensitive liposome with a whitening effect. The preparation method is characterized by comprising the following steps: A, weighing a whitening composition, liposome, a membrane stabilizer, ethyl alcohol, glycerol and deionized water; B, adding the liposome and the membrane stabilizer into the ethyl alcohol, stirring under the condition that the temperature is 20 to 25 DEG C and the rotating speed is 300 to 800 rpm till a mixture is completely dissolved; adding the glycerol and continuously stirring till the liquid becomes clear and transparent to obtain a lipid membrane mixed solution; C, adding the whitening composition into the lipid membrane mixed solution and stirring under the condition that the temperature is 20 to 25 DEG C and the rotating speed is 300 to 800 rpm till the liquid becomes clear and transparent to obtain a whitening agent and lipid membrane pre-mixed solution; D, adding the whitening agent and lipid membrane pre-mixed solution into the deionized water, stirring for 10 minutes under the condition that the temperature is 20 to 25 DEG C and the rotating speed is 300 to 800 rpm, putting into a refrigerator andreducing the temperature to 2 to 5 DEG C; then at the pressure of 1500 bar, homogenizing for 1 to 3 times by using a high pressure homogenizer, thus obtaining the thermosensitive liposome with the whitening effect. The thermosensitive liposome with the whitening effect, disclosed by the invention, has the beneficial effects of simultaneous loading of three whitening active substances, good whitening effect and thermosensitive characteristic after transdermal absorption.
Owner:苏州纳康生物科技有限公司

Making method of loquat, milk and lactic acid beverage

The invention discloses a making method of a loquat, milk and lactic acid beverage and relates to the technical field of beverage processing.The loquat, milk and lactic acid beverage is made from loquat leaves, licorice roots, rock candy powder, purified water and raw milk.The making method comprises the steps that the raw milk is firstly boiled, then the loquat leaves and the licorice roots are decocted into a solution, then the cooked milk and the purified water are poured into a jar for heating, then the rock candy powder is added, candy melts by using activated carbon to form syrup, the loquat leaf and licorice root solution is poured into the syrup, sterilization and cooling are performed, an acetic acid strain is inoculated in the cooled liquid for fermentation, strain control is conducted on the fermented liquid, and then acid adjustment is performed.The making method is simple in process, the steps are easy to control, the made loquat, milk and lactic acid beverage has a good, soft and refreshing taste, good quality and good stability.Due to the fact that the licorice roots and the loquat leaves are added, the loquat, milk and lactic acid beverage can prevent cough, excessive phlegm and other symptoms, further has the nutritional ingredients of lactic acid and moderate acidity and is suitable for people of all ages.
Owner:吴林媛

Processing method of lithium ion battery pole

The invention discloses a processing method of a lithium ion battery pole, which specifically comprises the following steps: step 1, preparing a base material, processing one end of a copper column into a step-shaped convex part, and processing an aluminum plate into a groove matched with the step-shaped convex part of the copper column; step 2, carrying out electroplating on the surface of the convex part of the copper column; step 3, coating the convex part of the copper column and the groove of the aluminum plate with metal brazing materials, and assembling the copper column and the aluminum plate; step 4, brazing the assembled copper column and the aluminum plate; step 5, removing an oxide layer and smudginess on the surface of a copper-aluminum composite pole; and step 6, carrying outoil removing and cleaning. Compared with a copper-aluminum friction welding process, the machining material utilization rate is high, the batch production efficiency is high, and the overall cost isreduced by about 30%. The copper-aluminum composite pole produced through the processing method is not prone to desoldering, the overall stability of the product is improved, and the overall weight islow. By use of the processing method, batch production can be achieved, equipment investment is low, production efficiency is high, and the production cost can be reduced.
Owner:广东九九华立新材料股份有限公司
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